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1.
Raney-type Ni precursor alloys containing 75 at.% Al and doped with 0, 0.75, 1.5 and 3.0 at.% Ti have been produced by a gas atomization process. The resulting powders have been classified by size fraction with subsequent investigation by powder XRD, SEM and EDX analysis. The undoped powders contain, as expected, the phases Ni2Al3, NiAl3 and an Al-eutectic. The Ti-doped powders contain an additional phase with the TiAl3 DO22 crystal structure. However, quantitative analysis of the XRD results indicate a far greater fraction of the TiAl3 phase is present than could be accounted for by a simple mass balance on Ti. This appears to be a (TixNi1−x)Al3 phase in which higher cooling rates favour small x (low Ti-site occupancy by Ti atoms). SEM and EDX analysis reveal that virtually all the available Ti is contained within the TiAl3 phase, with negligible Ti dissolved in either the Ni2Al3 or NiAl3 phases.  相似文献   
2.
Drop-tube processing was used to rapidly solidify droplets of Ni64.7Fe10Si25.3 and Ni59.7Fe15Si25.3 alloys. In the larger droplets, and therefore at low cooling rates, only two phases, γ-Ni31Si12 and β1-Ni3Si were observed. Conversely, in the smaller droplets, and therefore at higher cooling rates, the metastable phase Ni25Si9 was also observed. The critical cooling rate for the formation of Ni25Si9 was estimated as 5 × 103 K s−1. SEM and TEM analysis reveals three typical microstructures: (I) a regular structure, comprising single-phase γ-Ni31Si12 and a eutectic structure between γ-Ni31Si12 and β1-Ni3Si; (II) a refined lamellar structure with a lamellar spacing <50 nm comprising γ-Ni31Si12 and β1-Ni3Si; (III) an anomalous structure with a matrix of Ni25Si9 and only a very small proportion of a second, and as yet unidentified, phase. These results indicate that there is an extended stability field for Ni25Si9 in the Ni-rich part of the Ni–Fe–Si ternary system in comparison to the Ni–Si binary system. With an increase of cooling rate, an increasing fraction of small droplets experience high undercoolings and, therefore, can be undercooled into the Ni25Si9 stability field forming droplets consisting of only the anomalous structure (III). The Fe atoms are found to occupy different substitutional sites in different phase, i.e. Fe substitutes for Ni in the γ phase and Si in the L121) phase respectively.  相似文献   
3.
Ordered porosity metal materials belong to a relatively new class of porous materials named gasars. This paper presents a mathematical model of the complex physical phenomena in the production of gasars. Analyses for heat transfer, solidification kinetics and gas diffusion were coupled to describe the formation of unique gasar structure. Several criterial functions were introduced to provide significant quantitative information about the relationship between the operating technological parameters and the final structure. The computational outcomes of the numerical simulation were compared with the characteristics of real gasar ingots. The model was applied to determine the boundary conditions that would provide approximately constant physical conditions on the solidification front. The structure sensitiveness of gasars with respect to the different technological parameters is discussed.  相似文献   
4.
Heat transfer of highly consistent shear-thinning fluids flowing in a horizontal cylindrical channel has been investigated numerically and experimentally when the outer channel wall is subjected to a constant convective heat exchange. The case considered being cooling, a possible ice deposit must be taken into account. The variation of the rheological properties with temperature must be considered as well.  相似文献   
5.
结合工程概况及工程特点,从机械设备配置、劳动力组织、现场管理等方面介绍了大窝山隧道进口Ⅱ级,Ⅲ级围岩段的快速掘进施工组织与管理措施,为类似隧道的快速掘进施工组织与管理提拱了相关经验.  相似文献   
6.
Directional solidification studies of gelatinized corn starch-water mixtures were undertaken in order to examine, in situ, the freezing behavior of this food model. The solidification rate was controlled by varying sample cell velocity as it moved from a 25°C hot stage to a -25°C cold stage. While freezing at cell velocities ≤7.5 μm/sec, starch granules were alternately pushed or entrapped by the advancing solid-liquid interface producing a segregated structure consisting of alternating high-starch and low-starch bands. At a cell velocity of 10 μm/sec, the frozen product was homogeneous. The relationship between the solid-liquid interface velocity and segregation behavior was quantified and compared to an existing model of particle-interface interactions.  相似文献   
7.
ListofSymbol  B———Buoyancy ,m·s- 2 ;  c———Concentrationofsoluteelement ;  Cμ———Turbulentconstant;  D———Diffusivityofsoluteelement ,m2 ·s- 1 ;  fl,fs———Liquidandsolidfraction ;  fμ———Turbulentcoefficient ;  h———Enthalpy ,J·kg- 1 ;  k———Turbulentkineticenergy ,m2 ·s- 2 ;  kp———Equilibriumpartitioncoefficient;  Kp———Permeabilityofmushyzone ,m2 ;  K0 ———Permeabilitycoefficient;  p———Pressure ,Pa ;  Pr———Prandtlnumber ;…  相似文献   
8.
This paper is a summary of an extensive research program carried out by the authors on the structure of rapidly solidified aluminum alloys; and a comparison with the work of others also involved in this field. The paper discusses the changes in the dendritic and non-dendritic structure of the matrix at cooling rates from 10–3 to 1010 K/s and discusses the hetergeneity of the structure caused by interdendritic-segretion during solidification.  相似文献   
9.
魏朋义  桂钟楼 《材料工程》1995,(6):10-11,42
利用ZM定向凝固装置研究了镍基单晶高温合金DD3在高温度梯度(700~1200K/cm)定向凝固条件下的微观组织演化特征及其对工艺参数的响应函数,结果表明:该合金在高界面温度梯度条件下,柱晶生长速度范围向高速区扩展,从而使单晶亚结构细化成为可能。所得单晶棒中亚结构一次间距可比传统HRS法定向凝固籽晶中相应尺度减小5~10倍。本文还对其组织演化机制进行了分析。  相似文献   
10.
YAG激光熔覆的研究现状与发展趋势   总被引:1,自引:1,他引:0  
本文介绍了YAG激光熔覆的特点,并与CO2激光进行了比较,显示了YAG激光熔覆的优势和潜力。叙述了YAG激光熔覆的研究进展及其应用前景。  相似文献   
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