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101.
MCS接枝共聚物的结构和形态 总被引:4,自引:0,他引:4
将甲基丙烯酸甲酯(MMA)、苯乙烯(S)在氯化聚乙烯(CPE)存在下进行悬浮接枝共聚,获得MCS树脂。本文着重考察了MCS树脂的化学结构及胶粒形态。结果表明,确实发生了接枝共聚。CPE用量、RSH含量、引发剂浓度、反应温度、溶胀时间及聚合转化率对MCS树脂的接枝率、接枝效率均有影响。MCS树脂是接枝共聚物、MMA/S共聚物与MMA均聚物的混合物,橡胶相CPE在MCS树脂中的分散情况为“海岛结构”, 相似文献
102.
Image segmentation towards new image representation methods 总被引:1,自引:0,他引:1
Diogo Cortez Paulo Nunes Manuel Menezes de Sequeira Fernando Pereira 《Signal Processing: Image Communication》1995,6(6):485-498
Very low bit-rate video coding has recently become one of the most important areas of image communication and a large variety of applications have already been identified. Since conventional approaches are reaching a saturation point, in terms of coding efficiency, a new generation of video coding techniques, aiming at a deeper “understanding” of the image, is being studied. In this context, image analysis, particularly the identification of objects or regions in images (segmentation), is a very important step. This paper describes a segmentation algorithm based on split and merge. Images are first simplified using mathematical morphology operators, which eliminate perceptually less relevant details. The simplified image is then split according to a quad tree structure and the resulting regions are finally merged in three steps: merge, elimination of small regions and control of the number of regions. 相似文献
103.
104.
Emma P. Bullock Allison L. Roxburgh Patricia S. Moyer-Packenham Elif Bektas Joseph S. Webster Kathleen A. Bullock 《Journal of Computer Assisted Learning》2021,37(2):557-586
This study focused on an examination of how type, quality and children's awareness of design features in digital math games, along with an awareness of the mathematics goals of the game, were related to learning outcomes. We conducted a parallel conversion mixed methods study with 45 students in Grades 3 and 4 (ages 9–10). Students participated in clinical interviews using three digital math games. The results suggest a moderated mediation relationship in which the quality of the design features moderated the mediating impact of children's awareness of the game's design features, specifically when the child was aware of the mathematics content learning goal (MCLG) of the game. These findings show how important it is that design features are of high quality in a digital math game, and how this is intertwined with children's awareness of the features and the MCLG. When these variables intertwined in just the right way, the interactions between the children and the digital math game afforded mathematical learning growth. 相似文献
105.
Joseph H. Magill 《Journal of Inorganic and Organometallic Polymers》1992,2(2):213-229
Variations in thermotropic behavior have been investigated for many crystalline polyphosphazenes. Experimental results obtained from DSC, solid-state MAS NMR, dilatometry, mechanical property (creep and dynamic) measurements, birefringence, X-ray (wide and small-angle), and electron diffraction have been made as a function of temperature in an attempt to elucidate the structure-morphology behavior in these polymers. Initially all polyphosphazenes described in this study crystallize from dilute or moderately concentrated solutions in the monoclinic form with relatively low crystallinity (50%). When heated, these specimens expand atT(1) and adopt a chain-extended 2D mesophase morphology in order to relieve congestion. Above this first-orderT(1) temperature a chain-extended –P=N– chain backbone morphology transforms into an isotropic phase at the melting temperatureT
m. When cooled, samples transform into the mesostate. However, crystallization from the mesophase belowT(1) takes place into a 3D orthorhombic state. These two modes of ordering/disordering are in accordance with (i) a hexatic chain packing [betweenT(1) andT
m] with variously mobile side groups that also exhibits smectic features when mesogenic side groups are present and (ii) a 3D orthorhombic structure of high crystallinity belowT(1). The initial monoclinic phase is accessible only via a solution crystallization route. Solid-state MAS NMR, crystallization kinetic measurements, and optical microscopy studies obtained from oriented and unoriented polymers have been especially germane in providing a unifying picture for mesophase formation and ordering in polyoxyphosphazenes. X-ray and electron diffraction evidence is complicated by critical overlapping peaks that are found under these same conditions. They demonstrate that (a) positional disorder exists along the chain direction and (b) the side chain above, as well as below, theT(1) transition is governed by the mobility, size, and type of side group in circumstances where phase transformations occur. 相似文献
106.
声纳技术应用日益广泛,已成为海洋测量的重要工具,而去除噪声处理是对声纳图像进行正确判读的前提,本文采用了改进的形态学算法减少声纳图像中噪声的影响,对图像进行预处理,采用Matlab图形图像处理工具对处理的算法进行仿真的方式,从而使处理效果达到最佳。 相似文献
107.
Formation of WC/Ni hard alloy coating by laser cladding of W/C/Ni pure element powder blend 总被引:1,自引:0,他引:1
Minlin Zhong Wenjin Liu Yu Zhang Xiaofeng Zhu 《International Journal of Refractory Metals and Hard Materials》2006,24(6):453-460
WC/Ni coating was formed by laser cladding of a W/C/Ni powder blend. The formed WC crystals have rectangular or quadrangle cross-section shapes with size of 2–30 μm. Step, twist and cross growth morphologies of WC formation were observed. The coating contains WC, CW3, WNi, FeW3C, Fe6W6C, W3O, W, C, and (Fe,Ni) phases. 相似文献
108.
钢表面化学气相沉积TiC晶体的择优取向 总被引:1,自引:0,他引:1
本文用化学气相沉积(CVD)法,以TiCl_4-CH_4-H_2为原料气体,在不锈钢表面获得了致密的TiC膜.研究了TiC的成膜速度、表面形貌和晶体择优取向与沉积条什的关系.结果表明,沉积温度T_(dep),碳钛比CH_4/TiCl_4强烈地影响了TiC的成膜速度、表面形貌和晶体择优取向.CH_4/TiCl_4低时,TiC晶体的择优取向为(220):而CH_4/TiCl_4高时,TiC晶体的择优取向为(200).TiC晶体的择优取向主要取决于气氛中活性碳的平衡浓度。 相似文献
109.
聚酰亚胺的前聚体,聚酰胺酸,是通过4,4-二氨基二苯醚(ODA)与3,3,4,4二苯甲酮四羧酸二酐(BTDA)反应制备的。未改性的、酸改性和胺改性的多壁碳纳米管(MWCNT)被分别地单独加入到聚酰胺酸溶液中,并加热至300℃,从而制成聚酰亚胺/碳纳米管复合材料。扫描型电子显微镜(SEM)和透射电子显微镜(TEM)的显微照片表明,酸改性的多壁碳纳米管和胺改性多壁碳纳米管在聚酰亚胺基体中被均匀一致地分散开。通过对酸和胺改性的多壁碳纳米管MWCNTS对多壁碳纳米管/聚酰亚胺复合材料的表面和体积电阻率的影响进行了研究。了解到该纳米复合材料的表面电阻率ITES从1.28×10^(15)Ω/cm^(2)(纯聚酰亚胺),降到7.59×10^(6)Ω/cm^(2)(26.98%的未改性的多壁碳纳米管含量)。除此之外,添加多壁碳纳米管影响了纳米复合材料的玻璃化转变温度。改性多壁碳纳米管意义就是提高了纳米复合材料的机械性能。多壁碳纳米管/聚酰亚胺复合材料的拉伸强度从10^(2)MPa(纯的聚酰亚胺)增加到134 MPa(6.98%酸改性多壁碳纳米管/聚酰亚胺复合材料)。 相似文献
110.
周燕茹 《吉林化工学院学报》2021,38(9):107-111
传统的数据聚类统计方法仅适用于低维数据聚类问题,为此,本研究设计了基于模糊数据的高维稀疏数据聚类统计方法,以期提升高维稀疏数据的聚类统计效果。以模糊C均值聚类算法为基础,通过优化初始聚类中心解决局部最优问题,缩短聚类统计时间;然后引入权重机制,令该方法适用于高维稀疏数据聚类统计。基于此,以余弦距离替换原有的欧几里德距离,提高高维稀疏数据聚类统计效果。实验证明:在数据维度不同时,该方法均有较优的聚类统计效果。当数据维度较低时,分块比例为10%时聚类统计效果最优;当数据维度较高时,分块比例为40%时聚类统计效果最优。在不同稀疏度等级时,该方法的命中率和聚类统计效率均较高。 相似文献