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1.
High-performance YBCO 123 (YBa2Cu3O7-x) bulk superconductor samples were produced using the 3D printing paste-extrusion technique. The YBCO powder obtained after sintering a pre-mixture of Y2O3, BaCO3 and CuO powders at 950 °C was used in the formulation of pastes for extrusion in a 3D freeform printer. The 3D samples printed from pastes containing the pre-mixture powders were sintered, while those produced using the YBCO powder were not. X-ray diffraction (XRD), energy dispersive spectroscopy (EDS) and Raman analysis all confirmed the YBCO phase after sintering, both in the powder and in the samples made with the pre-mixture. Scanning electron microscopy (SEM) images revealed powder grains of heterogeneous size and geometry, as well as grain aggregation, in the sintered samples. Superconducting quantum interference device (SQUID) measurements taken within a fixed magnetic range revealed that the printed pieces have a typical magnetization temperature of 92 K, reaching ?1.43 emu/g and ?1.59 emu/g respectively a zero-field-cooled magnetization (ZFC) for sintered and non-sintered printed samples.  相似文献   
2.
《Ceramics International》2021,47(18):25314-25323
This work is devoted to investigate the structural and electrical properties of the Ce, Gd-doped YBCO superconductors bulk ceramics. YBa2-xRExCu3O7−δ (x = 0, 0.01, 0.05, 0.1) (RE = Gd, Ce) samples were prepared by means of conventional solid-state reaction. X-ray diffraction analysis was carried out to identify the present phases in the as-prepared samples followed by the determination of their lattice parameters. Fourier Transform Infrared Spectroscopy (FTIR) was used to identify the functional groups. Furthermore, the morphology and the surface roughness of the studied samples were characterized using Scanning Electronic Microscopy (SEM) and Atomic Force Microscopy (AFM). Vickers Micro-hardness of the as-prepared samples was examined. Besides, the electrical resistivity measurements were achieved to determine the critical transition temperature TC and the critical current density JC.The effect of Ce and Gd additions is clearly noticed in the obtained results, where all the prepared samples are superconductors with the presence of Y123 as a major polycrystalline phase. From the XRD patterns, the intensities of the Y123 corresponding peaks decrease with further increasing the Ce and Gd contents. In addition, the variation of the cell parameters was significant after additions of both Ce and Gd, which affect the grain size and the oxygen content of the YBa2-xRExCu3O7−δ system. An improvement of the structure and surface roughness is observed on SEM and AFM images. Likewise, Vickers micro-hardness has increased after the Ce and Gd additions. Although, the critical transition temperature TC was not further increased upon Ce or Gd additions compared to the undoped YBCO samples. Nevertheless, an exception has been recorded with an increase of TC for YBa2-xRExCu3O7−δ with (RE = Gd, x=0.01) to reach 88 K. In contrary, an improvement of the deduced critical current density JC was achieved for all Ce-doped YBCO samples unlike those of Gd-doped samples.  相似文献   
3.
4.
YBa2Cu3O7-δ (YBCO) is a well-known high-temperature superconductor. However, its critical current density and thus maximum trapped magnetic field can be improved significantly by introducing the secondary phases (artificial pinning centers). In this contribution, we successfully prepared YBCO single-grain bulks with Y2Ba4CuWO10.8 phase serving as a source of pinning centers. This phase was prepared by solid-state reaction and further refined by milling. In the next step single-grain YBCO bulks with homogeneously distributed Y2Ba4CuWO10.8 were prepared by top-seeded melt growth. Precursors as well as the final product were characterized by XRD, SEM and EDS. The phase composition of YBCO bulks containing Y2Ba4CuWO10.8 was analyzed using Rietveld analysis. Thermal stability of YBCO bulk was studied by STA. Furthermore, PPMS was used to study electrical resistivity and critical current density. Bulk superconducting properties such as levitation force and trapped field ability were also measured.  相似文献   
5.
A corrosion process caused by reaction of surfaces of oxygenation cracks of YBCO bulk single‐grain superconductor with air moisture was studied. X‐ray photo‐emission spectroscopy, done on air exposed (001) surfaces, confirmed oxygen bonds related to barium hydroxide. Thermal analyses and mass spectrometry of exposed samples has shown a release of water caused by decomposition of barium hydroxide hydrates during sample heating. The sample weight increase versus time was related to formation of barium hydroxide phases at the surfaces of oxygenation cracks. The morphological changes of these phases at heating were observed with scanning electron microscope.  相似文献   
6.
《Ceramics International》2017,43(12):8845-8849
This paper describes the synthesis and characterization of YBa2Cu3O7−x (YBCO) nanoparticles obtained through an environmentally friendly chemistry approach. Y-, Cu- acetates and Ba trifluoroacetate were used for the synthesis of the precursor gel. Moreover, sucrose and pectin reagents were added as chelating agents inducing the formation of small size oxide nanoparticles. The thermal decomposition process of the precursor powder was investigated by thermal analysis correlated with mass spectrometry. The chemical nature, structure and morphology of the particles were investigated by X-Ray diffraction (XRD), Transmission Electron Microscopy (TEM) and Fourier Transform Infrared Spectroscopy. According to XRD analysis the nanoparticles have an orthorhombic structure and the average diameter between 18–30 nm, additionally confirmed by TEM measurements. The superparamagnetic behavior at room temperature of the YBCO nanoparticles has been clearly evidenced by magnetization measurements. Furthermore, the effect of the annealing atmosphere on the magnetic properties has been studied.  相似文献   
7.
冷绝缘高温超导电缆的导电层一般设计为多层结构以满足大电流载流特性,但伴随层数的增加,超导体上的集肤效应会引起电缆输电导体各层电流分布不均匀的问题,从而造成电缆损耗增加和传输性能下降。采用基于动态惯性权重因子的粒子群优化算法,提出了电缆导体层电流层间均流优化的设计方法。应用第2代高温超导材料钇钡铜氧涂层导体,通过建立超导电缆的等效电路模型,考虑电场、磁场等约束因素,对一根1km长,110kV/3kA等级的冷绝缘高温超导电缆进行优化设计,获得了电缆本体结构参数及输电导体层和屏蔽层的电流分布。比较优化前后层电流的结果可知,优化后超导电缆各导体层电流与平均电流相比最大不平衡率小于3.5%,各屏蔽层电流达到均布,较好地实现了电缆各导体层电流均匀分布的优化目标。最后,超导模型样缆载流特性实验也验证了优化设计方法的有效性。  相似文献   
8.
对一种制备YBCO薄膜的光辅助MOCVD反应器内的流动现象进行了三维数值模拟研究.在模拟计算中,分别改变基座与进口的相对角度(Φ)、反应器顶壁倾斜角度(Ψ),得出反应器中流场的相应变化.根据对模拟结果的分析,发现当基座平面与进气口轴线之间的夹角Φ=22.5°及反应器顶壁倾角ψ=30°时,基片表面气流速度大小合适,分布均...  相似文献   
9.
采用低氟溶胶-凝胶法在Φ76.2 mm的LaAlO3(LAO)单晶衬底上制备YBCO薄膜,然后对Φ76.2 mm的YBCO薄膜样品的微观结构、膜厚及超导性能进行均匀性测试分析.结果表明:所制备的薄膜厚度均匀并具有较好的c轴外延生长取向和均匀的超导电性能.  相似文献   
10.
为实现高温超导储能系统(SMES)对电网功率波动的动态补偿,采用第1代铋系和第2代钇钡铜氧高温超导材料,设计并构建了过冷液氮温区运行、千焦级容量的混合高温超导储能系统。应用数字信号处理器和微控制器的双处理器形式,设计了LCL滤波的电压型SMES变流器的功率控制系统电路,基于空间矢量脉冲调制法(SVPWM),提出了SMES变流器对系统功率补偿的控制方法,并进行控制软件编程,实现对并网侧功率的动态监测和补偿策略的实时计算。最后应用SMES在一条200km输电线路上进行并网动模试验,针对电网负荷变化产生的功率波动状态,实现了毫秒级内对电力系统的快速功率输出和波动抑制,验证了超导储能系统对电网瞬时功率补偿策略和功率补偿变流装置的有效性。  相似文献   
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