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1.
Christopher J. Marvel Qirong Yang Scott D. Walck Kelvin Y. Xie Kristopher D. Behler Jerry C. LaSalvia Masashi Watanabe Richard A. Haber Martin P. Harmer 《Journal of the American Ceramic Society》2022,105(5):2990-3007
Compositional analysis of boron carbide on nanometer length scales to examine or interpret atomic mechanisms, for example, solid-state amorphization or grain-boundary segregation, is challenging. This work reviews advancements in high-resolution microanalysis to characterize multiple generations of boron carbide. First, ζ-factor microanalysis will be introduced as a powerful (scanning) transmission electron microscopy ((S)TEM) analytical framework to accurately characterize boron carbide. Three case studies involving the application of ζ-factor microanalysis will then be presented: (1) accurate stoichiometry determination of B-doped boron carbide using ζ-factor microanalysis and electron energy loss spectroscopy, (2) normalized quantification of silicon grain-boundary segregation in Si-doped boron carbide, and (3) calibration of a scanning electron microscope X-ray energy-dispersive spectroscopy (XEDS) system to measure compositional homogeneity differences of B/Si-doped arc-melted boron carbides in the as-melted and annealed conditions. Overall, the improvement and application of advanced analytical tools have helped better understand processing–microstructure–property relationships and successfully manufacture high-performance ceramics. 相似文献
2.
《Ceramics International》2022,48(6):8069-8080
Homogeneous thin films of Molybdenum oxide (MoO3) were grown on quartz and glass substrates using the thermal evaporation method. XRD results showed that the MoO3 powder has a polycrystalline structure with an orthorhombic crystal system whereas the MoO3 thin films have amorphous nature. SEM images showed that the MoO3 thin films have a nearly uniform surfaces with worm-like shape grains. The film thickness influences on the linear and nonlinear optical characteristics of MoO3 thin films that were examined using spectrophotometric measurements and from which, the linear optical constants of the MoO3 thin films were estimated. The electronic transition type was determined as a direct allowed one. The values of the optical band gap were obtained to be in the range of 3.88–3.72 eV. The dispersion parameters, third-order nonlinear optical susceptibility, and the nonlinear refractive index of the MoO3 thin films were determined and interpreted in the light of the single oscillator model. The temperature dependence of the DC electrical conductivity and the corresponding conduction mechanism for the MoO3 films were investigated at temperatures ranging from 303 to 463 K. 相似文献
3.
摘 要:为了提高码索引调制(code index modulation,CIM)系统的传输效率,提出了一种具有更低复杂度的单输入单输出(single input single output,SISO)的广义正交码索引调制(generalized orthogonal code index modulation,GQCIM)系统。CIM 系统使用扩频码和星座符号传输信息,但只能激活两个扩频码索引和一个调制符号。而 GQCIM 系统以一种新颖的方式克服了只激活一个调制符号的限制,同时充分利用了调制符号的正交性,增加扩频码索引以传输更多的额外信息位,提高了系统的传输效率。此外,分析了GQCIM系统的理论性能,推导了误码率性能的上界。通过蒙特卡罗仿真验证了GQCIM系统的性能,对比发现GQCIM系统的理论和仿真性能一致。而且在相同的传输效率下,结果显示GQCIM系统的性能优于同样具有正交性的调制系统,如广义码索引调制(generalized code index modulation,GCIM)系统、CIM系统、码索引调制-正交空间调制(code index modulation aided quadrature spatial modulation,CIM-QSM)系统、码索引调制-正交空间调制(code index modulation aided spatial modulation,CIM-SM)系统、脉冲索引调制(pulse index modulation,PIM)系统。 相似文献
4.
Effect of heat loss on the syngas production by fuel-rich combustion in a divergent two-layer burner
《International Journal of Hydrogen Energy》2022,47(34):15270-15281
The effect of heat loss on the syngas production from partial combustion of fuel-rich in a divergent two-layer burner is numerically studied using two-dimensional model with detailed kinetics GRI-Mech 1.2. Both the radiation and wall heat losses to the surrounding are considered in the computations. It is shown that two types heat losses have different effects on the syngas production. The radiation heat loss has significant effect on the syngas temperature and the syngas temperature is dropped as radiation heat loss is increased, but it has neglected effect on the reforming efficiency and methane conversion efficiency. The wall heat loss has a comprehensive effect on the syngas production. The wall heat loss not only reduces the conversion efficiency, but also significantly decreases the syngas temperature. The effect of wall heat loss becomes weak as the equivalence is increased. The reforming efficiency drops from 0.440 to 0.424 for equivalence ratio of 2 and mixture velocity of 0.17 m/s for the predictions between adiabatic wall and non-adiabatic conditions. 相似文献
5.
《Journal of the European Ceramic Society》2021,41(15):7381-7403
Silica-based ceramics have been explored extensively as a class of versatile materials for various applications in architecture, catalysis, energy, machinery, and biomedical engineering. Nevertheless, comprehensive information on silica-based ceramic and electromagnetic microwave (EMW) absorption is scarce, although excellent progress has been made in this field. Here, recent progress in the investigation of silica-based ceramics toward EMW absorption is reviewed. We first introduced the basis of ceramics (characteristics, classification, synthetic methods, potential applications). Subsequently, the silica-based ceramics, including Si-based oxides and alloys, SiOC/SiC/Si3N4/SiCN-based composite, Ti3SiC2 and composite for EMW absorption were systematically summarized. Notably, the fabrication strategies, absorption properties, and mechanisms of silica-based ceramics are described in detail, with a focus on structure and component design. Lastly, the prospects and ongoing challenges of this field in the future are presented. This review is expected to learn from the past and achieve progress toward the future of silica-based ceramic for EMW absorption. 相似文献
6.
Yingfeng XU Youiun HU Xiaodong ZHANG Xingyuan XU Lei YE Xiaotao XIAO Zhen ZHENG 《等离子体科学和技术》2021,23(9):95102-23
NBI fast ion losses in the presence of the toroidal field ripple on EAST have been investigated by using the orbit code GYCAVA and the NBI code TGCO. The ripple effect was included in the upgraded version of the GYCAVA code. It is found that loss regions of NBI fast ions are mainly on the low field side near the edge in the presence of ripple. For co-current NBIs, the synergy effect of ripple and Coulomb collision on fast ion losses is dominant, and fast trapped ions located on the low field side are easily lost. The ripple well loss and the ripple stochastic loss of fast ions have been identified from the heat loads of co-current NBI fast ions. The ripple stochastic loss and the collisioninduced loss are much larger than the ripple well loss. Heat loads of lost fast ions are mainly localized on the right side of the radio frequency wave antennas from the inside view toward the first wall. For counter-current NBIs, the first orbit loss due to the magnetic drift is the dominant loss channel. In addition, fast ion loss fraction with ripple and collision for each NBI linearly increases with the effective charge number, which is related to the pitch angle scattering effect. 相似文献
7.
微波隔离器是微波系统中不可或缺的器件,常见的隔离器都采用了铁氧体旋磁材料配合吸收负载实现电磁波的单向传输。这种器件虽然可以使电磁波单向传输,但是并不能改善能量的浪费问题,还增加了系统的复杂度。针对上述问题,本文基于电磁超材料设计了一种微波单向传输的圆波导,使用波导内壁涂覆折射率逐渐变化的材料来影响电磁波的传输特性,从而实现电磁波单向传输。本文给出了微波单向传输的电磁计算模型和超材料结构及属性,并通过简化这种超材料使其易于实现;最后通过电磁仿真分析了这种材料的电磁特性并给出了这种材料的实现方法。 相似文献
8.
This study evaluates environmental aggressiveness and atmospheric galvanic corrosivity categories in Chile (Classification of Industrial and Marine ATmospheres test) by installing bolts in electrical transmission towers in the Valparaiso region across four exposure sites: Playa Ancha, San Sebastián, Las Vegas, and San Felipe. Classifications of marine corrosion index (MCI), industrial corrosion index (ICI), and atmospheric corrosion index (ACI) used different galvanic couples: aluminum/steel for MCI, aluminum/copper for ICI, and aluminum/polyethylene for ACI. Corrosion indices varied by season (summer, autumn, winter, and spring), for which couples were exchanged every 3 months. Intraseason variation depended mainly on the meteorochemical variables of the zone, the Cl−/SO2 ratio, and the presence of general and pitting corrosion in the aluminum. The results indicate that, regardless of environmental condition, the aluminum in Al/steel (MCI) and Al/copper (ICI) couples presented a higher corrosion rate than when not forming a galvanic couple (ACI). Moreover, under higher environmental chloride, these differences increase. The Playa Ancha station presented the highest ACI. 相似文献
9.
Xiaoqin Yang Huy Q. Ta Huimin Hu Shuyuan Liu Yu Liu Alicja Bachmatiuk Jinping Luo Lijun Liu Jin-Ho Choi Mark H. Rummeli 《Advanced functional materials》2021,31(38):2104340
In this study, in situ transmission electron microscopy is performed to study the interaction between single (monomer) and paired (dimer) Sn atoms at graphene edges. The results reveal that a single Sn atom can catalyze both the growth and etching of graphene by the addition and removal of C atoms respectively. Additionally, the frequencies of the energetically favorable configurations of an Sn atom at a graphene edge, calculated using density functional theory calculations, are compared with experimental observations and are found to be in good agreement. The remarkable dynamic processes of binary atoms (dimers) are also investigated and is the first such study to the best of the knowledge. Dimer diffusion along the graphene edges depends on the graphene edge termination. Atom pairs (dimers) involving an armchair configuration tend to diffuse with a synchronized shuffling (step-wise shift) action, while dimer diffusion at zigzag edge terminations show a strong propensity to collapse the dimer with each atom diffusing in opposite directions (monomer formation). Moreover, the data reveals the role of C feedstock availability on the choice a single Sn atom makes in terms of graphene growth or etching. This study advances the understanding single atom catalytic activity at graphene edges. 相似文献
10.
《Ceramics International》2022,48(3):3609-3614
This work investigated the effect of replacing Zn2+ ions with Cd2+ ions on the microstructure and electromagnetic properties of NiZnCo ferrites. The studies show that the Cd2+ ions substituted for Zn2+ ions at the A sites (tetrahedral sites) of the ferrite lattice. The large ionic radius of the Cd2+ ions can cause lattice distortion. Concurrently, the low melting point of CdO can effectively reduce the sintering temperature of NiZnCo ferrite, thereby significantly changing the magnetoelectric properties of NiZnCo ferrite. These changes are mainly manifested as the decrease in the saturation magnetization (Ms) from 66.6 to 58.5 emu/g and the increase in coercivity (Hc) from 31.2 to 34.8 Oe. The dielectric constant increases considerably, dielectric loss tanδ gradually decreases from 4.71 to 0.83 at 10 kHz, and DC resistivity ρ decreases considerably from 8.0 × 104 to 1.61 × 104 Ω m. Therefore, the substitution of Cd2+ ions in NiZnCo ferrite provides excellent electrical and magnetic properties, which provide a reference for the development of high-frequency miniaturized electronic equipment. 相似文献