大长径比自旋弹箭横向自振特性的有限元计算方法与结果分析

本文研究大长径比自旋弹箭在飞行时横向振动的自振特性。本文将转子动力学应用于弹道学 ,采用有限元法 ,建立自旋弹箭横向振动自振特性方程。同时给出了计算方法。利用该方程和该方法 ,开发了相应的计算程序。通过数值计算 ,可给出细长旋转弹箭飞行时的进动转速和临界转速 ,以及相应的位移和角度振型。利用该程序 ,进行了实例计算和分析。     

DNA序列比对分析中的统计特征方法

提出了一种新的基于统计的序列特征定义,并以此对进化树进行构建.同时对这一方法进行了分类测试和进化树构建测试,发现所得测试结果与同样是用进化树进行构建的基于两序列比对的传统算法比较,其性能和适用性都有明显改善.     

复合形法优化内河航道重力式护岸

采用复合形优化法,结合《港口及航道护岸工程设计与施工规范》中推荐的抗滑、抗倾稳定的分项系数计算方法,并考虑了内河航道船形波等作用的影响效应,对重力式护岸断面进行了优化。     

燃烧—气体容量法测定冶金石灰中的二氧化碳

冶金石灰是石灰石经过工业煅烧的产品。其二氧化碳含量低，且经过高温煅烧后基本不含有机物。无需按照《石灰石、白云石化学分析国家标准中二氧化碳的化学分析方法》中用酸进行试样分解，只需在1200℃高温中灼烧，使石灰中残留的或煅烧后吸收空气中二氧化碳而形成的碳酸盐分解，象通常测定含碳耐火材料中二氧化碳那样，采用气体容量法进行测定。     

A continuum-based modeling of MEMS devices for estimating their resonant frequencies

A continuum-based modeling of coupled electrostatics-structure interactions is presented for the frequency computations of MEMS devices. The present general formulation of electrostatics accounting for free space is validated first by specializing it to one-dimensional uniform motion of conducting surfaces and comparing the resulting electrostatics to conventional lumped models. The general coupled electrostatics-structure interactions are then applied for the prediction of resonant frequencies of MEMS devices due to bias-voltage changes and temperature variations. Comparisons of predicted resonant frequencies obtained by the present coupled electrostatics-structure interaction models with experimental results available in the literature demonstrate that the proposed continuum-based interaction modeling yields high-confidence predictions of resonant frequencies of MEMS devices.     

阻燃聚氨酯软质泡沫塑料中氯含量的测定

叙述了阻燃聚氨酯软质泡沫塑料中氯含量的测定方法:在助燃剂存在下,氧瓶燃烧使聚氨酯软质泡沫塑料中的有机氯转化为HCl,用稀NaOH吸收,使用硫氰酸汞分光光度法测定聚氨酯软质泡沫塑料中阻燃剂的氯含量。该方法简单快捷、精确度高,回收率为99.64%～102.41%。     

Influence of accelerated ageing on methacrylate‐based denture resins heterogeneity as viewed by ESR‐spin‐probe method

The electron‐spin‐resonance (ESR) spin‐probe method, was used to study the heterogeneity of denture resins based on poly(methyl methacrylate). Results for three resins processed by microwave energy, conventional curing and cold curing (depending on the curing procedure and exposed to ageing in various environmental conditions) were compared. All three cured resins were stored over the same time (1200 h) in distilled water at ambient temperature and in artificial saliva at 348 K. The temperature‐dependent ESR spectra of a spin probe dispersed in the denture resins are analyzed in terms of line‐shapes and line‐widths. The appearance of two spectral components was taken as an indication of resin heterogeneity. The results reveal that the cold‐cured resin has a lower local density in comparison with microwave and conventionally cured resin. The amount of residual monomer also contributes to the local motion of polymer segments. The change of denture resins exposed to ageing is influenced both by the structure of the original resin and the ageing conditions. Restricted motion of a spin probe incorporated into the acrylic resins exposed to accelerated ageing suggests additional crosslinking of polymer chains. The differences are observed for all the investigated resins, but the highest change is observed with the cold‐cured resin. The ESR results are accompanied by T_g and T_m measurements. Copyright © 2005 Society of Chemical Industry     

Cholesterol‐imprinted polymer receptor prepared by a hybrid imprinting method

A novel cholesterol‐imprinted polymer (CMIP‐H) was prepared by a hybrid method of covalent imprinting and non‐covalent imprinting. This approach involves the copolymerization of a template‐containing monomer, cholesteryl 2‐hydroxyethyl methacrylate carbonate, and a cross‐linker, followed by hydrolysis to afford a flexible guest‐binding site accompanied with the easy and efficient removal of a ‘sacrificial spacer’. The effect of solvent on the binding capacity of CMIP‐H towards cholesterol was studied, indicating that a good binding capacity towards cholesterol could be achieved in a less‐polar solvent. The binding experiments of CMIP‐H towards a series of structural analogues of cholesterol, including cholesterol acetate, progesterone and stigmasterol, were carried out in hexane. The results showed that CMIP‐H almost did not bind cholesterol acetate at all because the hydrogen‐bonding site is blocked. It exhibited a similar binding towards both cholesterol and stigmasterol, but much higher binding towards progesterone. Copyright © 2005 Society of Chemical Industry     

几种地下水易污性评价方法在徐州张集地区的应用

选择GOD法、DRASTIC法S、INTACS法及SI法4种易污性评价方法用于徐州张集地区的地下水易污性评价,应用GIS/ARCINFO输出张集地区的地下水易污性指标图。不同易污性评价方法对张集地区裂隙岩溶地下水的易污性评价得到了不同的结论,经分析,SI法更适用于张集地区的实际情况。具体应用时,要根据评价地区的实际条件,并和评价地区污染监测情况结合,选择合适的易污性评价方法评价地下水的易污性。     

A comparative study of numerical solutions to non-linear discrete crack modelling of concrete beams involving sharp snap-back

Numerical problems are often encountered in modelling crack propagation in concrete beams using non-linear finite element (FE) analysis, especially when sharp snap-back behaviour in load-displacement relations occurs. This paper firstly identifies 16 arc-length control based numerical strategies based on extensive literature review. They are then used to carefully model the structural behaviour of a four-point single notched shear beam using discrete crack modelling approach in which cracks are represented by interface elements with bilinear softening constitutive laws. Based on extensive FE analyses, detailed comparisons of the merits and demerits of these numerical algorithms are then made. The results indicate that the effectiveness and efficiency of different algorithms may vary considerably from one to another, with the local arc-length based procedures in conjunction with tangential stiffness strategy and reversible unloading model being the most robust.