连续多跨大柱距空旷厂房的空间结构设计

以鞍钢大型厂房改造工程为例,介绍了一种打破常规的空间设计方法,并阐述了大跨度吊车桁架支座、节点等重要传力部位的构造形式及其利弊,可供同类工业厂房改造工程设计时参考。     

A new amperometric biosensor for fructose determination based on epoxy-graphite-TTF-TCNQ-FDH-biocomposite

In this work a novel amperometric biosensor for fructose determination in solutions was developed. The device was constructed by the incorporation of a tetrathiofulvalene-tetracyanoquinodimethane organic conducting salt and fructose dehydrogenase enzyme, include in a polymeric matrix of epoxy resin and graphite powder. Because of the electrocatalytic function of the salt, the direct transfer of the electron between the reduced prosthetic group (PQQH₂) of the enzyme and the transducing material, was verified at a low working potential (150 mV vs. Ag/AgCl), where the interfering reactions were minimized. The response time at 90% of the steady state value was less than 20 s. The current response was directly proportional to the D-fructose concentration from 0.01 to 0.3 mmol/l with a detection limit of 0.005 mmol/l (signal/noise of 3) and a sensitivity of 1.9985 μA/mmol. The biosensor sensitivity diminishes when its surface is not polished between successive determinations, and remains constant (rsd=1.85, n=10) when the surface is polished between determinations. The effects of temperature and pH on the biosensor response were studied and analyzed; also the properties of the enzyme (Km _ap, I _max, Q₁₀) were determinate in this work. The biosensor was used to determine fructose in high fructose syrups and there were not significant differences between these results and those obtained by HPLC (p≤0.05). During 4 months, in intermittent determinations the biosensor kept 100% of its original sensitivity and after 18 months stored at 4°C, it only lost 32% of its sensitivity. The simplicity, low working potential, high stability and good performance of this biosensor shows a great potential for its use in the fructose determination.     

EASY2000色谱处理系统在酒样色谱分析中的运用

介绍了EASY2000色谱处理系统在酒类产品分析实际应用过程中的方法，步骤，特点及注意事项等。     

XRF法测定高岭土中的主次量元素

采用X射线荧光光谱法取代原有的化学法，分析了高岭土中的9种主次量元素。通过对测定条件的选择以及样品制备等方面的考察，制定出最佳分析方案。分析结果表明，该方法准确、可靠，分析周期由原来的6h缩短为10min.     

示差光度法测定钛铁中钛含量

采用示差光度法测定钛铁中钛含量，钛的测定范围10．00％～30．00％，满足炼钢生产中的快速测定。     

混凝土框架节点有限元分析

以文献[4]中所做的碳纤维布加固节点的试验为依据,应用ANSYS程序对其中的试件2进行单调加载情况下的全过程数值模拟计算,最后通过数值计算结果与试验结果在承载能力、裂缝开展及破坏形态等方面的比较,来验证应用ANSYS程序模拟碳纤维布加固钢筋混凝土框架节点抗震性能试验的有效性和可行性。     

不锈钢网架结构试验研究

对奥氏体不锈钢网架结构的物理力学性能、焊接性能加以分析，并进行了不锈钢焊接空心球节点承载力试验，确定了该种节点的受拉和受压承载能力。在此基础上，又做了不锈钢组合扭网壳模型的破坏性试验研究，试验结果与理论计算值比较，吻合较好。     

Real-time accurate hand path tracking and joint trajectory planning for industrial robots (I)

Previously, researchers raised the accuracy for a robot’s hand to track a specified path in Cartesian space mainly through increasing the number of knots on the path and the number of the path’s segments, which results in the heavier online computational burden for the robot controller. Aiming at overcoming this drawback, the authors propose a new kind of real-time accurate hand path tracking and joint trajectory planning method. Through selecting some extra knots on the specified hand path by a certain rule and introducing a sinusoidal function to the joint displacement equation of each segment, this method can greatly raise the path tracking accuracy of robot’s hand and does not change the number of the path’s segments. It also does not increase markedly the computational burden of robot controller. The result of simulation indicates that this method is very effective, and has important value in increasing the application of industrial robots. Foundation item: Foundation of the Robotics Laboratory, Chinese Academy of Sciences (No. RL200002) Biography of the first author: TAN Guan-zheng, Dr., professor, born in Oct. 1962, majoring in artificial intelligence, robotics and automation.     

原子吸收分光光度法测定焦锑酸钾中锑含量

比较详细地研究用火焰原子吸收分光光度法测定焦锑酸钾中锑含量的技术条件和测定方法。     

从76届SEG年会看综合物化探技术的发展方向

文中在介绍76届SEG年会的展商、展台及会场专题报告与论文发布情况的基础上，阐述了参加本届SEG年会的体会，指出了重磁电技术发展的四个趋势：向海洋勘探技术方向发展、向复杂区综合勘探技术方向发展、向三维联合处理和三维可视化解释技术发展、向直接圈定和检测油气方向发展。