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101.
102.
《材料与设计》2015
Low thermal conductivity is one of the key requirements for thermal barrier coating materials. From the consideration of crystal structure and ion radius, La3 + Doped Yb2Sn2O7 ceramics with pyrochlore crystal structures were synthesized by sol–gel method as candidates of thermal barrier materials in aero-engines. As La3 + and Yb3 + ions have the largest radius difference in lanthanoid group, La3 + ions were expected to produce significant disorders by replacing Yb3 + ions in cation layers of Yb2Sn2O7. Both experimental and computational phase analyses were carried out, and good agreement had been obtained. The lattice constants of solid solution (LaxYb1 − x)2Sn2O7 (x = 0.3, 0.5, 0.7) increased linearly when the content of La3 + was increased. The thermal properties (thermal conductivity and coefficients of thermal expansion) of the synthesized materials had been compared with traditional 8 wt.% yttria stabilized zirconia (8YSZ) and La2Zr2O7 (LZ). It was found that La3 + Doped Yb2Sn2O7 exhibited lower thermal conductivities than un-doped stannates. Amongst all compositions studied, (La0.5Yb0.5)2Sn2O7 exhibited the lowest thermal conductivity (0.851 W·m− 1·K− 1 at room temperature), which was much lower than that of 8YSZ (1.353 W·m− 1·K− 1), and possessed a high coefficient of thermal expansion (CTE), 13.530 × 10− 6 K− 1 at 950 °C. 相似文献
103.
《材料与设计》2015
Superplastic behavior of fine and ultra fine-grained AA5083 Al alloy was examined using the shear punch test. To achieve fine- and ultra fine-grained microstructures, a relatively new severe plastic deformation (SPD) process, namely Double Equal Channel Lateral Extrusion (DECLE) was employed. The strain rate sensitivity indices (m) of samples were evaluated after 1, 2, 4, and 6 passes for shear strain rates in the range of 3 × 10− 3 to 3 × 10− 1 s− 1 and temperatures in the range of 573 to 673 K. For microstructural observations, TEM images together with the corresponding SAED patterns were prepared and utilized. A considerable increase in the m-value was observed after the first pass of the operation for all testing temperatures. The best condition for achieving a good superplasticity for the alloy was found to be a single pass DECLE at 673 K in the strain rate range of 10− 2 to 10− 1 s− 1. This process condition resulted in an m-value of 0.43, indicative of a high strain rate superplastic deformation behavior. Further passes of the SPD process did not show any sign of superplasticity until the last pass of the operation, during which the m-value slightly increased, compared with the previous pass. 相似文献
104.
《材料与设计》2015
Mg–5Li–1Al (LA51) and Mg–5Li–1Al–0.5Y (LA51–0.5Y) alloys were smelted and rolled with different accumulated strains (36% and 68%) and rolling temperatures (373 K and 573 K). The microstructure, mechanical properties, fracture morphology and texture of the specimens were investigated. Results show that, due to the PSN (particle stimulate nucleation) mechanism, the addition of 0.5 wt.% Y improves the deformation resistance and weakens the basal texture of LA51 alloy. The effect of Y on UTS (ultimate tensile strength) of as-rolled alloys is more obvious than that of the as-cast alloy. Accumulated strain and rolling temperature could influence the twinning number, slip systems and DRX (dynamic recrystallization), thus affecting the microstructure and mechanical properties of the alloy. Under the proper combination of the above factors, the as-rolled LA51–0.5Y alloy with an accumulated strain of 68% at 573 K possesses the best comprehensive mechanical properties. 相似文献
105.
《材料与设计》2015
Short fluoroalkyl chain of C3F7 instead of longer fluoroalkyl chain (C > 7) was robustly grafted on cotton fibers via an atom transfer radical polymerization (ATRP) strategy. This study focused on the influence of different finishing parameters (synthetic approach, grafting concentration) and post-treatment (washing, drying) conditions on wettability, liquid adhesion, air permeability, and mechanical (dry abrasion and wet laundering) properties. The results indicated that C3F7 chain was successfully grafting by a developed ATRP technique to construct superhydrophobic cotton fabrics. The optimized surfaces demonstrated super-anti-wetting property with a contact angle of about 163.7 ± 2.5° and an ultralow droplet adhesion of 62.3 ± 2.6 μN. The wettability remained highly hydrophobic even after 40 abrasion or 35 laundering cycles. This work also demonstrated the rational design and elaboration strategy of short fluorine-containing chains are vital for the construction of super-anti-wetting surfaces with controllable droplet adhesions. The results indicated that the anti-wetting, abrasion and laundering properties are much more influenced by the grafting strategy. We believe that environmental-friendly short fluoroalkyl chain (C < 4) can also be utilized for the construction of cotton fabric with good anti-wetting property and potentially applied in some practical fields, e.g., anti-wetting/icing outdoor cloth or self-cleaning sport textile. 相似文献
106.
针对实际工程应用的316L/15CrMoR爆炸复合板材,采用光学显微镜、扫描电镜(EDS)等手段对爆炸复合板结合区的形貌、波形、晶粒度、变形层厚度、扩散层和渗碳层等进行了检测及分析。研究结果表明:结合区具有强烈塑性变形、熔化和扩散等微观特征;结合区波形为小波分布,波长和波高平均值为1056和454μm;基板侧塑性变形区域的晶粒度分别为9.1,7.1,6.7和5.8级。波峰和波谷处变形层厚度分别为189和137μm;在较强爆炸载荷作用下不锈钢覆层侧出现了绝热剪切线,其长度在100~200μm范围之内,间距20~50μm。 相似文献
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