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Xing-Han Chen Kun Zhai Guo-Yu Qian Qing-Shan Fu Chiranjib Chakrabarti Cang-Long Li Hong-Xia Yin Yang Qiu Zhao-Ming Tian Song-Liu Yuan 《Journal of the American Ceramic Society》2021,104(7):3334-3343
The influence of applied magnetic field during annealing process as well as of Mg doping on the room-temperature magnetoelectric coupling effects in BaSrCo2-xMgxFe11AlO22 are experimentally studied through the magnetization, magnetodielectric, and magnetoelectric current measurements. Hexaferrite samples of Co2Y were found to be highly oriented by an applied magnetic field (Ho) during the annealing process, leading to an enhancement of the room-temperature magnetoelectric coupling effects. Although the substitution of nonmagnetic Mg ions in Co sites tends to reduce the ferromagnetism at macroscopic scale, a proper amount of Mg doping content facilitates the superexchange interaction between the adjacent magnetic blocks; meanwhile modulates the magnetic anisotropy in the samples. An appropriate adjustment of the competition between the anisotropy and the superexchange could enhance the magnetoelectric coupling at room temperature, which can be confirmed by the magnetic-field-induced dielectric constant and current density study. 相似文献
3.
《Ceramics International》2021,47(21):30358-30366
Stereolithography-based 3D printing is a promising method to produce complex shapes from piezoceramic materials. In this study, LCD-SLA 3D printing was used to create lead-free piezoceramics based on barium titanate (BaTiO3, BT). Three types of BT powders (micron, submicron and nanoscale) were tested in LCD-SLA 3D printing, and a technique for the preparation of a ceramic slurry suitable for LCD-SLA printing has been developed. Using TGA-DSC analysis, the thermal debinding parameters to obtain crack-free samples were determined, followed by further sintering and the study of the piezoelectric properties (εr = 1965, d33 = 200 pC/N, tan = 1,7 %). The results of the study demonstrate high potential for the production of complex piezoceramic elements that can be used in aviation, in particular, aviation radio equipment; in the marine industry for transceiver modules of hydroacoustic antennas; and in the nuclear industry for pressure control sensors in the steam–water path. 相似文献
4.
Christian Hopmann Nadine Magura Nicolas Rozo Lopez Daniel Schneider Kai Fischer 《Polymer Engineering and Science》2021,61(5):1353-1367
Wet filament winding technology has been extensively used for the manufacture of rotationally symmetric parts made of fiber-reinforced plastics (FRP). As the design and modeling of FRP-parts require numerous assumptions, deviations between calculated and achieved mechanical properties are expected. One aspect that contributes to this discrepancy is the assumption of a homogeneous rectangular cross-section of the fiber-band. In this work, the fiber-band geometry in a wet-winding process of carbon fiber cylinders is analyzed. An Infrared-optical system for the detection of the fiber bandwidth and winding-angle is implemented. The influence of the winding speed and the resin temperature is analyzed. An image processing algorithm for the automatic measurement of the fiber's bandwidth and winding-angle is developed. Manual and adaptive gamma corrections are implemented to improve image quality. A parameter study for the suitable selection of image processing parameters is performed. 相似文献
5.
探究聚合物辅料对难溶性药物结晶的影响机制,是指导无定形固体分散体制剂设计和制备中辅料筛选的关键。研究了不同因素(温度、搅拌速率、聚合物浓度、聚合物分子量和聚合物种类等)对阿司匹林晶体生长动力学的影响。首先,采用基于三种不同晶体生长机制的化学势梯度模型结合UNIQUAC活度系数模型,描述和预测了阿司匹林在不同条件下的结晶动力学。进一步分析了不同因素对晶体生长速率常数 和结晶热力学推动力 的影响以及对阿司匹林结晶动力学的影响机制。结果表明,阿司匹林晶体生长速率随着结晶温度、聚合物浓度的增加而降低,随搅拌速率的增加而升高;聚乙烯吡咯烷酮(PVP K25)和羟丙基甲基纤维素(HPMC E3)显著抑制了阿司匹林的晶体生长,在PVP K25和HPMC E3水溶液体系下阿司匹林的晶体生长属于二维成核机制,在纯水和PEGs水溶液体系下晶体生长属于粗糙生长机制。所采用的化学势梯度模型能很好预测不同温度和搅拌速率下阿司匹林的结晶动力学,可有效减少实验所需的人力、物力和财力。研究可为固体分散体制剂制备中聚合物的筛选提供理论研究基础。 相似文献
6.
基于方位特征(POC)方程的并联机构拓扑结构设计理论与方法,提出了一种能实现三平移一转动(3T1R)的2RRPaR+2RSS并联操作手机构。对该机构进行了结构特性分析,计算了其自由度及POC集,并得出其耦合度为2;依据该机构的结构特性及几何约束条件,采用二维搜索法对该机构的位置正解进行了求解,推导出了其位置逆解,并验证了位置正逆解的正确性;基于该机构的逆解公式,计算出其三维工作空间,并得到了一组Z向不同截面的切片形状,同时对Z=1000 mm截面处的转动能力进行了分析;最后,基于雅可比矩阵对机构奇异位形进行了分析。研究结果表明:所提2RRPaR+2RSS机构在与H4机构主要尺寸参数相同的情况下,其工作性能总体优于H4机构。与H4机构相比,所提机构的工作空间增加了27.87%,其转动能力提高了4.35%。 相似文献
7.
Bolun Wang Tao Wang Yong Ge Jianlin Lang Qiwei Sun Yuhong Chen Yue Yan 《应用聚合物科学杂志》2021,138(13):50125
Through a uniaxial hot compression method, polycarbonate (PC) plates were self-reinforced effectively by press-induced deformation. Relationships between macroscopic mechanical properties including tensile, impact as well as viscoelastic properties, and microscopic status such as morphologies and orientation were obtained in deformed PC plates. Results showed that PC plates which were compressed at appropriate temperatures (20°C–120 °C) obtained simultaneous enhancements in tensile strength (28%), elastic modulus (38%) and impact strength (700%), compared with the original plate. The impact fracture morphologies of deformed PC plates revealed evident ductile breakage. Wide-angle X-ray diffraction investigations were conducted to attribute mechanical behavior to molecular segment orientation, which was more sensitive to temperature. Self-reinforced mechanism was proposed to analyze the high correlation between various orientations of molecular segments and corresponding mechanical performance, explained by storage and loss moduli in dynamic mechanical analysis as supplemental verification. Press-induced deformation was proved to be a potentially effective method for the self-reinforcement treatment for PC transparent products. 相似文献
8.
针对现有谐振式磁传感器原理不能同时实现高品质因数(Q)和低功耗的缺点,利用双端固定石英音叉谐振器与铁镓磁致伸缩合金片复合,设计了一种隔离磁机阻尼的高Q值、数字频率输出的超低功耗谐振式磁传感器。利用音叉谐振器结构的解耦特性,设计应力耦合传递结构,隔离了磁致伸缩材料磁机阻尼,从而保证复合传感器Q值与音叉谐振器Q值相当。在磁场作用下,磁致伸缩力传递到音叉谐振器,由于音叉力敏感特性,实现磁-力-频率转换。制备了铁镓合金/石英音叉谐振器复合敏感结构,测试表明,在低气压封装条件下的品质因数约为16 764,门振荡电路功耗约为124.8μW,在线性区灵敏度为3.05 Hz/Oe,分辨率为6 mOe。 相似文献
9.
Panitha Phulkerd Atsuro Yamazaki Shohei Iwasaki Masayuki Yamaguchi 《Polymer Engineering and Science》2021,61(2):367-378
In this study, polypropylene (PP) films containing the β nucleating agent, N,N′-dicyclohexyl-2,6-naphthalenedicarboxamide, were prepared using PP with three different molecular weights (low, medium, and high) by extrusion process with T-shaped die. The structure and morphology of the films were studied after stretching. It was found that a unique molecular orientation, in which both the c-axis and crystalline lamellae were oriented perpendicular to the flow direction, was formed in all undrawn film samples, irrespective of the molecular weights of the PP. In the PP sheets stretched in the machine direction, the low-molecular-weight sample containing the nucleating agent exhibited brittle properties owing to a lack of tie chains in the stretching direction. In contrast, cavitation was prominent in the medium (M-PP)- and high (H-PP)-molecular-weight samples. Notably, M-PP containing the nucleating agent, with a high degree of molecular orientation, promoted the formation of a large number of voids. In H-PP containing the nucleating agent, the presence of numerous tie chains inhibited cavitation, resulting in fewer voids. The experimental results demonstrated the influence of the molecular weight on the void structure, which will be useful in the field of microporous membranes. 相似文献
10.