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101.
研究建立了同时测定三磷酸胞苷二钠中乙醇、丙酮、氯甲醚、甲苯、苯乙烯5种有机溶剂残留量的毛细管气相色谱法。样品以乙腈为溶剂,经DB-FFAP(30 m×0.32 mm×0.25μm)毛细管柱分离,氢火焰离子化检测器检测,这5种有机溶剂呈良好的线性响应,平均回收率在98.3%~99.5%,精密度RSD在0.21%~1.92%,最低检出限可达5.0~7.5 mg/kg。本方法简单、灵敏、准确,完全能满足药品中所述有机溶剂残留量的测定要求。 相似文献
102.
103.
The process of grinding soybeans to a fine flour and extracting the flour with hexane was studied on a pilot plant scale.
The crude oil from the pilot plant study had 15 ppm phosphorus and was suitable for physical refining after a light acid pretreatment
and bleaching. The refined oil showed a Lovibond color of 1.4 yellow and 0.3 red. The pilot plant study also showed that grinding
of the soybeans and the separation of solid from miscella were the most difficult steps in solvent extraction with fine flour.
A laboratory study on separation of miscella from meal by aqueous ethanol reduced the hold-up volume, but it did not remove
all the miscella. A test with betacarotene showed that only the miscella outside the flour particles was displaced.
Aqueous ethanol solutions used as a second solvent extracted additional nontriglyceride materials (primarily phospholipids)
from the meal. Also, the free fatty acid content of the oil was increased with aqueous ethanol solution wash. The quality
of the extracted crude oil was lowered by using a second solvent, but it had the advantage of needing only one centrifugation
to separate miscella from meal. 相似文献
104.
105.
大压差减温减压是能的严重贬值。根据公司供热现状,分析了热电联产的可行性,利用蒸汽余压发电后,再供生产系统各热用户,这样既节约了能源又缓解了集团公司用电紧张的局面,而且有相当可观的经济效益。 相似文献
106.
107.
108.
本文报道了用气相色谱法同时测定油墨中的正丁醇、丁酮、甲苯、乙酸丁酯、二甲苯、环己酮,这方法具有良好的精密度、回收率和线性关系,测定了四种油墨所含的溶剂。 相似文献
109.
Hydrogen transfer from donor solvent to coal must involve reactions such as hydrogen donation to free radicals and hydrogenation of aromatic structures. The relative reactivities of five typical hydrogen donor solvents, more reactive than tetralin, were determined using a competing elimination reaction in the liquefaction of a bituminous coal at 400 °C and a brown coal at 350 °C. 9,10-Dihydroanthracene, 9,10-dihydrophenanthrene and 1,2,3,4-tetrahydroquinoline exhibited outstanding hydrogen donating ability. Further, the relative reactivities of five mild hydrogen donor solvents such as acenaphthene and indan were determined by a similar elimination reaction using a bituminous coal at 450 °C. 相似文献
110.
The intrinsic viscosities of eleven narrow molecular weight distribution polystyrene samples ranging from number-average molecular weight 1820 to 1 292 000 have been determined in pure solvents of tetrahydrofuran and chloroform with a Ubbelohde No. 1 viscometer at 25°C. By combining the original and modified Fox-Flory viscosity treatments, respectively, with the Flory-Huggins Lattice theory, the interaction parameters were calculated. With the aid of original and modified UNIFAC methods the solvent activity, clustering function of the solvent, and the interaction parameter were computed and compared with the experimental data. It was established that the influence imposed by the polymer molecular weight on the activity of the solvent, the clustering function of solvent, and interaction parameter is insignificant. The modified UNIFAC method satisfactorily predicted the solvent activity as illustrated by previous investigators. However, both UNIFAC methods failed to predict the interaction parameter. 相似文献