基准平面垂直断面法在爆破漏斗试验中的应用

系统阐述了基准平面垂直断面法在爆破漏斗试验中测量爆破漏斗体积的基本原理,并将隧道激光断面仪应用于金厂河矿1 750 m水平15^#采场底部切割巷道爆破漏斗试验爆破漏斗体积测量中。通过与传统体重法等计算法所得漏斗体积分析比较,结果表明基于隧道激光断面仪与3D Mine软件分析的基准平面垂直断面法实用性强、操作方便、结果直观可靠,达到试验预期目的。     

Effect of ligand environment of rare-earth ions on temperature measurement performance of SrAO4:xEu3+ (A = Mo and W) phosphors

Molybdate and tungstate with scheelite-type structure are excellent self-luminescent materials, which can be used as ideal hosts for the doping of rare-earth ions. In this study, a series of Eu³⁺-activated SrAO₄ (A = Mo and W) phosphors were successfully synthesized, and their crystal structures, photoluminescence properties, and temperature measurement performance were analyzed in detail. These phosphors were excited by UV light (291 nm and 247 nm, respectively), with clear energy transfer (ET) (MoO₄^2?→Eu³⁺ or WO₄^2?→Eu³⁺). According to fluorescence intensity ratio (FIR) and Judd–Ofelt (J–O) theory, compared to SrWO₄:0.01Eu³⁺ phosphor, SrMoO₄:0.01Eu³⁺ phosphor exhibited better thermal stability, with relatively low Sa value (maximum values were 5.082 %K^?1 and 20.74 %K^?1, respectively), and their Sr values were not significantly different (maximum values were 0.864 %K^?1 and 0.83 %K^?1, respectively). Sa value was negatively correlated to central asymmetry of Eu³⁺, but the optimal Sr value tended to be more suitable for central asymmetry of Eu³⁺. In addition, Eu³⁺ exhibited stronger central asymmetry as well as covalency of Eu–O bond in SrMoO₄. Results reveal that SrMoO₄:xEu³⁺ and SrWO₄:xEu³⁺ can be used for luminescent thermometers.     

倾斜入射下的单截面平面度绝对检验

针对大尺寸光学平面的直线度的纳米级测量精度需求，提出了倾斜入射下单截面平面度绝对检验方法，实现了对超过相移干涉仪口径的长平晶绝对检验。利用棱镜转向实现倾斜入射角度的精密预标定，棱镜标定角度的精度高于圆光栅和图像分析等方法，可提高测量不确定度到0.0042 μm。对比了常规三面互检绝对检验结果与本方法的差异，在相同尺寸下，直线度误差仅为1.2 nm。在确认标定反射镜位置后，整个倾斜入射的干涉图调整过程将被完全集中到待测长平晶的工作面上，不需要再对反射平晶进行操作。调整长平晶时各个维度的操作互不干涉，可快速简便地得到测量结果。     

Generation,validation and application of dynamic load profiles in flow measurement using cavitating Herschel–Venturi nozzles

Today, utility meters for water are tested for measurement behavior at stable operating conditions at specified flow rates as part of the approval process. The measurement error that occurs during start and stop or when changing between flow rates may not be taken into account. In addition, there are new technologies whose measuring behavior under real-world conditions is only known to a limited extend. To take these facts into account, a new method has been developed and tested to determine the measurement behavior of water meters under dynamic load profiles as they occur in the real application. For this purpose, a test rig for flow rate measurement was extended by a cavitation nozzle apparatus and the generation of dynamic load profiles was validated. For the cavitation nozzles used, possible factors influencing the flow rate, such as temperature and purity of the water as well as the upstream pressure were investigated. Using different types of domestic water meters, the applicability of the dynamic test procedure was demonstrated and the measurement behavior of the meters was characterised.     

Pu同位素的AMS测量方法研究进展

锕系超铀元素Pu主要来自于各类人工核活动，现广泛存在于自然界中。其在多个基础研究及应用领域具有重要研究和使用价值，并已得到广泛应用。本文比较了目前Pu的主要测量方法，对各种方法的优缺点加以分析。在所有Pu的测量方法中，加速器质谱（AMS）方法具有样品用量小、测量时间短、能区分²³⁹Pu与²⁴⁰Pu，同时探测限低等优点，是从技术上最适合于测量超痕量Pu的方法。国外已有澳大利亚、奥地利、瑞士等多个国家的实验室基于各自的AMS系统设备参数建立了不同的AMS测量Pu的方法。本文对国外已建立的AMS测量Pu的方法进行介绍和总结，对中国原子能科学研究院（CIAE）现已开展的相关研究作了介绍。CIAE基于350 kV AMS系统建立的Pu测量方法探测限达到1×10⁶原子。     

Compressive thermal stress and microstructure-driven charge carrier transport in silicon oxycarbide thin films

This work correlates the charge carrier transport mechanism of silicon oxycarbide-based thin films with their morphology and thermal stress. Segregation of highly-graphitized carbon-rich, oxygen-depleted C/SiC areas homogeneously dispersed within an oxygen-rich C/SiOC matrix was seen on the 500 nm-SiOC thin films. Compressive biaxial stress induced by the mismatch with the Si-substrate thermal expansion coefficient was calculated at 109 MPa. Through Hall measurements, p-type carriers were shown dominating the SiOC film similar to monolithic samples. Thin films and monoliths have comparable carrier concentrations while the carrier mobility in SiOC thin films was 2 magnitudes higher than that of monolithic samples and is considered a consequence of the compressive thermal stress acting on the film. Improved conductivity of 16 S cm -1 is measured for the SiOC thin film sample which is assumed considering the enhanced carrier mobility alongside the reduced percolation threshold ascribed to the phase-separated morphology of the thin film.     

食品包装高精度计量控制方法

目的 为提高食品包装过程计量组件的称量精度和效率,采用智能控制算法设计一种高精度计量控制系统.方法 在分析动态称量系统工作原理的基础上,建立称量过程数学模型,将控制对象由放料阀门开度转换为电机轴位置.考虑到传统PID控制的缺陷,结合PI Ziegler-Nichols和预测控制设计一种高精度计量控制系统.该控制系统可实现比例和积分系数的在线调整,能够抑制参数变化、负载扰动;预测控制可提高系统收敛速度和跟踪能力.最后进行仿真和实验研究.结果 仿真结果表明,智能控制算法具有比较强的自适应、自整定能力,计量精度可以达到静态称量水平,均高于99.5％.结论 食品包装高精度计量控制系统具有精度高、稳定性好、称量效率高等特点,在实际应用中对称量过程的控制效果相对较好.     

Design and fabrication of a full elastic sub-micron-Newton scale thrust measurement system for plasma micro thrusters

In this work,a force measurement system is proposed to measure the thrust of plasma micro-thruster with thrust magnitude ranging from sub-micro-Newtons to hundreds micro-Newtons.The thrust measurement system uses an elastic torsional pendulum structure with a capacitance sensor to measure the displacement,which can reflect the position change caused by the applied force perpendicular to the pendulum axis.In the open-loop mode,the steady-state thrust or the impulse of the plasma micro-thruster can be obtained from the swing of the pendulum,and in the closed-loop mode the steady-state thrust can be obtained from the feedback force that keeps the pendulum at a specific position.The thrust respond of the system was calibrated using an electrostatic weak force generation device.Experimental results show that the system can measure a thrust range from 0 to 200 μN in both open-loop mode and closed-loop mode with a thrust resolution of 0.1 μN,and the system can response to a pulse bit at the magnitude of 0.1 μN s generated by a micro cathode arc thruster.The background noise of the closed-loop mode is lower than that of the open-loop mode,both less than 0.1 μN//√Hz in the range of 10 mHz to 5 Hz.     

放射性检测领域的能力验证

放射性检测领域长期以来没有能力验证提供者,从事放射性检测工作的人员对实验室间比对和能力验证的认识不够深入。能力验证的关键过程包括能力验证物品的制备及其均匀性和稳定性检验、包装及分发、参加者结果的评定等内容。其中参加者结果的评定可参考IAEA的评定方法,更为全面可靠。