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1.

Fe-based bulk metallic glasses (BMGs) with high boron content have potential application as a coating material used in the framework for storing spent nuclear fuels to support their safe long-term disposal. The high glass forming ability (GFA) and large supercooled liquid region are therefore required for such Fe-based BMGs in either the glassy powder fabrication or the subsequent coating spraying. In order to meet these requirements, the influence of Nb content on the GFA of Fe57Cr10Zr8B18Mo7−xNbx (x=1–5, at.%) alloys was investigated, as Nb has positive roles in GFA and thermal stability of BMGs. The results indicate that a fully amorphous phase in the as-cast samples with 3 mm in diameter is obtained for both the Fe57Cr10Zr8B18Mo5Nb2 and Fe57Cr10Zr8B18Mo4Nb3 alloys. The corresponding supercooled liquid regions of the two BMGs are 78 K and 71 K, respectively. The mechanism for improving their GFA was analyzed based on the principle of metal solidification, the parameters for glass formation and thermal properties of the alloys. The compression strength and Vicker’s hardness of the two BMGs are 1,950 MPa and 1,310 HV, 2,062 MPa and 1,180 HV, respectively. The developed BMGs with high B content, good GFA, and very high hardness can be used as coating materials to the framework for spent nuclear fuels.

  相似文献   
2.
500kV单相自耦中压无载调压的变压器,当调压绕组与低压绕组相邻、中压截波入波时,会在低压到铁心之间感应出很高的冲击传递电压,本文使用波过程仿真的方法,对比了不同的调压连接方式下低压到铁心之间传递电压的变化,进而得出调压的最优连接方案.  相似文献   
3.
Refining ceramic microstructures to the nanometric range to minimize light scattering provides an interesting methodology for developing novel optical ceramic materials. In this work, we reported the fabrication and properties of a new nanocomposite optical ceramic of Gd2O3-MgO. The citric acid sol-gel combustion method was adopted to fabricate Gd2O3-MgO nanocomposites with fine-grain sizes, dense microstructures and homogeneous phase domains. Nanopowders with low agglomeration and improved sinterability can be obtained by elaborating Φ values. Further refining of the microstructure of the nanocomposites was achieved by elaborating the hot-pressing conditions. The sample sintered at 65 MPa and 1300 °C showed a quite high hardness value of 14.3 ± 0.2 GPa, a high transmittance of 80.3 %–84.7 % over the 3?6 μm wavelength range, due mainly to its extremely fine-grain size of Gd2O3 and MgO (93 and 78 nm, respectively) and high density.  相似文献   
4.
Negatively charged fluorescent carbon dots (CDs, Em=608 nm) were hydrothermally prepared from thiophene phenylpropionic acid polymers and then successfully loaded with the positively charged anticancer cargo coptisine, which suffers from poor bioavailability. The formed CD-coptisine complexes were thoroughly characterized by particle size, morphology, drug loading efficiency, drug release, cellular uptake and cellular toxicity in vitro and antitumor activities in vivo. In this nano-carrier system, red emissive CDs possess multiple advantages as follows: 1) high drug loading efficiency (>96 %); 2) sustained drug release; 3) enhanced drug efficacy towards cancer cells; 4) EPR effect; 5) drug release tracing with near-infrared imaging. These properties indicated that red emissive CDs prepared from polymers could be used as a novel drug delivery system with integrated therapeutic and imaging functions in cancer therapy, which are expected to have great potential in future clinical applications.  相似文献   
5.
针对复阻抗式结冰探测技术中急需解决环境温度影响的问题,分析了冰的驰豫极化过程,并结合实验数据求解出了冰的复介电常数与温度的关系,提出了一种复阻抗式结冰探测技术下的温度补偿方法。为了提高温度补偿准确性,降低标定工作量,通过对驰豫极化理论的分析及温度漂移模型的构建,实现了准确可靠的温度测量补偿方法,该方法减小了结冰厚度对温度补偿效果的影响,极大降低了复阻抗参数温度补偿工作的复杂度。结冰实验结果表明,本文提出的温度补偿方法在-24℃~-3℃的环境温度条件下,可将温度漂移对测量结果的影响减少80%以上,有望显著提高复阻抗式结冰探测器的温度补偿准确性及标定效率,具有一定的工程应用价值。  相似文献   
6.
研究了不同Sn含量流变铸造AZ91合金的组织演化、拉伸行为及磨损性能。结果表明:Sn的合金化改变了Al在镁基体中的固溶度,并且显著细化了微观组织。加入0.8%(质量分数,下同)的Sn后,合金平均晶粒尺寸从105.0 μm降至42.1 μm。高熔点的金属间化合物为析出相提供了异质形核点,这些弥散析出的第二相在流变凝固过程中有效地细化了镁基体。弥散分布的第二相抑制了枝晶组织生长,从而进一步提升了合金的力学性能。随着Sn含量的增加,合金磨损率显著降低,磨粒磨损逐渐消失。3.0%Sn合金化的流变铸造AZ91合金具有最高的抗拉伸强度以及最好的耐磨损性能。  相似文献   
7.
The recycling of solid waste is a win-win solution for humans and nature. For this purpose, magnesite tailings and silicon kerf waste were employed to prepare MgO–Mg2SiO4 composite ceramics by solid-state reaction synthesis in the present work. Then, effects of sintering temperature and raw material ratio on as-prepared ceramics were systematically studied. As-prepared ceramics showed improvement in their relative density (from 47.55%–68.12% to 90.96%–95.25%) and cold compressive strength (from 7.34–118.66 MPa to 303.39–546.65 MPa) with the increase in sintering temperature from 1300 to 1600 °C. In addition, it was found that Si promoted synthesis process of Mg2SiO4 phase through transient liquid phase sintering and Fe2O3 accelerated sintering process through activation sintering. Consequently, the presence of Mg2SiO4 phase effectively improved the density and strength of MgO–Mg2SiO4 composite ceramic, while reducing its thermal conductivity. This work provides a potential reutilization strategy for magnesite tailings, and as-prepared products are expected to be applied in fields of construction, metallurgy, and chemical industry.  相似文献   
8.
介绍了二元、三元和多元等不同结构甲基丙烯酸酯类共聚物对柴油低温流动性能的改进效果,总结了纳米改性和复配等手段对聚甲基丙烯酸酯类降凝剂的改进效果,进而指出了未来降凝剂的发展和改进方向,为新型高效降凝剂的开发和应用提供参考.  相似文献   
9.
Silica-based ceramic cores are extensively used in investment casting process, during which they must exhibit sufficient flexural strength and deformation resistance. In this study, micro-sized mullite was used as an additive to silica-based ceramic cores to optimize their high temperature properties. To investigate the effects of micro-sized mullite on cristobalite crystallization, mechanical and thermal properties of silica-based ceramic cores, ceramic cores with different amounts of micro-sized mullite were fabricated. The XRD results showed that additional micro-sized mullite diminished the crystallization of cristobalite at high temperatures, primarily caused by the mullite related compressive stresses on the surface regions of fused silica particles. Three-point bending tests and SEM results showed that micro-sized mullite had a more significant effect on the flexural strength of ceramic cores compared with conventional additives. Particularly, the fracture mechanism of silica-based ceramic cores had been changed from intergranular fracture into a mixed fracture consisting of both intergranular and transgranular fracture. The mechanical and thermal properties of ceramic cores were all reduced slightly as the mullite content exceed 4.6 wt%. Hence, to optimize the properties of silica-based ceramic cores, the micro-sized mullite content should not exceed 4.6 wt%.  相似文献   
10.
采用纵向和横向两条线进行"虚拟仿真综合实训"课程思政内容设计.纵向即按照实训的不同阶段来安排思政内容,横向即按照实训的不同主体单位来安排思政内容.对"虚拟仿真综合实训"课程思政教育教学体系的探索,必将使学生在学习专业技能的同时不断提高自身思想政治水平,真正成为德才兼备的新时代人才.  相似文献   
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