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排序方式: 共有822条查询结果,搜索用时 16 毫秒
1.
Yang Luo Shi-li Zheng Shu-hua Ma Chun-li Liu Xiao-hui Wang 《Journal of the European Ceramic Society》2018,38(16):5282-5293
A novel mullite-bonded SiC-whisker-reinforced SiC matrix composite (SiCw/SiC, SiC whisker-to-SiC powder mass ratio of 1:9) was designed and successfully prepared. Before preparing the composite, the inexpensive lab-made SiCw was first modified by an oxidation/leaching process and then coated with Al2O3. The kinetics results indicate that the oxidation process can be described by improved shrinking-cylinder models. The aspect ratio of SiCw improved after modification. Subsequently, raw materials with a SiC–SiO2–Al2O3 triple-layered structure were obtained after the Al2O3-coating process and used as feedstocks during the subsequent hot-pressing sintering. Finally, the characterization of the composites indicates that the mullite-bonded sample performs better (relative density of 93.8?±?1.4%, flexural strength of 533.3?±?18.2?MPa, fracture toughness of 13.6?±?2.1?MPa?m1/2, and Vickers hardness of 20.6?±?2.5?GPa) than the reference sample without the mullite interface. The improved toughness could essentially be attributed to the moderately strong interface bonding and effective load transfer effects of the mullite interface. 相似文献
2.
为克服迭代最近点(ICP)算法易陷入局部最优的缺陷,提出一种基于线特征及ICP算法的地基建筑物点云自动配准方法。首先,基于法向一致性进行建筑物点云平面分割;接着,采用alpha-shape算法进行点簇轮廓线提取,并拆分和拟合处理得到特征线段;然后,以线对作为配准基元,以线对夹角和距离作为相似性测度进行同名特征匹配,实现建筑物点云的粗配准;最后,以粗配准结果为初值,进一步采用ICP算法完成点云精确配准。利用两组部分重叠的建筑物点云进行配准实验,实验结果表明,采用由粗到精的配准方法能有效改善ICP算法对初值依赖的问题,实现具有部分重叠的建筑物点云的有效配准。 相似文献
3.
Determination of changes in the concentration and distribution of elements within olive drupes (cv. Leccino) from Se biofortified plants,using laser ablation inductively coupled plasma mass spectrometry 下载免费PDF全文
4.
通过微电子机械技术(MEMS)在抛光的熔融石英基材表面制作了平面精度达到0.4μm的超大单片面积的全息透镜。采用了分辨率达到0.2μm的步进投影式拼接光刻,适合石英基材的专用等离子耦合刻蚀(ICP)干法刻蚀技术,特殊的物理清洗方法,以及相关的多项辅助工艺。透镜理想面形横截面曲线为分段抛物线,每一片由23个柱状结构单元周期横向排列构成,采用等深度不等宽度的4台阶结构拟合,单元宽度约为2.966mm。在4in(10.16cm)圆片上,获得了单片尺寸为68mm×68mm的方形透镜。采用接触式台阶仪,扫描电子显微镜(SEM),高倍光学显微镜等方法进行不同阶段检测。结果显示:台阶平面精度为0.4μm,垂直精度为30nm,有非常好的立墙陡直度和刻蚀均匀性。此工艺方案可实现小规模批量生产,成本适中,可以直接用于制作6in(15.24cm)以上同等级要求的石英透镜,经适当改进也可用于蓝宝石等基底材料的制作。 相似文献
5.
6.
微波消解—电感耦合等离子体质谱法测定膨化食品中铝 总被引:1,自引:0,他引:1
建立了微波消解—电感耦合等离子体质谱法测定膨化食品中铝的方法。采用微波消解法处理膨化食品,利用内标元素补偿基体效应,结合动态反应池技术消除质谱干扰,进行电感耦合等离子体质谱分析。在优化的实验条件下,铝元素在0.1~1.0 mg/L的浓度范围内呈良好线性关系,相关系数r=0.999 7,检出限为0.023 mg/L(n=11),加标回收率为90.8%~103.0%,相对标准偏差为0.4%~3.2%。本方法具有快速、简单、准确、灵敏度高等特点,适合膨化食品中铝的测定。 相似文献
7.
Differing cytotoxicity and bioavailability of selenite,methylselenocysteine, selenomethionine,selenosugar 1 and trimethylselenonium ion and their underlying metabolic transformations in human cells 下载免费PDF全文
8.
Over the past several decades, the technology of micro-electromechanical system (MEMS) has advanced. A clear need of miniaturization and integration of electronics components has had new solutions for the next generation of wireless communications. The aluminum nitride (AlN) MEMS contour-mode resonator (CMR) has emerged and become promising and competitive due to the advantages of the small size, high quality factor and frequency, low resistance, compatibility with integrated circuit (IC) technology, and the ability of integrating multi-frequency devices on a single chip. In this article, a comprehensive review of AlN MEMS CMR technology will be presented, including its basic working principle, main structures, fabrication processes, and methods of performance optimization. Among these, the deposition and etching process of the AlN film will be specially emphasized and recent advances in various performance optimization methods of the CMR will be given through specific examples which are mainly focused on temperature compensation and reducing anchor losses. This review will conclude with an assessment of the challenges and future trends of the CMR. 相似文献
9.
《中国工程学刊》2012,35(1):101-113
Changes of the cartilage morphology over time can tell the progression of osteoarthritis (OA) and show particular promise for evaluating the efficacy of disease-modifying OA drugs. Hence, cartilage matching is required prior to cartilage morphology comparison. An accurate cartilage matching allows one to ensure longitudinal focal and local changes of cartilage morphology due to OA. The method described in this article meets this need. The proposed method consists of three steps. First, the knee femur surfaces are aligned, using the principal axes transformation to correct for different knee joint positions and orientations in the magnetic resonance (MR) scanner. Second, we present a global registration algorithm based on Lipschitz optimization theory for accurately identifying the corresponding points of the knee femur surface. Third, the rigid transformation of the knee femur surface registration is applied to the cartilage surface. Our registration algorithm is efficient and robust, and its performance is evaluated on MR images of pig knees. 相似文献
10.
Daniela Drescher Ingrid Zeise Heike Traub Peter Guttmann Stephan Seifert Tina Büchner Norbert Jakubowski Gerd Schneider Janina Kneipp 《Advanced functional materials》2014,24(24):3765-3775
By adding a gold core to silica nanoparticles (BrightSilica), silica‐like nanoparticles are generated that, unlike unmodified silica nanoparticles, provide three types of complementary information to investigate the silica nano‐biointeraction inside eukaryotic cells in situ. Firstly, organic molecules in proximity of and penetrating into the silica shell in live cells are monitored by surface‐enhanced Raman scattering (SERS). The SERS data show interaction of the hybrid silica particles with tyrosine, cysteine and phenylalanine side chains of adsorbed proteins. Composition of the biomolecular corona of BrightSilica nanoparticles differs in fibroblast and macrophage cells. Secondly, quantification of the BrightSilica nanoparticles using laser ablation inductively coupled plasma mass spectrometry (LA‐ICP‐MS) micromapping indicates a different interaction of silica nanoparticles compared to gold nanoparticles under the same experimental conditions. Thirdly, the metal cores allow the investigation of particle distribution and interaction in the cellular ultrastructure by cryo nanoscale X‐ray tomography (cryo‐XT). In 3D reconstructions the assumption is confirmed that BrightSilica nanoparticles enter cells by an endocytotic mechanism. The high SERS intensities are explained by the beneficial plasmonic properties due to agglomeration of BrightSilica. The results have implications for the development of multi‐modal qualitative and quantitative characterization in comparative nanotoxicology and bionanotechnology. 相似文献