影响陶瓷餐具中温釉铅溶出量几个因素的探析

对陶瓷餐具中温釉在配方、熔块制各、氧化物、着色剂添加量、烧成方式和烧成温度几方面的试验，分析和探讨了以上因素对陶瓷餐具中温釉铅溶出量的影响，提出了在陶瓷中温釉生产中应该注意及改进的几个方法。     

新的组合赋权 TO PS IS 法及其在船舶设计决策中的应用

多属性决策的结果与权重向量的选取有密切的关系。分析了主观赋权和客观赋权的优劣,提出了一种新的组合赋权方法。该方法通过在专家评分法、层次分析法、信息熵法、变异系数法这四种主客观赋权方法间建立平衡系数的概念,使最终的组合赋权向量与原向量间欧氏距离最小。将这种组合赋权方式与 TOPSIS法结合应用于载重量DW＝35000t原油船船型方案决策分析,评判结果表明,新的组合赋权 TOPSIS法简单易行,意义明确。同时能兼顾主客观赋权的优点,合理、客观地给出排序方案。这种综合方法也能推广应用于船舶决策的其他领域。     

Evaluation of methods of measurement of nitrogen in poultry and animal manures

Kjeldahl nitrogen (N), total N and forms of inorganic N (ammoniacal (NH₄)-N, nitrate (NO₃)-N and nitrite (NO₂)-N) were measured in a range of animal manures. The manures include fresh samples of poultry manure, sheep manure, horse manure, dairy slurry and pig slurry and composted poultry manure. Kjeldahl N was measured by standard micro-Kjeldahl digestion. For total N measurements, NO₃-N and NO₂-N were recovered during Kjeldahl digestion by pretreatments with various oxidizing and reducing agents. Inorganic forms of N were measured by extraction with 2M KCl solution.Kjeldahl digestion alone allowed measurement only of organic N and NH₄-N. Amongst various modifications to the Kjeldahl, pretreatment with either acidified (H₂SO₄) Zn-CrK(SO₄)₂ or acidified (H₂SO₄) reduced Fe achieved complete recovery of NO₃-N. Nitrite N was only recovered by first oxidising the NO ₂ ^- to NO ₃ ^- with KMnO₄ followed by reduction to NH₄-N with acidified (H₂SO₄) reduced Fe.More than 95% of the total N in fresh animal manure was present as organic N and NH₄-N which were recovered by the standard Kjeldahl digestion. In the case of fresh manures there was no difference between the amount of total N measured by the Kjeldahl digestion and its modified methods. However composting of poultry manure or drying of poultry manure, pig slurry and dairy slurry resulted in an increase in NO₃-N which was not recovered during Kjeldahl digestion alone. Under these conditions the total N could be measured by pretreating the samples with KMnO₄ and reduced Fe prior to Kjeldahl digestion.Drying of animal manures caused a decrease in organic N and NH₄-N, especially in poultry, pig and dairy manures. There was a slight increase in NO₃-N; but most of the decrease in N content with drying was attributed to the volatilization loss of ammonia (NH₃). Amongst various drying methods examined air drying caused maximum loss of N as NH₃ whereas freeze drying caused minimum loss of N. This suggests that fresh animal manures can be freeze dried for analysis of N which causes minimum loss of N.     

改进校园人才招聘会的对策探讨

校园招聘会已经成为高校毕业生就业签约的主要渠道。如何提高校园招聘会的成效,对于促进高校的就业工作具有重要的现实意义。通过分析校园招聘会的现有形式及存在的问题,提出改进校园招聘会的对策,以提高毕业生在招聘会上的就业成功率。     

基于边缘敏感的SLIC和二次密度聚类的GGO分割

针对磨玻璃肺结节(Ground Glass Opacity,GGO)边界对比度低、大小各异和灰度不均匀等造成分割准确率低的问题,提出一种基于边缘敏感的SLIC和二次密度聚类相结合的分割算法。将图像边缘检测结果与SLIC超像素算法相结合,并将其中含有边缘的超像素块用区域质心代替其原始聚类中心,改善SLIC边界黏连性较差的问题;针对密度聚类不能完整分割GGO的问题,提出二次密度聚类的方法,对密度聚类定位到的簇及其邻域簇进行二次密度聚类。实验结果表明,该算法分割GGO的平均准确率达90.17%,灵敏度达84%。     

Leaching Stability of Simulated Waste Forms for Immobilizing An3＋ by Gd2Zr2O7 with Nd3＋

In order to investigate the anti-leaching capability of pyrochlore Gd2Zr2O7 immobilized An3+, trivalent neodymium was used as the simulacrums for radioactive wastes with trivalence, Gd2-xNdxZr2O7(0.0x 2.0) series samples were successfully synthesized by high temperature solid reaction and using Gd2O3, Zr O2 powders as starting materials. The experiments of long-term chemical stability were conducted in synthetic seawater at 40 and 70 ℃. The XRD diffractive data and extraction ratio of as-received samples were collected with the help of X-ray diffraction(XRD) instrument and inductively coupled plasma mass spectrometry(ICPMass). The results indicate that the phases of as-received compounds keep the single phase of pyrochlore. The extraction ratio of Gd3+, Zr4+ and Nd3+ in waste forms is increasing with the increase of immersion time in synthetic seawater. The extraction ratio of waste forms at 70 ℃ is higher than at 40 ℃. The highest extraction ratio of Gd3+, Zr4+ and Nd3+ after 42 days is near 0.025 8, 0.003 8 and 0.045 2 μg·m L-1, respectively.     

市政污水处理厂化学除磷及过程优化研究

对比了二价和三价铁及其复合药剂对城市污水处理厂除磷效果,研究了搅拌条件对除磷效率的影响,同时研究了混凝后不同形态磷的变化情况。研究结果显示,原始混合液中颗粒态磷、无机溶解态和有机溶解态的磷分别为2.63、0.99、0.28 mg/L。三价铁化学除磷效果最佳,复合药剂次之。当复合混凝剂投加量达到污泥体积0.15%时,TP的去除效率达到最高,之后会随着混凝剂投加量的增加而降低。水力剪切过程对化学除磷效果影响较大,随着搅拌速率的提高,混凝效率逐渐提高,转速达到200 rpm时TP去除率达到最大。     

PID参数整定的MCP标准传递函数法公式

根据MCP标准函数,利用控制器标准传递函数设计方法推导得出了一种新的PID参数整定公式.通过理论分析和仿真试验,验证了用MCP法公式整定的系统具有超调量小和鲁棒性高的优点.     

侧爆作用下锚固洞室破坏形式及机理研究

为了进一步提高锚固洞室在侧爆作用下的抗爆能力,利用数值分析软件LS-DYNA3D程序,研究了在侧爆作用下的锚固洞室的破坏形式及机理.数值分析结果表明:压应力波一开始是以球形向四周传播的,当压应力波碰到洞室壁时,会在洞室壁表面产生拉应力波,并以椭圆形式向反向传播;在应力波整个传播过程中,由于反射拉伸可能会在洞室锚固区和非锚固区先后产生二次拉伸破坏,最后可能会由于洞室反射的拉伸波和地面反射拉伸波相遇共同作用,在离地面比较浅的地方产生拉伸破坏区.