全文获取类型
收费全文 | 22607篇 |
免费 | 1690篇 |
国内免费 | 1310篇 |
专业分类
电工技术 | 281篇 |
综合类 | 1035篇 |
化学工业 | 3711篇 |
金属工艺 | 8666篇 |
机械仪表 | 863篇 |
建筑科学 | 184篇 |
矿业工程 | 417篇 |
能源动力 | 593篇 |
轻工业 | 341篇 |
水利工程 | 8篇 |
石油天然气 | 384篇 |
武器工业 | 157篇 |
无线电 | 673篇 |
一般工业技术 | 5409篇 |
冶金工业 | 2433篇 |
原子能技术 | 266篇 |
自动化技术 | 186篇 |
出版年
2024年 | 85篇 |
2023年 | 474篇 |
2022年 | 603篇 |
2021年 | 777篇 |
2020年 | 860篇 |
2019年 | 717篇 |
2018年 | 677篇 |
2017年 | 811篇 |
2016年 | 671篇 |
2015年 | 741篇 |
2014年 | 1091篇 |
2013年 | 1450篇 |
2012年 | 1241篇 |
2011年 | 1771篇 |
2010年 | 1153篇 |
2009年 | 1325篇 |
2008年 | 1052篇 |
2007年 | 1363篇 |
2006年 | 1393篇 |
2005年 | 1160篇 |
2004年 | 1063篇 |
2003年 | 883篇 |
2002年 | 664篇 |
2001年 | 558篇 |
2000年 | 480篇 |
1999年 | 395篇 |
1998年 | 333篇 |
1997年 | 324篇 |
1996年 | 248篇 |
1995年 | 222篇 |
1994年 | 187篇 |
1993年 | 126篇 |
1992年 | 137篇 |
1991年 | 87篇 |
1990年 | 97篇 |
1989年 | 78篇 |
1988年 | 35篇 |
1987年 | 35篇 |
1986年 | 39篇 |
1985年 | 22篇 |
1984年 | 29篇 |
1983年 | 26篇 |
1982年 | 33篇 |
1981年 | 19篇 |
1980年 | 19篇 |
1979年 | 12篇 |
1978年 | 15篇 |
1977年 | 6篇 |
1976年 | 8篇 |
1975年 | 8篇 |
排序方式: 共有10000条查询结果,搜索用时 305 毫秒
41.
冷轧形变量对钛板材再结晶织构形成的影响 总被引:1,自引:0,他引:1
采用三维晶体学取向分布函数(CODF)分析法研究了工业纯钛板材不同冷轧形变量对织构形成的影响。结果表明,冷轧形变量为50-70%时,再结晶退火后形成了(2118)(0110)和(1018)(1210)的部分纤维织构,而在30%较低或86%较高的形变量冷轧时,形成典型的轧制织构(2115)(0110)和再结晶织构(1013)(1210)型式。 相似文献
42.
Hyun-Goo Kim Wha-Nam Myung K. Sumiyama K. Suzuki 《Journal of Alloys and Compounds》2002,340(1-2):270-274
We report upon the chemical leaching and magnetic properties of nanoscale crystalline Al0.6(Co25Cu75)0.4 alloy powders produced by rod milling. X-Ray diffractometry (XRD), transmission electron microscopy, differential scanning calorimetry, vibrating sample magnetometry, and superconducting quantum interference device magnetometry were used to characterize the as-milled and leached specimens. After 400 h of milling, only the b.c.c. phase of the intermetallic compound γ-Al3.892Cu6.10808 was detected by XRD. After annealing the leached specimen at 600 °C for 1 h, the nanoscale crystalline phase was transformed into the f.c.c. Cu phase, and this was accompanied by a change in the magnetic properties. The peaks of the magnetization shifted towards lower temperature with increasing external field. The temperature behavior at Tf (45 K) for direct current (d.c.) magnetic susceptibility measurements was quite different for field cooling and zero-field cooling. After cooling the leached specimen from 800 °C, magnetization increased gradually. 相似文献
43.
Thin films on aluminum-tungsten alloys were prepared by co-deposition of pure aluminum and pure tungsten, each sputtered by an independently controlled magnetron source, on glass and sapphire substrates. Completely amorphous films were obtained in the Al80W20-Al67W33 composition range. Passivity and corrosion behavior of amorphous Al-W alloys were investigated in 1 M deaerated hydrochloric acid solution using polarization and impedance spectroscopy measurements and have been correlated with the properties of pure alloy components. Tungsten and sputter-deposited Al-W thin films are inherently passive materials while aluminum undergoes pitting corrosion in hydrochloric acid solution. The passive film formed at the OCP on each alloy possesses excellent electric and dielectric properties comparable to those of the isolating film on tungsten. The absolute impedance increases with increasing tungsten content in the alloy. According to electrochemical polarization measurements, alloying Al with W in solid solution significantly enhances the material's resistance to pitting corrosion by shifting the breakdown potential above 2000 mV (Al67W33) and lowering the corrosion rate at the OCP by more than two orders of magnitude. The most likely mechanism explaining the passivity of amorphous Al-W alloys, the Solute Vacancy Interaction Model (SVIM), involves the formation of complexes between highly oxidized solute atoms (W+6) and mobile cation vacancies, which restrict the transport of Cl− through the oxide film and inhibit its breakdown in hydrochloric acid solution. The role that film stress relaxation effects and microscopic defects in amorphous Al-W films, of the some composition, and deposited on various substrates play in their corrosion resistance is discussed. 相似文献
44.
45.
The Synthesis of Sulfated Titanium Oxide Nanotubes 总被引:1,自引:0,他引:1
Chiu-Hsun Lin Shu-Hua Chien Jiunn-Hsing Chao Chyi-Yang Sheu Yu-Cheng Cheng Ya-Jean Huang Chih-Hsiang Tsai 《Catalysis Letters》2002,80(3-4):153-159
TiO2 nanotubes can be prepared in gram quantities by treating anatase TiO2 powder with concentrated NaOH solution. These TiO2 nanotubes acquired strong acidity after being impregnated with sulfuric acid solution and calcined at 300 °C. The anatase TiO2 powder used to prepare the nanotube did not catalyze the esterification between cyclohexanol and acetic acid, while sulfated TiO2 nanotubes were very reactive toward the esterification reaction. 相似文献
46.
47.
A new method of studying the corrosion inhibition mechanism of rare earth metal(REM) on LC4 Al alloy with the spilt cell technique was studied. The principle and experimental method of the spilt cell technique were analyzed. By measuring the change of net-electric current between the two electrodes caused by the change of the amount of oxygen in the solution and the addition of CeCl3, the influence of corrosive performance of CeCl3 on LC4 super-power aluminum alloy in the 0.1 mol·L−1 NaCl solution was investigated. Meanwhile, the conditional changes of pH values, CeCl3 solution, additire and time of performance were also studied. Finally, the features of electrode surface were revealed by using SEM and X-ray energy-dispersive spectrometry (EDS). By combining these with other electric chemical techniques, such as potential-time curve, polarization curve et al. 相似文献
48.
49.
M. Guerioune Y. Amiour W. Bounour O. Guellati A. Benaldjia A. Amara N. E. Chakri M. Ali-Rachedi D. Vrel 《International Journal of Self-Propagating High-Temperature Synthesis》2008,17(1):41-48
Aiming at preparation of shape memory alloys (SMAs), we explored the SHS of Cu1 − x
Zn1 − y
Al1 − z
alloys (0.29 < x < 0.30, 0.74 < y < 0.75, and 0.83 < z < 0.96). The most pronounced shape memory effect was exhibited by the alloys of the following compositions (wt %): (1) Cu(70.6)Zn(25.4)Al(4.0),
(2) Cu(70.1)Zn(25.9)Al(4.0), and (3) Cu(69.9)Zn(26.1)Al(4.0). The effect of process parameters on the synthesis of CuZnAl
alloys was studied by XRD, optical microscopy, and scanning electron microscopy (SEM). The grain size of CuZnAl was found
to depend on the relative amount of the primary CuZn and AlZn phases. Changes in the transformation temperature and heat of
transformation are discussed in terms of ignition intensity and compaction. Mechanism of the process depends on the level
of the temperature attained relative to the melting point of components. At the melting point of AlZn, the process is controlled
by the solid-state diffusion of AlZn into a product layer. The ignition temperature for this system depends on the temperature
of the austenite-martensite transformation in CuZnAl alloys. The composition and structure of the products was found to markedly
depend on process parameters. The SHS technique has been successfully used to prepare a variety of SMAs.
相似文献
50.
Vibration cavitation erosion tests were carried out on Ni-Mn-Ga alloys of three different crystal structures: (1) the cubic austenite, (2) the non-modulated tetragonal martensite (T) and (3) the five-layered martensite (5M). All Ni-Mn-Ga alloys exhibited cavitation behaviour characterized by a step-wise curve of mass loss versus test time. This behaviour is correlated to the microstructural nature of the alloys as well as the surface conditions of the pre-test samples. The type and concentration of the defects at the surfaces were critical to the cavitation resistance of the alloys. The best cavitation resistant alloy was of a cubic austenitic structure, followed with the alloy of a tetragonal T-martensite. The largest material loss was found in the alloy with a 5M martensite. All the studied Ni-Mn-Ga alloys had an excellent cavitation resistance compared to that of the reference stainless steel, and they even excelled some NiTi alloys found in literature. This may be due to the superelasticity of the cubic austenite and the twinning of the martensitic phases. 相似文献