使用Surfer软件绘制雨量等值线图

结合福建尤溪流域公司20050615号洪水某时段实际降雨情况,详细介绍了使用Surfer（以Surfer8.0为例）软件具体绘制雨量等值线图的制图原理和步骤,并说明绘制雨量等值线图需要注意的几个问题。在此应用中绘制雨量等值线图仅花费5min时间,说明使用Surfer软件绘制雨量等值线图具有速度快、效果好等特点,对水文、防汛管理工作有着实用的现实意义。     

Role of misfit in precipitation crystallography in non-ferrous metals

The crystallography and morphology of precipitates in different systems were rationalized based on the optimum matcing conditions. The interfaces that obey these conditions were conveniently identified in reciprocal space, in terms of three Ag＇s parallelism rules. The theoretic basis of the O-lattice and CSL/DSC theory for these rules was provided briefly. Examples of small lattice misfit system （a Ti alloy）, and large lattice misfit systems （A1 and Mg alloys） were presented. The effect of lattice parameters on the orientation relationship and morphology was also discussed.     

钒钛对贝氏体非调质钢组织与性能的影响

研究了微合金钒，钛对贝氏体型非调质钢的组织与性能的影响。结果表明在贝氏体型非调质钢中，钛的碳氮化物不但能细化奥氏体晶粒，还能促进钒的碳氮化物的析出，有利于提高钢的强韧性，在该负名的尚未观察到Ｖ（Ｎ，Ｃ）其析出相为富Ｔｉ，Ｎ的（Ｔｉ，Ｖ）（ＮＣ）。     

蛋白质沉淀分离

蛋白质一级、二级、三级和四级结构决定其物理、化学、生物化学、物理化学和生物学性质;该文综述不同蛋白质之间性质存在差异或改变条件使之具有差异,利用一种同时多种性质差异,在兼顾收率和纯度情况下,对其进行分离。     

Gravimetric determination of tannins and their correlations with chemical and protein precipitation methods

Abstract. A method for gravimetric determination of tannins based on binding with insoluble polyvinylpyrrolidone (PVP) is presented. The gravimetric method gives the absolute amount of tannins and avoids problems of standards associated with spectrophotometric methods. The method was applied to nine browse and tree leaves. The values obtained correlate significantly with tannins determined spectrophotometrically, protein precipitation capacities and protein precipitable phenotics. This method together with other tannin assays will be useful in nutritional studies. The present study also demonstrates the different behaviour of tannic acids from different commercial sources towards PVP suggesting the presence of different moieties in tannic acids from different commercial sources and even among batches from the same source thereby affecting the results obtained using the spectrophotometric methods. Use of well-defined tannic acid as a standard in spectrophotometric methods is suggested which will allow meaningful comparison of values obtained from different laboratories.     

Aggregation and Precipitation Kinetics of Canola Protein by isoelectric precipitation

Kinetics of aggregation, nucleation and growth of canola protein particles were developed in a 100 mL mixed-suspension mixed-product removal precipitator (MSMPRP) using isoelectric precipitation with HCI at pH 4.2. Protein yield in terms of total nitrogen was measured by Kjeldahl system. The size distribution of protein aggregates was determined by a Coulter counter. The effects of pH, protein concentration driving force, mean residence time, agitation rate, ionic strength of the solution, and the operating temperature on the size distribution and yield of protein particles were investigated. Population balance on the protein particles was used to derive empirical correlations for the index of aggregation, nucleation rate of primary particles and growth rate of protein aggregates.     

微波干燥制备Al2O3纳米粉体的研究

以AlCl3 和NH3 ·H2 O为原料 ,采用沉淀法制备Al2 O3 纳米粉体 ,利用XRD、TEM、DTA等分析测试手段对所得A12 O3 粉体的晶相组成、粒径分布等性质进行了研究 ,发现间歇式微波处理 10min后在 5 5 0℃加热 30min研磨可得到平均粒径小于 35nm的A12 O3 纳米粉体     

连续和离散系统的鲁棒严格正实性*

本文提出了一种统一的鲁棒严格正实性判定准则，既适用于连续系统，又适用于离散系统，在此准则的基础上，形成了鲁棒严格正实滤波器和补偿器的设计方法，当考虑的系统是线性参数摄动系统或由若干个独立线性参数摄动系统串联成的，则本文给出的是端点结果。     

GH169高温合金主要相分析

用透射电镜对GH169高温合金主要强化相γ′、γ″进行分析观察及稳定相δ的亚结构及有关晶体学的测量计算。结果得出,γ″相具有三种不同位向的变体。利用γ′、γ″在(110)倒易面上超结构斑点重合来同时显现γ′、γ″相。通过迹线分析方法测量得出δ相的亚结构为层错,层错面为。     

掺锗CZSi原生晶体中氧的微沉淀

利用锗硅单晶(锗浓度约为1019cm-3)切制成的籽晶和一般无位错硅单晶生长的缩细颈工艺以及从晶体头部至尾部平稳降低拉速的工艺,生长了直径为60、50和40mm,掺锗量为0.1%和0.5%(锗硅重量比)的锗硅单晶.利用化学腐蚀-金相显微镜法、扫描电子显微镜(SEM)能谱分析和X射线双晶衍射等方法观测了掺锗硅的原生晶体中缺陷及氧的沉淀的状况.发现用CZ法生长的锗硅原生晶体与常规工艺生长的CZSi晶体不同,体内存在着较高密度的氧微沉淀.在晶体尾部,由于锗的分凝使熔体中锗高度富集,出现了"组分过冷"现象,在晶粒间界应力较大处有锗的析出并出现了枝状结晶生长.晶体中高密度氧的微沉淀经过1250℃热处理1h后会溶解消失.