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101.
102.
Fuel cells wherein zinc particles form a negative electrode and a gas-diffusion electrode (air electrode) is the positive electrode, are under development. Such cells are dependent on the regeneration of the zinc particles (and electrolyte). This paper describes experiments on electrolytic cells equipped with spouted bed cathodes for use in this application. Experiments have been carried out on laboratory scale cells to determine the operability of cells for growing 'seed particles in the range from 0.4 to 1 mm to measure cell voltage and current efficiency (and thereby energy consumption rate), and to identify a suitable material that could be used as a diaphragm (separating the spouted bed from the oxygen evolving anode). A larger cell, capable of producing up to 10 kg Zn per day, was designed and built. The larger cell was run successfully fifteen times and showed cell voltages and energy consumption rates comparable with those of smaller cells. 相似文献
103.
在溶剂(丙酮)-反溶剂(水)体系下,采用反溶剂重结晶法制备了超细萘普生微粒。研究了不同溶剂-反溶剂体积比、重结晶温度、表面活性剂用量及陈化条件对重结晶产物粒径和形貌的影响。采用扫描电子显微镜(SEM)、表面吸附(BET)、红外光谱(IR)、X射线衍射(XRD)等检测手段对原料药和重结晶产物进行了对比分析。实验结果表明,当溶剂与反溶剂体积比为1:20,重结晶温度为4~8℃,表面活性剂聚乙烯吡咯烷酮(PVP)的质量分数为0.5%~1.0%,60℃下陈化2 h时。可得到短径300~500 nm,长径1~2μm的超细萘普生粉体。重结晶所得产物的晶型和物理性质均未发生变化,但粒度显著减小,形貌趋于规整且比表面积增加至原料药的5.3倍。 相似文献
104.
Chateau Marie-Elise Galet Laurence Soudais Yannick Fages Jacques 《Journal of surfactants and detergents》2004,7(4):355-362
A new test was developed to assess the efficiency of no-wiping hard-surface cleaning. The test allows cleaner comparisons
according to their ability to remove greasy soils. The chosen approach minimizes the mechanical forces applied while cleaning
so that the interactions between a detergent solution and the soil to be removed can be characterized. For this, immersion
cleaning was chosen, with coated stainless steel as substrate and pigmented oils as the model soil. Several parameters were
studied in defined ranges using the Experimental Design method and systematic comparisons. The test shows high reliability
on degreasing assessments and is there-fore especially suited to optimization of nonionic surfactant mixes. The originality
of the test lies in the possibility of keeping a visual trace of the cleaned substrate appearance by imprinting it on a piece
of paper. The validation of the test leads to corroboration of several practical observations. Temperature and agitation play
a major role in cleaning efficiency. Detergent solution concentration is a more relevant parameter than pH. Sodium carbonate
is shown to have a higher buffering effect than pentahydrated sodium metasilicate. The test is easy to set up, highly sensitive,
and can be adapted to solve the problems encountered by formulators of detergent cleaners, such as screening the best ethoxylated
fatty alcohol mix for better degreasing properties. 相似文献
105.
106.
以过硫酸铵为引发剂,十二烷基硫酸钠为乳化剂,采用种子聚合工艺,合成了偏氯乙烯质量分数为23%~43%的羧基偏氯乙烯丁苯胶乳。通过电镜观察到所合成的胶乳粒子具有核-壳结构。通过测定胶闰子表面层的羧基数量,研究了羧基的分布,结果表明,羧酸种类对羧基在胶乳粒子中及在聚合体系中的分布有重要影响,该胶乳作为地毯背衬粘合剂,具有粘合力高,极限氧指数高的特点,是一种较好的阻燃性粘合剂。 相似文献
107.
研究了三相鼓泡床中的临界固含率,以空气作气相,水、乙醇-水、丙酮-水、萜松醇-二甲苯作液相,石英砂、煤、雷奈镍作为固相。分析了鼓泡柱的高径比、气体速度、固体粒子的大小和比重、液体的粘度对临界固含率的影响,提出了含有这些参数的无因次数群的关联式,讨论了本文提出的关联式和文献报导的差别。 相似文献
108.
The microstructure, mechanical properties, and fracture behavior of polypropylene (PP)/barium sulfate (BaSO4) composites were studied. Four composite samples with different PP‐BaSO4 interface were prepared by treating the filler with different modifiers. The fracture behavior of the composites under different strain rates was studied by means of Charpy impact tests and essential work of fracture (EWF) tests. It is shown that a moderate interfacial adhesion is favorable for toughening, which ensures that the particles transfer the stress and stabilizes the cracks at the primary stage of the deformation, and satisfies the stress conditions of plastic deformation for matrix ligaments subsequently via debonding. Very strong interfacial adhesion is not favorable for toughness, especially under high strain rate, because the debonding‐cavitation process may be delayed and the plastic deformation of matrix may be restrained. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 99: 1207–1213, 2006 相似文献
109.
脲醛树脂乳液干燥成粉末的试验研究 总被引:2,自引:0,他引:2
进行了用惰性粒子流化床干燥器将脲醛树脂乳液干燥成粉末的试验研究,产出了品质好的干粉,得出了在试验条件下的干燥强度和热效率,并作了经济性评价。 相似文献
110.
对原电解质凝聚工艺生产CR322(混合调节型氯丁橡胶)进行了改进,实现了冷冻凝聚新工艺法生产切块CR322,即主乳化剂由松香皂/脂肪酸皂复合型代替了单一松香皂。新工艺解决了冷冻转鼓装置生产CR322过程中“黏杆”及干胶门尼黏度控制等问题。产品无焦烧粒子。且焦烧时间明显延长。 相似文献