络合沉淀法制备BaTiO_3超细粉末

在分析ＢａＴｉＯ_３前驱体形成机理的基础上，提出了以草酸作为络合剂，用络合沉淀法制备超细ＢａＴｉＯ_３新工艺。用化学分析法测定产物Ｂａ／Ｔｉ比，用ＸＲＤ、ＴＥＭ、ＢＩ－９０激光散射粒度仪对产物的晶型、粒度及形貌进行表征。结果表明：采用该法合成的前驱体，微观组分确定，粒径小，粒度分布窄，近似球形，煅烧后为高纯超细ＢａＴｉＯ_３粉末。     

非冲击式印刷和热敏成像技术的发展概述

本文概述了ＮＩＰ印刷的特点，类型和发展背景，着重介绍了ＮＩＰ印刷中热敏成像技术的发展历程，热敏成像材料的分类及热成像用热源的新发展。     

激光扫描共焦荧光显微镜的电子控制系统研究

介绍了激光扫描共焦荧光显微镜的电子控制系统，为了提高激光扫描器的定位精度，在系统中提出采用基于闭环象素时钟发生器的检流计振镜所固有的扫描非线性失真补偿方案，减少输出图象的枕形畸变，实现行扫描空间位置的均匀性。在以细分梯形波电流驱动反应式步进电机情况下，根据实测θｉ曲线，用反插法求得与步进电机运行非均匀性相补偿的相电流波，从而获得在小电流情况下高角度均匀的步进电机细分运行特性。     

Electronic data acquisition forms in construction management

Effective management of construction projects depends on good access to and control of data, especially data pertaining to cost and schedule control functions. However, the proper design and development of automated mechanisms have not had the facility to acquire and store quality data in a timely manner. The purpose of this paper, then, is to discuss a prototype, automated data acquisition system that was developed to support an integrated project management system. The data acquisition system is composed of an integrated set of electronic forms used in conjunction with a bar coding data-entry tool.     

电子称在化工生产中的应用

针对化工生产环境的特点对电子称重仪器在化工计量中的正确选择和使用作一些分析阐述。     

Synthesis and characterisation of carboxylic acid and diphenylphosphine derivatives in the 1,3-diyne series: Spectral properties of polydiacetylene carboxylates

Symmetrically substituted 1,3-diynes containing hydroxyalkyl ( 1a-d ), bromoalkyl ( 1e-h ) (diphenylphosphinyl) ( 1i-k ) and carboxyalkyl ( 2a-d ) substituents have been prepared and characterised; the phosphine derivative ( 1k ) has been converted with alkyl iodides ( RI ; R = Me, Et) into bis(phosphonium) salts ( 1l and m ). During preparation of the diynedioic acid. ( 2a ), the non-centrosymmetrical diyne, HO₂CCH₂C?C—C?C(CH₂)₂OH ( 3 ), was also isolated. ⁶⁰Co γ-Irradiation of diacetylene monomers ( 2a – d ) and 10,12-tricosadiyn-1-oic acid gave the corresponding polydiacetylene derivatives ( 4a – d and 5 ), respectively. Rubidium salts of ( 4c ) and ( 4d ), a barium salt of ( 4c ), and a potassium salt of ( 5 ) were prepared and isolated; soluble potassium salts of the carboxylic acid polymers ( 4 ) were generated in aqueous solution. The effects of changes in pH on the UV/visible absorption spectra of aqueous solutions of selected carboxylic acid polydiacetylenes have been recorded, and are discussed.     

基于Multisim7.0软件平台的电子电路设计型实验研究

介绍了EDA(电子设计自动化)技术中Multisim7.0软件平台的功能特点.利用EDA技术进行设计性实验的研究与开发,是改革传统电子电路实验教学模式的有效途径,能帮助学生掌握最先进的电子电路设计方法和技能.结合EDA技术在电子电路设计型实验中的应用实例分析,阐明了利用Multisim7.0软件平台进行电子电路设计的优越性,其方便的更改电路和元器件参数的能力,使得能够更快更好地进行电子电路设计与仿真分析,同时缩短设计电路的时间,因而是一种全新的培养学生实际动手能力的有效工具.     

电子商务中SET协议的安全缺陷研究

目前SET协议在电子商务交易中应用越来越广泛,因此,对SET协议的安全性的要求就越来越高。论文在SET协议的交易流程基础上,分析了其安全机制采用的技术和优点,指出了SET协议安全性存在的一些问题。     

Development of a Magnetic Suspension Densimeter and Measurement of the Density of Toluene

The development of a magnetic suspension densimeter that has been built for measurement of the density of compressed liquid at pressures up to 30 MPa in the temperature range 20 to 150°C is described. The densimeter was first built by the author and his coworkers at NIST. We describe here further improvements made on a second system built at NMIJ based on the same principle. The densimeter uses a small coil suspended from an electronic balance. Within the coil is placed a sample cell in which the pressurized sample and a buoy, which is a permanent magnet, are enclosed. For measurement of density, balance readings are recorded (1) with the buoy at rest and (2) with the buoy in magnetic suspension. The measurement procedure is basically a hydrostatic weighing, which is simpler than those of conventional magnetic densimetry. As an example, measurements of toluene density performed as part of an inter-laboratory comparison are presented. The data agreed with reliable literature values to within a few hundredths of a per cent.     

浅谈图书馆网站的建设

对我国现阶段公共图书馆网站的总体情况进行了分析和概括 ,列举了具有代表性的几个网站的主要特点 ,指出了存在的问题 ,提出了相应的对策 ,强调了网站建设首先应有以读者需要为依归的理念 ,并将之贯穿在网站的内容设置和页面设计的整个过程中。