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1.
对航天用紧固件TC4钛合金棒材进行固溶时效处理,对棒材不同位置进行显微组织观察、硬度和室温拉伸性能检测。结果表明:TC4钛合金棒材经固溶时效后表面至心部的组织与性能受冷却速度的影响呈现显著差异。固溶时效后的显微组织由稳定的等轴α相、弥散的马氏体α′相和亚稳定β相组成,试样端面上因冷却速度相差不大,次生α相的形态和含量没有明显差异;中部截面上边部至心部的次生α相含量逐渐增多,同时次生α相片层厚度逐渐增大并趋于等轴化。端面上不同位置显微硬度值没有明显差异,但中部截面上由边部至心部的显微硬度值呈总体降低趋势,且中部截面上边部的显微硬度值与端面相差不大。试样心部因固溶过程中冷却缓慢,整体试样的室温拉伸性能明显低于去除心部的试样。 相似文献
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以玉米粉作为主要原料,利用蛹虫草固态发酵同时生产多糖和纤溶酶。以多糖含量和纤溶酶活力为指标,通过单因素和正交试验优化了蛹虫草固态发酵培养基和培养条件。结果表明:培养基由玉米粉和麸皮构成,比例为18:2(g/g),料水比例1:1(m/V),接入6%(V/m)蛹虫草液体菌种,23℃发酵时间3 d。在优化条件下获得浸提液中的胞外多糖含量为3.23 mg/mL,纤溶酶在血纤维蛋白平板上形成的溶圈面积为169.34 mm2。研究结果为生产蛹虫草功能食品基料提供了基础。 相似文献
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Noor Zamin Khan Sayed Ali Khan Muhammad Sohail M. A. Majeed Khan Jahangeer Ahmed Li Zhan Feihong Wang Muhammad Tahir Abbas Xin Xu 《Journal of the American Ceramic Society》2021,104(9):4911-4922
The trivalent rare-earth (RE3+) doped phosphors show tremendous achievement in narrow band multicolor line emission for various applications. However, the 4f–4f absorption transition of these ions is forbidden in UV and blue light excitation. Usually, a sensitizer having spin allowed transition was used as a co-dopant to excite these ions via the energy transfer phenomenon. Another approach promisingly using to excite these ions by efficient energy transfer from the intrinsic emission of the Ca2LuTaO6 double perovskite phosphors host lattice. Phosphors of Ca2LuTaO6 with double perovskite structure were synthesized by using a high-temperature solid-state reaction method. The produced Ca2LuTaO6 double perovskite phosphors show an intrinsic broad band emission centered at 424 nm under the excitation of 313 nm UV light. The origin of this broad band blue emission was deeply investigated by using computation and experimental approaches. The trivalent activator Dy3+ and Eu3+ were doped is a single and co-dopant in the produced Ca2LuTaO6 phosphors to check their excitation in UV and near-UV spectral region. X-ray diffraction and scanning electron microscopy were used to investigate the structure and phase analysis. Various characterizations such as photoluminescence excitation, emission, and CIE chromaticity coordinates were measured which illustrate the potential of Dy3+ and Eu3+ activated Ca2LuTaO6 double perovskite phosphors for narrow band multicolor line emission for various applications. 相似文献
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Yi Qin Tao Xiong Ting Zhao Jianfeng Zhu Jun Yang Yi Liu Xingang Kong Xiaohan Li 《Ceramics International》2021,47(9):12641-12650
The strengthening method of multi-element M-site solid solution is a common approach to improve mechanical properties of MAX phase ceramic. However, the research on capability of multi-element A-site solid solution to improve mechanical properties has rarely been reported. Thereupon, quasi-high-entropy MAX phase ceramic bulks of Ti2(Al1?xAx)C and Ti3(Al1?xAx)C2 (A = Ga, In, Sn, x = 0.2, 0.3, 0.4) were successfully synthesized by in situ vacuum hot pressing via multi-elements solid solution. The multi-elements solid solution in single-atom thick A layer was confirmed by X-ray diffraction and X-ray photoelectron spectroscopy as well as by energy dispersive X-ray spectroscopy mappings. Effects of doped multi-elements contents on the phase, microstructure, mechanical properties, and high temperature tribological behaviors were studied. Results demonstrated that the Vickers hardness, anisotropic flexural strength, fracture toughness, and tribological properties of Ti–Al–C based MAX ceramics could be remarkably improved by constitution of quasi-high-entropy MAX phase in A layers. Moreover, the strengthening and wear mechanisms were also discussed in detail. This method of multi-element solid solution at A-site provides new way to enhance mechanical properties of other MAX phase ceramics. 相似文献
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《中国有色金属学会会刊》2021,31(10):3063-3074
The transient liquid phase (TLP) bonding of CoCuFeMnNi high entropy alloy (HEA) was studied. The TLP bonding was performed using AWS BNi-2 interlayer at 1050 °C with the TLP bonding time of 20, 60, 180 and 240 min. The effect of bonding time on the joint microstructure was characterized by SEM and EDS. Microstructural results confirmed that complete isothermal solidification occurred approximately at 240 min of bonding time. For samples bonded at 20, 60 and 180 min, athermal solidification zone was formed in the bonding area which included Cr-rich boride and Mn3Si intermetallic compound. For all samples, the γ solid solution was formed in the isothermal solidification zone of the bonding zone. To evaluate the effect of TLP bonding time on mechanical properties of joints, the shear strength and micro-hardness of joints were measured. The results indicated a decrement of micro-hardness in the bonding zone and an increment of micro-hardness in the adjacent zone of joints. The minimum and maximum values of shear strength were 100 and 180 MPa for joints with the bonding time of 20 and 240 min, respectively. 相似文献
9.
《Journal of the European Ceramic Society》2021,41(13):6548-6558
To repair the damaged SiC coated C/C composites, a double-layer coating including a SiO2-Nd2O3 external layer (∼60 μm) and a Si-SiC inner layer (∼240 μm) was prepared by a slurry-based laser cladding technique, and the laser-ablation tests under two heat fluxes (23.89/39.81 MW m−2) were performed. The spectrophotometer, X-ray diffraction, scanning electron microscopy and 3D profilometer were used for characterization. For avoiding the secondary damage of laser-ablation, the laser-reflection of the repaired area was enhanced, which was conducive to the mitigation of mass and linear ablation. Combined with Finite Element Analysis, by raising the reflectivity, the surface and back temperature of samples could be reduced greatly by 1224 K and 983 K respectively, and plenty of ablation reactions could be avoided. Therefore, the SiO2-Nd2O3 coating possessed an excellent laser-ablation resistance and protected the C/C substrates from thermal damage and oxidation effectively. 相似文献
10.
原油、天然气长输管道建设完工后,必须要进行管径通径检测,其目的在于发现施工过程可能产生的管道异常变形。我们以检测管径原始尺寸完整性为目标,进行管道变形缺陷数字化建模、非接触通径检测器运行过程控制、制造工艺、系统优化等方面的研究,基于激光传感器等技术的结合,研发了新型非接触式智能管道通径检测器,弥补传统的接触式(机械式)通径检测器运行状态不稳定造成的数据信号失真、探头易磨损、维护费用高等不足之处,提高了管道内壁变形缺陷识别、数据采集以及变形量大小、变形点位置分析处理的准确性,据此进行开挖作业,对管道及时进行修整,消除事故隐患,为油气长输管道的安全生产运行提供保障。本文重点介绍了该非接触式智能管道通径检测器的工作原理、结构特点的设计分析。 相似文献