高速钢高温形变诱发析出的研究

本文探讨了高速钢在高温形变过程中碳化物析出的行为及奥氏体组织状态对析出的影响。用透射电镜和扫描电镜分析了不同热处理状态奥氏体的组织结构,分析了高温形变过程中碳化物析出的部位,颗粒尺寸及形态。试验表明, 碳化物主要在奥氏体的缺陷处呈点状和点列状析出,大小为20mμ。处于回复状态的奥氏体缺陷诱发碳化物析出,析出碳化物钉札缺陷阻止再结晶进行。当再结晶驱动力较大时,由于动态再结晶充分发展,使缺陷大量消除,碳化物析出显著地减少。     

Heat transfer mechanism of a swirling impinging jet in a stagnation region

Heat transfer characteristics of a swirling impinging jet have been experimentally examined using a combined particle image velocimetry (PIV) and laser‐induced fluorescence (LIF) technique for simultaneous measurement of velocity and temperature fields. The present study shows that the radial width of the jet stretches with increasing swirl intensity, and that the stretching phenomenon contributes to the maximum local heat transfer coefficient. At the stagnation region, the flow near the heated surface is mixed intermittently by reverse flows toward upstream, and spatial distributions of temperature are correlated with instantaneous velocity vector maps. The dynamic behavior of recirculation zones, attributed to swirl number Sw and impinging distance, mainly determines the turbulent heat transfer at the stagnation region. © 2003 Wiley Periodicals, Inc. Heat Trans Asian Res, 32(8): 663–673, 2003; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/htj.10120     

Organosoluble and light-colored fluorinated polyimides derived from 2,3-bis(4-amino-2-trifluoromethylphenoxy)naphthalene and aromatic dianhydrides

A novel fluorinated bis(ether amine) monomer, 2,3-bis(4-amino-2-trifluoromethylphenoxy)naphthalene, was prepared through the nucleophilic aromatic substitution reaction of 2-chloro-5-nitrobenzotrifluoride and 2,3-dihydroxynaphthalene in the presence of potassium carbonate, followed by catalytic reduction with hydrazine and Pd/C. A series of new fluorine-containing polyimides having inherent viscosities of 0.54 to 1.10 dl/g were synthesized from the diamine with various commercially available aromatic dianhydrides using a standard two-stage process with thermal imidization of poly(amic acid) films. These polyimides were highly soluble in a variety of organic solvents, and most of them afforded transparent, light-colored, and tough films with good tensile strengths. These polyimides exhibited glass transition temperatures (T_gs) of 247-300 °C and showed no significant decomposition below 500 °C under either nitrogen or air atmosphere. Except for the polyimide derived from pyromellitic dianhydride, the polyimide films were almost colorless, with an ultraviolet-visible absorption cutoff wavelength below 400 nm and low b∗ values (a yellowness index) of 10.7-41.9. These polyimides had dielectric constants of 3.09 to 3.65 (1 MHz) and moisture absorptions in the range of 0.2-0.3 wt%.     

Combined PIXE and SEM study of the behaviour of trace elements in gel formed around implant coated with bioactive glass

Bioactive glasses are used as coating biomaterials to facilitate anchorage of metallic prostheses implanted into the body. The aim of this work is to study the behavior of gel formed in contact with alloys and BVA and BVH bioactive glasses implanted. Cylinders of metallic implants composed by Ti, Al and V, are coated with bioactive glass. Three sheep were implanted for different time length: 3, 6 and 12 months in the femoral epiphysis. Results obtained with particle induced X-ray emission and scanning electron microscopy show that BVA coating induces a better contact between the metallic implant and bone. On the other hand, BVH coating prevents corrosion from the metallic implant.     

高分子材料辐射接枝苯乙烯的研究进展

对各高分子材料辐射接枝苯乙烯的动力学，接枝方法及接枝材料的应用进行了综述，讨论限辐射剂量，剂量率，温度，后效应，溶剂，添加剂和高分子材料厚度及结晶性等方面对接枝反应的影响。     

MBS树脂改性PVC的研究

研究了不同类型及用量的MBS树脂对PVC抗冲击性、光学性能、拉伸性能及加工塑化性能的改性效果以及加工条件等因素的影响。结果表明 :在低用量条件下 ,随MBS树脂含量增加 ,MBS/PVC抗冲击性能有所提高 ,光学性能略有下降。此外 ,MBS/PVC制品的拉伸性能和加工性能受MBS树脂类型及用量影响不大。     

Ionoluminescence decay measured with single ions

A new ion beam analysis-based, single ion technique called the time to first photon has been developed to measure the decay of the luminescence signal of phosphors. Such measurements are currently needed to study luminescence decay mechanisms following high-density excitations and to identify strongly luminescent phosphor coatings with short lifetimes for ion photon emission microscopy (IPEM). The samples for this technique consist of thin phosphor layers placed or coated on the surface of PIN diodes. Single ions from an accelerator strike this sample and simultaneously create ion beam induced luminescence (IBIL) from the phosphor that is measured by a single-photon-detector, and an ion beam induced charge collection (IBICC) signal in the PIN diode. In this case, the IBICC signal provides the start pulse and the IBIL signal the stop pulse to a time to amplitude converter. It is straightforward to show that this approach also measures a signal proportional to activity versus time with an accuracy of 5% as long as the number of detected photons per ion is less than 0.1, which usually requires the use of absorbers for the IBIL detector or electronic discrimination for the IBIL signals. Details of the new analysis are given together with examples of luminescence decay measurements of several ceramic phosphors being considered to coat IPEM samples. IPEM is currently being developed at Sandia National Laboratory (SNL), the University of North Texas in Denton, and the Universities and INFN of Padova and Torino.     

Measurements of turbulent mass transport of a circular wall jet

The results of a laboratory investigation on the turbulence characteristics of a circular three-dimensional turbulent wall jet are presented. Measurements were taken up to 50 nozzle diameters using combined particle image velocimetry and planar laser induced fluorescence. The results showed that the induced turbulence was still evolving in the present range and had not achieved similarity. While the turbulent intensity for both velocity and concentration increased downstream, the turbulent mass transport showed a decline over distance for both the streamwise and spanwise directions, implying weakening dispersion from the jet core.     

Semantic Transparency,Brain Monitoring and Evaluation of Hybrid Cognitive Architectures

In constructing hybrid systems, there is a need for a principled basis to determine the relative roles or functions of artificial neural network and symbolic approaches. The primary objective of the work to be reported is the construction of a conceptual and methodological framework that permits an iterative sequence in which a hybrid model predicts the basis of cognitive performance and an objective analysis of performance provides empirical data, evaluating (and thus constraining) the structure and processes of the model. In seeking a linkage between a hybrid model of cognition and human performance the concept of “semantic transparency” has been adopted, since it can be used in analyzing and describing both the chracteristics of a model of cognition and the processes underlying human performance. An overview of a specific, ”strong” hybrid architecture is presented. The characteristics of the virtual machines which compose it and the nature of their interaction are illustrated. An approach to the questions of evaluation is described based on empirical data obtained by brain monitoring of subjects during cognitive performance.     

水文自动测报系统防雷的探讨

水文自动测报系统若配备有线／无线（GSM，GPRS）双通道，可提高系统的可靠性，保证系统的畅通。然而，有线组网方式最致命弱点是防雷能力差，针对防雷问题，在实践中探讨其有效途径，论述接地装置的设计、安装中应注意的几个问题，并介绍在实践中电话线防雷从一级防护发展到三级防护，提高防雷的效果，有待在实践中，再认识，再提高。