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References: 《过程工程学报》2004,4(Z1):449-454
Arc Spray Nanoparticle Synthesis System (ASNSS) has been used to prepare the silver nanofluids in this study. The metal electrodes under the electrical discharge will melt and evaporate rapidly and condense to form the nanoparticles in the dielectric fluid at lower temperature and produce the suspended nanoparticle fluid. Thus, the mechanism of the ASNSS process is superheating the electrodes by plasma to form metallic nuclei and supercooling these nuclei by dielectric liquid to produce nanofluid. This study considers the different controlling parameters such as discharge current,discharge voltage, pulse-duration time, electrode diameter, and the temperature of dielectric liquid. The optimally operated parameters can be obtained to produce the finer particle size in nanofluid. The results indicate the silver electrodes in alcohol fluid will produce the spherical nanosilver particles. The mean particle size of silver in different dielectric liquid temperatures of-40, -20, 0, and 10℃ is about13.4, 15.8, 17.5, and 21.6 nm, respectively. This indicates that the well suspended fluid can be obtained by controlling the lower dielectric fluid temperature. 相似文献
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采用电化学阳极氧化法制备了管长约为1.48μm,管径约为87 nm的Ti O2纳米管,然后采用光还原沉积法在不同浓度的AgNO3溶液中制备了沉积单质Ag的Ti O2纳米管.利用SEM,XRD和XPS对Ag-Ti O2纳米管进行了表征,并以罗丹明B溶液为目标降解物评价了其光催化活性.结果表明:Ag微粒是以稳定的单质形式存在,Ag-Ti O2纳米管的光催化活性随着AgNO3溶液浓度的增大而呈增大的趋势,当AgNO3浓度达到0.08 mol/L时其活性达到最大值,而后随着浓度的增大活性反而下降. 相似文献
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The effect of surface finish and annealing treatment on the oxidation behavior of Ti-48Al-8Cr-2Ag (molar fraction, %) alloy
was investigated at 900 and 1 000 °C, respectively in air. Thermal gravimetric analysis (TGA) was conducted for the characterization
of oxidation kinetics. The microstructures of oxide scales were studied by scanning electron microscopy (SEM) and transmission
election microscopy (TEM) techniques. Unfavorable effect of the annealing treatment on the oxidation behavior of the coating
was also investigated. The results indicate that the oxidation behavior of the alloy is influenced by surface finish and annealing
treatment. The oxidation rate of ground sample is lower than that of the polished alloy at 1 000 °C in air. The former forms
a scale of merely Al2O3, and the latter forms a scale of the mixture of Al2O3 and TiO2. Annealing can improve the formation of TiO2.
Foundation item: Project(2007430028) supported by the Science and Technique Foundation of Henan Educational Committee, China 相似文献
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Practice has proven that CrN performs better than TiN under some specific tribological applications. Nevertheless, the relatively soft nature of CrN still remains a problem. This paper reports experimental results on increases in hardness of sputtered PVD CrN coatings by means of additions of varying content of Ag or W. The resulting Cr-Ag-N and Cr-W-N coatings, grown on JIS SKH51 steel substrates, were characterized using SEM, EDS, WDS, XRD, micro-indentation hardness testing and scratch adhesion tests. Moreover, wear behavior was studied on two types of tribometer, employing different contact regimes — a ‘cylinder-on-disk’ line-contact reciprocating-sliding regime and a ‘ball-on-disk’ point-contact rotating-sliding regime.The experimental results can be summarized as follows: The hardness of Cr-W-N coatings increased with increasing W content; reversely, that of Cr-Ag-N coatings decreased with increasing Ag content. The additions of Ag and W resulted in a formation of secondary phases, elemental Ag and WN, respectively, uniformly embedded in the CrN coatings. With the two different types of tribometer, the observed trends for wear behavior, wear and friction coefficient, were nearly identical, indicating that both Ag and W additions to CrN coatings were beneficial. However, the Cr-W-N coatings were significantly more wear resistant than the Cr-Ag-N coatings. With the addition of W at 6.8 at.%, the largest wear improvement of 73%-85% was achieved. 相似文献
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通过XRD、TEM测试研究了自制ZnO/Ag纳米复合材料的结构和形貌,通过UV检测确定了以该纳米复合材料为光催化剂,在不同条件下对甲基橙的光催化降解率。结果表明:与空气煅烧相比,真空煅烧所得纳米复合材料的光催化降解效果更好,且光催化降解率随纳米复合材料用量增加而增大:甲基橙溶液的pH在5左右时,光催化降解率最高:H2O2浓度为0.9g/L时,光催化降解率可达100%。 相似文献
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The mechanical properties and microstructures of Al-8Cu-0.5Mg alloy with and without Ag addition were studied at both room- and elevated-temperatures. The results show that the alloy with Ag is strengthened by a homogeneous distribution of coexistent θ' and Ω precipitates on the matrix (001) and (111) planes, respectively, whereas the alloy without Ag by θ' precipitates only. The small size and high volume fraction of θ' and Ω precipitates in the Ag-containing alloy improve the tensile strength and yield strength, especially those at the elevated temperatures. However, it is also responsible for the decrease in elongation, compared with the alloy without Ag, which is due to the microcracks initiated from the inherent incompatibility between the particles and the AI matrix during deformation. 相似文献
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