Analysis of lipid classes by solid-phase extraction and high-performance size-exclusion chromatography

An improved method to analyze lipid classes of edible oils and fats by solid-phase extraction (SPE) and high-performance size-exclusion chromatography (HPSEC) is presented. A mixture of lipid standards was fractionated by the solid-phase extraction procedure (NH₂ phase) into polar and nonpolar fractions; these were then submitted to analysis by HPSEC. The size-exclusion chromatographic columns were three styrene/divinylbenzene columns with pore sizes of 100 Å and 50 Å. Light-scattering was used for the detection system, and the parameters of the detector were optimized to minimize the difference between the responses of the compounds studied. With this procedure it was possible to separate the following lipid classes: triacylglycerols, diacylglycerols, monoacylglycerols and free fatty acids, sterols, sterol esters, tocopherols and carotenoids. Quantitative analysis was studied for a light-scattering detector with several lipid standards of different molecular weights and unsaturation levels.     

光伏锑化铟红外探测器的老化现象与处理

光伏锑化铟红外探测器在长期使用过程中会逐渐老化,出现一些如等效阻抗降低、噪声增大等现象。本文叙述了闪光处理对于降低这类老化的探测器的噪声特别有效,加上一些清洁措施,已使一个工作了6年多的探测器基本上恢复了性能。     

近红外仿灸仪的研制与临床应用

近红外仿灸仪,也称为经络灸疗仪,是采用我国传统医学与现代科学技术相结合而研制成的一种新型中医治疗、保健仪器,可以用于治疗多种疾病。本仪器根据艾灸燃烧时所辐射的光谱,运用仿真技术进行模拟,根除了传统灸法燃烧缓慢、效率不高、烟雾较大、刺鼻熏眼、易于灼伤、操作不便等缺点,充分发挥了我国传统灸法的温经通络、补气活血、化瘀消肿,祛湿止痛的功效。     

IR Radiometry Optical System View Factor and Its Application to Emissivity Investigations of Solid and Liquid Phases

An optical system for fast IR radiometry designed for investigations of thin film thermal properties and pulsed laser melting was analyzed in this work. A methodology for determination of the view factor from calibration measurements was developed. The view factor (0.0255) of the optical system containing two paraboloid mirrors was determined experimentally from calibration measurements on pure metals and metallic alloys. The knowledge of the view factor was then applied to normal emissivity investigations at IR wavelengths. The emissivity of tungsten films prepared by magnetron sputtering was determined for different deposition conditions, varying between 0.036 and 0.071. Liquid phase emissivities of Cu, Mo, Ni, Si, Sn, Ti, and steel were also determined and were found to be higher than solid-state emissivities as predicted from the literature. A knowledge of the liquid-state emissivity of silicon enabled recalculation of the IR signal evolution to the temperature evolution, during and after a nanosecond laser pulse. This was not possible by use of the usual calibration because of silicon’s semi-transparent behavior in the IR range (1–10 μm) in the solid-state phase.     

红外加热节能技术的现状与发展前景

本文综述了国内外节能的现状与发展趋势,论述了远红外电加热领域的发展前景,强调了加强基础理论研究的重要性,介绍了我国红外加热应用的领域和国外新开发的红外产品。     

红外警戒系统的运动参数估计算法

通过对目标飞行轨迹的参数化建模，提出了由红外传感器对目标角度和辐射功率的测量实现对目标距离和其它位置、速度参数估计的算法，从而可以此作为目标威胁程度估计和目标特性识别的依据。仿真计算表明，该方法计算的精度高，对目标位置的初始先验值依赖程度较小。该算法也适合于其它测量体制的目标运动参数估计。     

应用ITO膜作电荷收集极的位置灵敏探测器

首次尝试将ITO（Indium Tin Oxide）膜与微通道板（Microchannel Plate）结合用作位置灵敏探测器，并对该探测器的线性、位置分辨及探测效率作了测试，得到了令人满意的结果。     

铑自给能中子探测器的灵敏度

本文给出了铑自给能探测器的热中子灵敏度和中子灵敏度的理论计算公式、燃耗修正公式以及不同中子温度下的换算公式。运用这些公式对ZTRh 123型铑自给能探测器的热中子灵敏度和中子灵敏度进行了理论计算,并在反应堆中对其进行了实验验证。其结果表明,理论计算值和实验标定值是相吻合的。其偏差:热中子灵敏度为8.5％,中子灵敏度为3.9％。     

锅炉炉膛红外成像温度实时检测系统研究

说明电厂锅炉炉膛温度及结焦直接影响锅炉正常运行及安全；给出了基于多探测器的锅炉反应温度红外成像实时测温系统的系统结构、系统原理、系统标定和温度测定方法。     

体积-表面淬火中加热温度的自动控制

根据表面-体积淬火奥氏体规范的要求，分析了感应加热过程中温度控制的特点和方式，并介绍了采用红外线光导纤维测温和微机控温技术成功用于体积-表面淬火中透热温度的自动控制。