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51.
The d.c. electrical conductivity of sodium vanadate, rubidium vanadate, cesium vanadate and their solid solutions sodium-rubidium
vanadate and sodium-cesium vanadate were studied by a two-probe method in the temperature range covering their transition
points. The electrical conductivity shows sharp change at the phase transition temperature of these materials. In NaVO3, RbVO3 and CsVO3, increase in d.c. conductivity is observed in the ferroelectric region while nonlinearities are observed above transition
temperatures. In solid solutions, the activation energy in the paraelectric state is higher than that in the ferroelectric
state and depends upon sodium concentration. 相似文献
52.
Grazing incidence reflection absorption Fourier transform infrared (GIRA-FTIR) spectroscopy was used to characterize the ferroelectric behavior of a thin poly(vinylidene fluoride–trifluoroethylene) P(VDF–TrFE) copolymer. The lab-built GIRA-FTIR apparatus allowed the heating and corona poling process to be carried out whilst collecting the GIRA spectra of the thin polymer film. The Curie transition from the ferroelectric to paraelectric phase was confirmed from the abrupt change in intensity of the 849 cm−1 band in the RA-FTIR spectrum. It was found that the Curie temperature dropped dramatically when the film thickness was lowered to below a certain critical value of approximately 100 nm. The switching of the CF2 dipoles in the ferroelectric crystals after applying the external electric field could be determined by monitoring the change in the 849 cm−1 band intensity. For the 600 nm thick P(VDF–TrFE) film, the switching of the dipoles appears to occur almost instantaneously, while the kinetics of dipole switching of the 75 nm thick film were significantly retarded. The repeated switchability of the CF2 dipoles upon the application of a bipolar cyclic electric field was also confirmed. The bistability of the film due to remnant polarization was also confirmed from the absorbance of the 849 cm−1 band after removing the applied voltage during corona poling. 相似文献
53.
Manipulation of molecular orientation alignment in MCTLCPs (main-chain thermotropic liquid crystalline polymers) by pure shear at nano scale has been investigated for the first time using molecular dynamics (MD) simulation. Results indicate that high planar shear induces long-range uniform orientation ordering (liquid crystalline phase) of initially randomly orientated molecules of MCTLCP fluid confined in a nanochannel, which is confirmed by analyzing the orientation order parameter and the snapshots of MCTLCP liquid in a nanochannel under different shear rates. Insights into the origin of the phase transition phenomena are given at molecular level through investigating the thermodynamic density distribution of MCTLCP molecules in the nanochannel, suggesting that the energy shift due to a radical jump of system density affects both the magnitude and the orientation of the molecular ordering. Simulation results also show that there is a critical shear rate for transforming isotropic phase into liquid crystalline phase. The critical shear rate is dependent on the temperature of the MCTLCP system. Findings in this paper may present useful information for processing TLCP molecules at nano scale and the understanding of nanoflow. 相似文献
54.
陈志刚 《制冷与空调(四川)》2003,17(2):25-28
水是食品材料中最重要的成分。本文介绍了食品中水的性质以及水对食品相变的影响,并从水活性、水的吸附性以及水的增塑性三方面描述了水在食品相变中所起的作用。另外,还着重分析了水对食品冻结温度的影响。 相似文献
55.
Yen-Cho ChenJ.N. Chung 《Computers & Fluids》2003,32(6):795-822
This study intends to provide an increased understanding of the laminar-turbulent transition phenomena for the buoyancy-assisted heated vertical channel flow during the early transient stage. The spectral method with weak formulation is applied in the direct numerical simulation. Initial disturbances consist of the finite-amplitude two-dimensional TS wave and a pair of three-dimensional oblique waves for the K-type disturbances. The results from the harmonic energy competitions of different wave modes show that for the buoyancy-assisted heated flow, the (kx=1, kz=1) or (1,1) and (1,0) modes would gain energy immediately and start to rise at almost the same rate. This phenomenon is different from that of the buoyancy-opposed flow, where the (1,1) mode decays slowly in the beginning until other modes gain enough energy and then it begins to grow quickly and overtakes the (1,0) mode after a short time period. These different transition patterns match with the experimental results that the flow transition is supercritical and subcritical for the buoyancy-assisted and -opposed flows, respectively. Buoyancy-assisted heated flow transition follows the general trend of an isothermal flow in the beginning, but the thermal-buoyant force is crucial in accelerating the instability and also causing notable differences during the subsequent transition process. All of the results for the vortex structures development, kinetic energy budget of the disturbances, flow visualization by tagged fluid particles, and the local temperature fluctuations are consistent in pointing to a clear pattern for the buoyancy-assisted heated flow transition. 相似文献
56.
Differential pressure fluctuation time series were obtained at different locations in a two-dimensional spout-fluid bed with a cross section of 300 × 30 mm and height 2000 mm. Shannon entropy analysis of differential pressure fluctuations was developed to characterize the dynamic behavior. Effects of two important operating parameters (spouting gas velocity and fluidizing gas flow rate) on the Shannon entropy were examined. It was demonstrated that a spout-fluid bed at a high spouting gas velocity or fluidizing gas flow rate was a deterministic chaos system since the Shannon entropies at all bed locations increased sharply and asymmetric unstable flows occurred. Shannon entropies were found to be significantly different at various bed locations. Shannon entropies of different flow regimes were distinct, so they were used to identify the flow regimes. The results show that the Shannon entropy helps to grasp the complex characteristics of dynamic behavior in spout-fluid beds. 相似文献
57.
本文对八种新型功能晶体Li2B4O7、Bi12TiO20、Bi12GeO20、Bi12GeO20、Bi4Ge3O12、Sr1-xBaxNb2O6(x=0.33,0.48)、LiTaO3等在130~973K范围内的比热行为及其与相变、组分之间的关系进行了实验研究,给出了比热的多项式拟合方程,并与用纽曼-卡普定律及用Wikelmann经验方程的比热计算值作了对比,为晶体比热的估算提供了依据和方法。 相似文献
58.
The width of the transition layer between the crystalline and amorphous zones in nylon 1010 was determined by SAXS with point collimation and long-slit collimation, respectively. The width of the transition layer, E, was found to be 1.7 nm. The results show that the width of the transition layer is independent of crystallinity. 相似文献
59.
The mechanism of “475°C embrittlement” of a duplex stainless steel was investigated using finite element modelling of the stress distribution at brittle fracture initiation. Brittle fracture initiated at a critical shear stress, which increased with ferrite hardness. The fracture stress was affected by the duplex microstructure. Fracture was nucleated by deformation twins, which were identified using electron back-scatter diffraction. The ductile-to-brittle fracture transition was sensitive to age-hardening and could be described simply by the effect of age-hardening and test temperature on the yield stress. 相似文献
60.
化学沉积法制备的Ni(P)、Ni(B)纳米薄膜的结构与磁性 总被引:3,自引:0,他引:3
用化学沉积法制备了系列Ni(P),Ni(B)合金薄膜样品,用X射线衍射结构分析方法证明样品由尺寸为纳米量级的颗粒组成,样品在磁性上表现出超顺磁性,对热磁处理前后的磁学参数进行了比较研究。 相似文献