Melting and crystallization behaviour of elastoplastic semicrystalline copolymers: poly(ether ester)

The melting and crystallization behaviour of an elastoplastic semi-crystalline poly(etherester) has been studied by differential scanning calorimetry. The shape of the melting endotherm is strongly dependent on heating rate and annealing time and results from the sum of simultaneous melting and crystallization phenomena. Samples prepared by different techniques, i.e. by solvent evaporation or by melt extrusion, behave very differently owing to specific crystal morphologies. By applying the Hoffman-Weeks plot, the equilibrium melting temperature has been extrapolated. The Avrami treatment allows the calculation of the index n and of the rate constant K from the isothermal kinetic data.     

硅酸铋晶体的蚀像形貌

本文研究了提拉法生长的硅酸铋晶体(BSO)的蚀像形貌,比较了{100},{110},{211},{111}面族的腐蚀像特征和腐蚀速度,并用周期性键链(PBC)的形貌理论分析了腐蚀形貌。通过蚀像形貌特征便可方便地进行晶体定向,准确地确定各族晶面之间的相对位置和极轴的方向等。     

Properties of ligno‐cellulose fiber Hildegardia

Studies on some properties such as the density, the degradation temperatures, the morphology and the spectral features of the ligno‐cellulose fiber Hildegardia were carried out in both untreated and alkali treated form. The fibers are found to have good morphology and moderate initial and final degradation temperatures. On alkali treatment, the lignin was found to be eliminated. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 2216–2221, 2002     

城市建设的休克疗法——大连现象解说

在启动大规模的现代化建设的进程中，应对发展中听中型城市实施“休克疗法”，强调性终止城市发展的无序而缓慢的自然进程。选择短暂的“回归”或“中断”历史的调整时，应以能否适当地的历史文化特质从而把握当代的发展机遇为依据。     

Effect of heating-rate on failure temperature of pre-loaded brass H62

The response and failure of brass H62 specimens subjected to different levels of pre-loaded stresses and heating rates were investigated using a Gleeble-1500 thermal-mechanical material testing system. The metallographs of the tested material were also observed and analyzed. It is found that the increase of either pre-loaded stress or heating-rate decreases the failure temperature. Metallographic analysis shows that high heating-rate may cause stronger local thermal inconsistency （LTI） and remarkably increase the microdefects in the material, which may markedly degrade the macroscopic mechanical properties of the material.     

一个光纤综合业务环网的故障自动恢复

光纤综合业务区域网是近年来迅速发展的一个领域，环形网是这种网最常用的一种拓扑结构。由于环形网结点串联的特点，网络的可靠性是必须解决的问题。本文针对一个具有３４Ｍｂ／ｓ速率，可以传输计算机数据、话音、传真和会议电视的光纤综合业务环网（ＩＳＲ），研究了其故障的自动隔离。文中分析了ＩＳＲ的故障，讨论了故障的检测、定位和隔离的方法。为了适应综合业务的混合电路交换和分组交换技术，本文提出了采用二分搜索法来定     

局部施肥对植株生长及根系形态的影响

本文论述了局部施肥对植株地上部与地下部的影响。局部施肥促进了施肥区根系的发达 ,第一侧根与第二侧根较多 ,根的吸收表面积增多 ,根鲜重增加 ,对养分的吸收能力增强 ,但整个根系与地上部的干鲜重下降。     

局域网视频广播接收器的设计

描述了一个局域网视频广播接收器的设计。发送端以计算机按UDP/IP的方式向局域网中发送视频广播，在接收端利用FPGA器件设计的接收器对广播进行接收、缓冲、格式转换，以电视作为显示终端，并介绍了在FPGA器件中所设计的各个模块。     

自适应指纹预处理算法

基于大量的实验提出了一套行之有效的指纹处理算法，主要包括使用基于方向图的自适应旋转滤波器、与自适应增强滤波同时进行的自适应阀值边缘处理、自适应阀值二值化，很好地增强了指纹图像的清晰度，同时起到了很好的滤波作用，为可靠、准确地实现指纹自动识别系统奠定了最可靠的基础．     

Surface tailoring of an ethylene propylene diene elastomeric terpolymer via plasma‐polymerized coating of tetramethyldisiloxane

In the research presented here, we explore the use of a low‐energy plasma to deposit thin silicone polymer films using tetramethyldisiloxane (TMDSO) (H(CH₃)₂? Si? O? Si? (CH₃)₂H) on the surface of an ethylene propylene diene elastomeric terpolymer (EPDM) in order to enhance the surface hydrophobicity, lower the surface energy and improve the degradation/wear characteristics. The processing conditions were varied over a wide range of treatment times and discharge powers to control the physical characteristics, thickness, morphology and chemical structure of the plasma polymer films. Scanning electron microscopy (SEM) shows that pore‐free homogeneous plasma polymer thin films of granular microstructure composed of small grains are formed and that the morphology of the granular structure depends on the plasma processing conditions, such as plasma power and time of deposition. The thicknesses of the coatings were determined using SEM, which confirmed that the thicknesses of the deposited plasma‐polymer films could be precisely controlled by the plasma parameters. The kinetics of plasma‐polymer film deposition were also evaluated. Contact angle measurements of different solvent droplets on the coatings were used to calculate the surface energies of the coatings. These coatings appeared to be hydrophobic and had low surface energies. X‐ray photoelectron spectroscopy (XPS) and photoacoustic Fourier‐transform infrared (PA‐FT‐IR) spectroscopy were used to investigate the detailed chemical structures of the deposited films. The optimum plasma processing conditions to achieve the desired thin plasma polymer coatings are discussed in the light of the chemistry that takes place at the interfaces. Copyright © 2004 Society of Chemical Industry