Properties of Graphite‐Strengthened Magnesium

Mg was dispersion‐strengthened with graphite by powder metallurgy. The material was produced by ball milling Mg micropowder (median particle diameter 40 μm) with 3 vol.‐% graphite powder (median particle diameter 1–2 μm). After 8 h ball milling the product was consolidated by hot extrusion. Structural analysis revealed that a submicrocrystalline structure developed during ball milling. Tensile tests showed that the material was brittle even up to 300 °C and, therefore, most mechanical tests were carried out under compression. Under those conditions the reinforced material showed yield stresses of 270 MPa at ambient temperature, 170 MPa at 150 °C, and 125 MPa at 300 °C. Mg processed under the same conditions, but without graphite addition, had significantly lower yield stresses. The dispersion‐strengthened Mg showed a marked increase in creep resistance: at 200 °C and a stress, σ_c, of 100 MPa, the secondary creep rate, ?_s, was in the lower 10^–9 s^–1 range and at 300 °C and σ_c of 80 MPa, ?_s values of up to 1 × 10^–8 s^–1 were measured. The results are discussed.     

Structural Analogies and Differences Between Graphite Oxide and C60 and C70 Polymeric Oxides (Fullerene Ozopolymers)

A brief survey of the chemical structural analogies and differences between graphite oxide and fullerene ozopolymers or polymeric fullerene oxides (PFO) is presented. Graphite oxide is the product of oxidation of graphite prepared with strong oxidizing agents while PFO is the products formed by prolonged ozonation of C₆₀ or C₇₀ in solution. Notwithstanding the different starting substrates and oxidation conditions, elemental analyses, FT-IR spectroscopy and ¹³C-NMR spectroscopy suggest a very similar chemical structure for graphite oxide and PFO. A further analogy is the possibility to perform reduction or oxidation reactions on both substrates considered. Graphite oxide and PFO have also in common the ability to act as ion exchangers and as metal ion binders. Even the thermal behavior is comparable. However, X-ray powder diffraction has confirmed that graphite oxide still has a layered structure derived from graphite but with the graphene sheets at much bigger distance from each other due to the intercalation of oxidized groups and solvent molecules, while PFO do not show at all any sign of layered structure either from the X-ray spectra and also by its behavior in solution which is strikingly different from that shown by graphite oxide.     

三脉冲不等强度激光片光源的研制及应用

本文报道了最近研制成功三脉冲不等强度调Q红宝石激光片光源系统.利用小颗粒对片光源90°方向的散射光对动态颗粒场进行高速摄影,从底片中能够精确直观地判断微小颗粒的瞬时分布、运动方向、速度和加速度情况.     

The result of a wall failure in-pile experiment under the EAGLE project

The WF (wall failure) test of the EAGLE program, in which 2 kg of uranium dioxide fuel-pins were melted by nuclear heating, was successfully conducted in the IGR (Impulse Graphite Reactor) of NNC/Kazakhstan. In this test, a 3 mm-thick stainless steel (SS) wall structure was placed between fuel pins and a 10 mm-thick sodium-filled channel (sodium gap). During the transient, fuel pins were heated, which led to the formation of a fuel-steel mixture pool. Under the transient nuclear heating condition, the SS wall was strongly heated by the molten pool, leading to wall failure. The time needed for fuel penetration into the sodium-filled gap was very short (less than 1 s after the pool formation). The result suggests that molten core materials formed in hypothetical LMFBR core disruptive accidents have a certain potential to destroy SS-wall boundaries early in the accident phase, thereby providing fuel escape paths from the core region. The early establishment of such fuel escape paths is regarded as a favorable characteristic in eliminating the possibility of severe re-criticality events. A preliminary interpretation on the WF test results is presented in this paper.     

Aspen plus软件及其在燃煤发电工程中的应用

介绍了ASPEN PLUS软件的基本流程模拟和功能。结合该软件在我国燃煤发电工程中的应用．指出了该软件的应用方向，为燃煤发电工程的研究和技术的应用提供参考。     

钻井岩屑粒径分布规律的研究

钻井振动筛是固控系统的重要分离设备,其主要任务是清除钻井液中直径大于74μm的固相颗粒。对辽河油田7口井深0～3500m的钻井岩屑进行了实地取样,分析了岩样颗粒直径大于74μm的粒径分布特征。分析结果表明,钻井岩屑具有明显的片状特征,颗粒的粒径分布主要与地层岩性和破岩工具有关,随着井深的变化,其岩样粒径分布呈现出幂分布、2分布和瑞利分布等3组典型规律。给出了岩屑颗粒的概率直径;建议在筛面颗粒运动特性研究、筛网工作载荷的计算和激振方式的选择中,应考虑岩屑颗粒片状特性的影响。     

地震断裂带高铁大跨拱桥深基坑钢板桩围堰支护试验与监测

针对大跨度高速铁路拱桥建设对深基坑开挖施工的安全性要求,为了研究钢板桩围堰支护在大跨度高速铁路拱桥深基坑施工中的可行性,以新建徐盐高铁徐洪河特大桥工程项目为依托,通过数值模拟及现场试验监测,对深基坑钢板桩围堰支护在施工过程中的形变及受力情况进行分析。结果表明:通过有限元模拟分析,钢板桩围堰最危险受力点处于钢板桩中部、中上部及四角连接处,围堰第4道内支撑内力较其他3道内支撑大。整个施工过程中工况5为施工最不利工况。由监测结果可知,在施工过程中钢板桩单日最大位移值为2.8mm,最大累计位移值为24.0mm,均未达到预警值,施工过程中钢板桩形变稳定。钢支撑轴力受基坑周边荷载的影响明显,围堰钢支撑最大压力值为147.31kN,最大拉力值为24.95kN,未达到预警值,结构安全。研究结果可供同类型工程施工参考。     

海域双排钢板桩围堰与明挖基坑变形特性分析

以深圳海滨大道一期Ａ段海底隧道工程为背景,针对海域环境双排钢板桩围堰与明挖基坑在施工过程中的变形控制难题,利用ＰＬＡＸＩＳ数值模拟软件建立有限元模型,通过建立有限元模型,系统的研究了海域双排钢板桩围堰与明挖基坑变形特性及相互影响规律,分析了围堰与基坑距离、基坑内支撑形式及基坑开挖步序等因素对钢板桩围堰变形的影响作用。研究结果表明:基坑开挖将造成围堰较大的水平位移;地连墙最大变形出现在墙体中下部;减小施工平台宽度和增大基坑内支撑刚度等方式可以有效减小钢板桩围堰变形。研究成果可以为类似工程的钢板桩围堰与明挖基坑设计提供参考依据。     

不锈钢薄板等离子电弧加热柔性成形试验研究

介绍了等离子电弧加热金属薄板柔性成形的特点,分析了等离子电弧柔性成形的机理.通过实验,得出了扫描次数、电弧电流、扫描速度、电弧高度、薄板厚度等参数对弯曲变形的影响规律.该规律对于提高弯曲效率、改善表面质量具有一定的指导意义.     

EB-PVD制备钛合金薄板渗铝相结构转变研究

对电子束物理气相沉积（EB-PVD）技术制备的钛合金薄板进行粉末包埋法渗铝，研究不同温度渗铝后的相结构转变规律。结果表明：制备态合金薄板相结构为Ti和Ti3Al，材料组织致密均匀，X射线衍射峰发生宽化，具有不对称性。在较低温度（600℃和620℃）渗铝后薄板两边的相结构变为Al3Ti相，但薄板的中心部位仍然为制备态的Ti3Al相，两边的Al3Ti组织和中心部位的Ti3Al组织都很均匀致密。在两相之间，存在清晰、平整的界面。在较高温度（700℃）渗铝后薄板的相结构为A13Ti，此时整个板材都被渗穿，组织均匀致密，并在局部小区域内出现铝元素的富集。