激光超塑性成型技术研究

本文探讨了激光超塑成型技术中所涉及的合金板材制备、光能耦合及成型工艺，给出了标样拉伸实验和实际工件成型的结果，并对金相组织进行了分析．     

光柱显示技术探讨

本文叙述自动化仪表用光柱显示技术的工作原理及器件结构，重点论述直流等离子体光柱，发光二极管光柱，真空荧光及液晶光柱器件的结构和驱动电路，还展望光柱显示的发展趋势。     

K418B合金细晶铸造整体涡轮真空热处理工艺研究

通过力学性能评估和金相组织观察，研究五种热处理制度，两个周期的试验结果，确定了Ｋ４１８Ｂ合金细晶铸造整体涡轮的真空热处理工艺。     

热镀锌渣真空蒸馏回收锌

在钢件热镀锌过程中，产出约占锌总量１０％的热镀锌渣，渣中含锌和少量铁，铅，铜，铝等杂质。用直空蒸馏方法从热镀锌渣中提取锌；具空度１．３３×１０＾２－１．３３×１０＾３Ｐａ，温度９００℃，作业时间１１ｈ／炉，电耗约２０００度／ｔ锌，试验表明，锌的直收离可达８４％，为热镀锌渣中锌的回收提供了一英经济而合理的方法。     

High concentration erbium doping of silicon-rich SiO2 thin films on silicon

In this work, high concentration erbium doping in silicon-rich SiO₂ thin films is demonstrated. Si plus Er dual-implanted thermal SiO₂ thin films on Si substrates have been fabricated by using a new method, the metal vapor vacuum arc ion source implantation with relatively low ion energy, strong flux and very high dose. X-Ray photoelectron spectroscopy measurement shows that very high Er concentrations on the surfaces of the samples, corresponding to 10 at.% or the doping level of 10²¹ atoms cm⁻³, are achieved. This value is much higher than that obtained by using other fabrication methods such as the high-energy ion implantation and molecular beam epitaxy. Reflective high-energy electron diffraction, atomic force microscopy and cross-section high-resolution transmission electron microscopy observations show that the excess Si atoms in SiO₂ matrix accumulate to form Si clusters and then crystallize gradually into Si nanoparticles embedded in SiO₂ films during dual-ion implantation followed by rapid thermal annealing. Er segregation and precipitates are not formed. Photoluminescence at the wavelength of 1.54 μm exhibits very weak temperature dependence due to the introduction of Si nanocrystals into the SiO₂ matrix. The 1.54-μm light emission signals from annealed samples decrease by less than a factor of 2 when the measuring temperature increases from 77 K to room temperature.     

第二套常减压装置低温热回收技术的应用

常减压装置低温余热较多.利用较少,造成热量损失。利用初顶油气、稳定石脑油等低温余热加热除盐水建立热水站,在节汽、节电等方面取得了较好的效果。     

活性碳和5A分子筛的吸附特性及其在真空获得中的作用

评述了活性碳和５Ａ分子筛的吸附等温线及其在真空佩温绝热夹层真空获得中的作用。分析了真空夹层抽真空除气时用Ｎ＿２气置换以及用“多次吸附－脱附Ｎ＿２气”方法活化吸附剂等先进工艺的机理。论述了根据吸附剂吸水的吸附等温线，合理确定活化工艺条件的方法。     

中置式高压电容器柜改进设计

分析了南屯煤矿白马河风井变电所高压电容器柜原设计方案存在的问题,并对其进行了改进设计:选用适用于容性负载的真空断路器;添加放电线圈,并将放电线圈与电容器直接并联,使放电线圈与电容器组成一个完整的放电回路;添加接地开关,接地开关既有机械闭锁又有电气联锁,操作方便,安全性高。实际应用表明,改进设计后的高压电容器柜功能更加完善,更加安全、可靠。     

Fabrication of Nano-TiO2 Coating for Dye-Sensitized Solar Cell by Vacuum Cold Spraying at Room Temperature

Deposition of nanocrystalline TiO₂ coating at low temperature is becoming more attractive due to the possibility for continuous roll production of the coating for assembly lines of dye-sensitized solar cell (DSC) at a low cost. In this study, porous nano-TiO₂ coating was deposited by vacuum cold spraying (VCS) at room temperature on a conducting glass substrate using commercial P25 nanocrystalline TiO₂ powder. The microstructure of TiO₂ coating was characterized by field emission scanning electron microscopy (FESEM) and nitrogen adsorption test. A commercial dye (N719) was adsorbed on the surface of TiO₂ particles within the coating to assemble a DSC. The cell performance was evaluated by employing simulated solar light at an intensity of 100 mW/cm². The results showed that TiO₂ coating was deposited by the agglomerates of nano-TiO₂ powders. The Brunauer-Emmett-Teller (BET) test of the as-sprayed TiO₂ coating yielded a porosity of 49% and an average pore size of 17 nm. The assembled solar cell yielded a short-circuit current density of 7.3 mA/cm² and an energy conversion efficiency of 2.4%. The test results indicate that VCS was a promising method to deposit nanocrystalline TiO₂ coatings at low temperature applied to DSCs. This article is an invited paper selected from presentations at the 2007 International Thermal Spray Conference and has been expanded from the original presentation. It is simultaneously published in Global Coating Solutions, Proceedings of the 2007 International Thermal Spray Conference, Beijing, China, May 14-16, 2007, Basil R. Marple, Margaret M. Hyland, Yuk-Chiu Lau, Chang-Jiu Li, Rogerio S. Lima, and Ghislain Montavon, Ed., ASM International, Materials Park, OH, 2007.     

真空烧结炉预估自适应温控系统设计

论文在分析真空炉温控对象特性的基础上,提出一种PID参数自适应控制算法,该算法首先在试生产阶段采用继电自整定方式得到几组基准PID参数,此后在每炉正式生产时,利用升温阶段的信息预估由于装炉量不同等原因所带来的参数变化,预估结束及时对这几组PID基准参数进行在线更新。实例改造结果表明,该智能控制方案简单、有效,完全满足硬质合金真空烧结炉温度的控制要求。