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排序方式: 共有2369条查询结果,搜索用时 31 毫秒
1.
《Ceramics International》2021,47(23):32610-32618
AA7075 + 6%B4C+3%ZrC nano hybrid composite was successfully fabricated, with nano reinforcements composition in AA7075 alloy selected based on previous investigation, to achieve better mechanical performance. Two different sintering techniques, namely conventional and microwave, were implemented to determine the effect on microstructural and mechanical properties. Microstructural investigation was performed with the help of W-SEM. Tensile, compression, and hardness were measured with the help of UTM and Vickers microhardness machine. Porosity was calculated by using Archimedes principle. It was observed that the added nano ZrC particles formed agglomerates and the B4C particles were distributed homogenously. Composites processed by microwave sintering showed excellent mechanical properties compared to the conventionally sintered composites. No intermetallic compounds were detected in microwave sintered composites through XRD analysis, indicating strong and clean interface bonds between matrix and reinforcement particles. High strain to fracture value of 12.24% was noted in microwave sintered nano hybrid composite, while it was 6.12% for conventional sintered one. Fractography revealed no peeling action of reinforcements from the matrix material, and the mode of failure was brittle. It was concluded that, while fabricating nano range hybrid composites, the implementation of advanced sintering technique (microwave sintering) with low sintering temperatures and low sintering times with internal heat generations, helps in eliminating defects that may develop because of high surface energies of nano range reinforcements. 相似文献
2.
Effect of milling ball size on the densification and optical properties of transparent Y2O3 ceramics
Hyeon-Myeong Oh Young-Jo Park Ha-Neul Kim Jae-Woong Ko Hyun-Kwuon Lee 《Ceramics International》2021,47(4):4681-4687
In this study, we report highly transparent Y2O3 ceramics fabricated by hot-pressing only at 1500 °C without a HIP treatment, featuring in-line transmittance levels of 77% and 84% at a wavelength of 400 and 1100 nm, respectively with the grain size suppressed to 710 nm. The effect of the ball size during the grinding of Y2O3 powders on the correlation between the thus-prepared Y2O3 powders and the optical properties of the hot-pressed samples is demonstrated for the first time. With a decrease in the diameter of the ZrO2 balls from 5 mm to 1 mm, the milling efficiency was enhanced and admirable transparency of Y2O3 was attained at a short milling time. However, several micron-sized pores remained in the transparent specimens prepared with 1 mm balls, originating from the inhomogeneously packed region of the green body. Finally, the 2 mm was found to be optimum for obtaining a fine-grained and pore-free microstructure with the best in-line transmittance of Y2O3 ceramics. 相似文献
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黑钨矿极易发生泥化现象,导致其有效浮选仍是一个难题。本研究在实验室球磨机中,探讨了不同尺寸的钢球作为介质对黑钨矿细度和形状的影响,在干磨条件下进行了6种不同球径(20、30、40、50、60、70 mm)的磨矿试验。结果如下所示:各磨矿条件下获得的产品粒径均随磨矿时间的增加而减小。以70 mm钢球为磨矿介质时,大颗粒含量最低,-10μm过磨颗粒含量最高。这些粒径比x80/x20随着产品尺寸的减小先增大后减小,每一个球的粒径都趋于平缓。中值粒径x50随球径的减小先减小后增大,其中40mm球径最小(0.06 mm);但当球直径小于40 mm时,破碎混合颗粒物料的粉碎能力减弱。在相同的磨矿时间下,粒径比x80/x20随球径的减小先增大后减小,其中40mm球的粒径比最大;对于40mm钢球,产品的细度和宽度不一致,因此选择钢球直径不容易。当球直径小于40 mm时,粒径比x90/x10越来越大。粒径比(x90-x10)/x50随着产品粒径的减小先增大后减小,减小趋势随着球径的减小而趋于平缓,在x50为0.075 mm-0.085 mm范围内达到最大;另一方面,20毫米球下,(x90-x10)/x50磨矿产品尺寸几乎是不变的,为20.66。当产品粒径小于1 mm时,产品颗粒的球形度急剧增加,且随着球直径的减小,球形度增加的更快。当产品粒径小于0.04 mm时,产品颗粒球形度的变化趋势趋于平缓,这可能是在磨机内表面和球表面形成粘附颗粒层。0.8 ~ 0.3 mm的球形度变化趋势小于0.3 mm以下的球形度变化趋势。 相似文献
5.
《Advanced Powder Technology》2022,33(3):103450
In the present investigation, systematic grinding experiments were conducted in a laboratory ball mill to determine the breakage properties of low-grade PGE bearing chromite ore. The population balance modeling technique was used to study the breakage parameters such as primary breakage distribution (Bi, j) and the specific rates of breakage (Si). The breakage and selection function values were determined for six feed sizes. The results stated that the breakage follows the first-order grinding kinetics for all the feed sizes. It was observed that the coarser feed sizes exhibit higher selection function values than the finer feed size. Further, an artificial neural network was used to predict breakage characteristics of low-grade PGE bearing chromite ore. The predicted results obtained from the neural network modeling were close to the experimental results with a correlation of determination R2 = 0.99 for both product size and selection function. 相似文献
6.
Jiri Cermak Lubomir Kral Pavla Roupcova 《International Journal of Hydrogen Energy》2021,46(27):14494-14507
Effect of chemical composition of Mg-xCu based alloys (x = 9.94–58.00 wt %) modified by KCl upon their hydrogen storage performance was studied. Kinetic curves and pressure-concentration isotherms were measured in the ranges up to 60 bar and 388 °C, respectively. It was observed that desorption rate dc/dt is not significantly influenced by the composition. Unknown Cu-rich phase was detected that has shown a catalytic effect on desorption from a mixture with other phases. Activation energy of hydrogen desorption decreased with increasing x from 180 kJ/mol down to 98 kJ/mol. Average hydride dissociation enthalpy, ΔH, for the lowest plateau was 75 kJ/mol which is equal to literature value for pure Mg. Slightly lover average value, 67 kJ/mol was obtained for the second plateau and ΔH for the third one decreased from 70 kJ/mol for the lowest to 49 kJ/mol for the highest x. 相似文献
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Type 316LN stainless steel (SS) is the principal structural material for the components of sodium cooled fast reactors operating under elevated temperature conditions. In order to assess the degradation in strength of service exposed components using a small specimen testing technique such as automated ball indentation (ABI), it is necessary to carry out prior detailed ABI studies on the virgin material. In this investigation, the tensile behaviour of as-received 316LN SS were investigated at several temperatures in the range 298–973 K using ABI technique. The load-depth of indentation data measured from ABI tests was analyzed using semi-empirical relationships to obtain the tensile properties. The yield stress and the flow curves were determined by correlating ABI results with corresponding uniaxial tensile test results. Trend curve for tensile strength with temperature, as estimated from ABI tests, exhibited a plateau region in the temperature around 823 K, similar to uniaxial tensile tests. The variations of strength coefficient, strain hardening exponent, yield ratio, hardness and uniform ductility with temperature were evaluated from ABI tests. The ABI technique was found to estimate the influence of temperature on tensile properties sensitively. 相似文献
9.
《International Journal of Hydrogen Energy》2020,45(3):2084-2093
In this study, we propose a method to produce nanocrystalline TiFe powder by high-energy ball milling, in order to avoid the common sticking problem of the material to the milling tools, assuring a material prompt to absorb hydrogen as well. The method consists of making a preliminary milling operation with the elemental powders (50:50 stoichiometric ratio) to form a strong adhered layer of the milled material on the surfaces of the vial and balls. The main milling operation is then performed with a new powder charge (same composition as before), but now adding a process control agent (stearic acid). Various processing times - 2, 6, 10 and 20 h - were used in the milling experiments. Nanocrystalline TiFe was synthesized in this way with low oxygen contamination, full yields for milling times of 6 h or over, requiring no heat treatments for the first hydrogen absorption. Hydrogen storage capacity of 1.0 wt% at room temperature under 20 bar was attained by the sample milled for 6 h. Kinetic data from samples milled for 2 h and 6 h agreed with Jander model for the rate limiting step of the hydriding reaction, which is based on diffusion with constant interface area. 相似文献
10.
Ball screws are crucial for improving the reliability and interchangeability of transmission mechanical systems; however, existing contact measurement methods that utilise stylus contact are not efficient, which precludes their use for rapid in-situ geometry evaluation. This paper presents a vision-based two-stage method for rapid measurement of key parameters (raceway arc radii and centre distance) of ball screws. The edge contour information is extracted from the acquired image using the dual-tree complex wavelet transform and non-maximal suppression. In the matching stage, a shape-matching algorithm is used for detecting approximate geometrical centres of raceway arcs. The refinement stage, on the other hand, is implemented for acquiring precise dimensional results. Furthermore, the method of averaging multiple measurements is performed to suppress random noise. A comparative experiment is presented to validate the robustness of the proposed method. Based on experimental results, the calculated mean absolute errors in the measurement of the two raceway arc radii and the centre distance are found to be 0.0082 mm, 0.0079 mm and 0.0055 mm, respectively. This study therefore paves the way for key parameter measurement without removing ball screws. 相似文献