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1.
The effectiveness of the hybrid system sonication followed by wet oxidation (SONIWO) to treat otherwise refractory waste has been demonstrated. In such a hybrid system homogeneous CuSO4 catalyst was found to be very efficient.  相似文献   
2.
This paper describes the parameters that are important in the industrial practice of silver removal from photographic fixers. The experiments were performed under potentiostatic control using synthetic solutions. The current efficiency was analysed as a function of the cathodic potential taking into account the deposit quality. A cathodic potential of ?0.5 V against a saturated calomel electrode is recommended. The conditions to prevent the darkening of the electrodeposit were investigated. The determination of silver concentration in the solution was made by direct potentiometry. The results obtained with synthetic fixers were corroborated by making the silver deposition from commercial fixers in an electrochemical reactor with rotating cylinder electrode intercalated in an electrolytic flow circuit in order to simulate practical conditions.  相似文献   
3.
Laboratory-scale and parametric experiments of SO2 and NOx removal from the simulated combustion gas by pulsed corona discharge have been performed by changing the combustion gas composition and temperature, the electrode configuration of plasma reactor, and the polarity of high-voltage electrode. The following results are obtained: 1) the higher the concentration of H2O and O2, the higher the efficiency of desulfurization and denitrification at the same specific input; 2) the pulsed corona discharge with a voltage pulsewidth as short as 200 ns of negative polarity shows the possibility to attain almost 90 percent deSOx and deNOx efficiency at the specific discharge input of 20 J/g, which is almost the same as the specific input in the electron-beam process; 3) the deNOx characteristics show a little temperature dependence in the range of 70 to 130°C, but the deSOx efficiency increases rapidly in the temperature region below 100°C suggesting the thermochemical dependence of deSOx reaction; 4) when desulfurization and denitrification proceed, the white dendritic powder deposits on the plasma reactor whose composition is identified to be 49 mol% (NH4)2SO4 and 47 mol% of 2NH4NO3 · (NH4)2SO4, and the ratio of SO2, NO and NH3 of the deposit is almost equal to that of supplied gas.  相似文献   
4.
Shear rate vs. shear stress data were obtained on avocado pulp in water emulsions using a concentric cylinder rheometer and fitted to a power law model. Dilution, as volume fraction of water, had a pronounced effect on the apparent viscosity of the pulp emulsions and the Richardson equation, (ηR= exp.( a φ) for the emulsion viscosity fitted the data well. A mean slope coefficient, a , of 4.57 can be used as a first approximation. Enzymatic treatment (40°C, 1 h), is slightly more effective than thermal treatment (65°C, 1 h), in reducing the initial apparent viscosity of the pulp-water emulsions  相似文献   
5.
High resolution XPS analysis of chemical functionalised multi-wall carbon nanotubes (MWCNTs) and single wall carbon nanotubes (SWCNT) was done with ESCA300 (overall instrument resolution of 0.35 eV). Information to the degree of functionalisation was ascertained by argon ion bombardment of the samples followed by XPS analysis to detect the functional groups, the percentage atomic concentration of various elements present and whether or not the detected functional groups imposed a chemical shift on the CNT atoms. The results show that true chemical functionalisation was achieved and by argon ion bombardment these functional groups can be altered relative to the C 1s carbon atoms of the CNT. The choice of chemicals used for functionalisation, the techniques employed and the types of nanotubes treated are important factors in chemical characterisation. The carbon atom on the nanotube ring to which the functional group (atom) is bonded, the chirality of the CNT, the electronegativity of the functional group, the bond type and whether the CNT is single-wall or multi-wall, or cut (short) could play a role in determining the chemical shift on the CNTs atoms. These investigations are relevant to chemical functionalisation of carbon nanotubes for various applications for example DNA sensors and other biomedical sensors.  相似文献   
6.
Shu-Juan Zhang  Hui-Min Feng 《Carbon》2006,44(10):2059-2068
A novel method was developed for the fabrication of activated carbon fiber (ACF) with wet spinning polyvinyl alcohol (PVA) fibers as the precursors. Through a combination of preoxidation, dehydration, carbonization and activation under a certain tension, PVA-based ACFs (PVA-ACFs) with high yields and good mechanical properties were obtained. The surface and cross-section morphologies, pore structures, surface geometries, surface functional groups and crystal structures of the PVA-ACFs were characterized using field emission scanning electron microscopy, low temperature nitrogen adsorption, Fourier transformed infrared spectrophotometry, X-ray photoelectron spectroscopy and X-ray power diffraction. All the PVA-ACF samples prepared had lotus root-like axially meso- and macroporous structures with the domination of micropores. Fractal geometries of PVA-ACFs deduced from nitrogen adsorption isotherms indicates that capillary force dominated in the interactions between nitrogen and the PVA-ACFs. The surface functional groups of the PVA-ACFs depend on the activating agents. Graphitoidal crystal structures were observed for the PVA-ACFs. The small crystal size and short range ordering between the crystallites ensured a high specific surface area of the PVA-ACFs.  相似文献   
7.
云南省永善县云荞水库自建成蓄水以来运行良好,2008年5月12日,四川省汶川县发生8.0级地震,云荞水库震感强烈,水库内水浪约1.0m高,水库受损,面板裂缝加大;震后云荞水库工程管理局高度重视云荞水库的安全问题,特请某水利水电勘测设计研究院对面板进行健全性检测,管理局根据检查单位对大坝面板的整体性能做出的评价及提出相应的处理意见,对面板裂缝进行了化学灌浆和表面封闭处理,至今运行良好。  相似文献   
8.
An original process of superficial thermal treatment is described. This process has been successfully applied to partially stabilized yttria-zirconia coatings (ZrO2-Y2O3) to increase the lifetime of the thermal barriers. A thin superficial layer was melted, and morphological transformations were observed. A microstructural comparison between as-sprayed layers and thermally treated layers is presented.  相似文献   
9.
邓忠民 《贵金属》1992,13(2):43-45
研究了热处理对Ag-15Al(at%)固溶体合金电阻率和有序参数的影响,由X射线衍射分析表明,合金的短程序转变不是Ag_3Al化合物型的δ第二相的形成,而是α-Ag-Al固溶体原子的有序排列。  相似文献   
10.
12Cr2MoWVTiB钢焊后热处理工艺改进的研究   总被引:2,自引:0,他引:2  
研究了焊后热处理保温时间对12Cr2MoWVTiB钢的显微组织及力学性能的影响。结果表明,在其它条件不变的情况下,焊后热处理保温时间由原来1.5h缩短为1h,既可以满足其组织性能的要求,又缩短了生产周期,降低了生产成本。  相似文献   
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