非常规气藏储层改造体积评价方法研究

为精确描述非常规气藏压裂后的复杂流动特征及定量评价储层改造体积（SRV），利用自主研发的缝网重构算法“破裂树生长法”建立压后缝网模型，并以此为基础提出了使用拟稳态流动时特定的压力等值线来确定SRV范围的定量评价方法，最后以长宁201井区为例进行了矿场实例分析。该方法根据微地震监测点的位置，重构出微裂缝网的连通关系。在复杂微裂缝网的基础上建立离散裂缝地质模型并进行生产数值模拟，根据数值模拟结果的压力分布精确划定SRV的范围。利用该方法计算出长宁201井区的SRV体积为0.052 1 km3，以该缝网模型的数值模拟产量预测结果符合实际生产规律，方法实用性较好。     

煤峪口矿81010工作面煤层底板裂隙发育特征及防治

针对煤炭开采过程中出现的突水事故,采用RFPA数值模拟软件建立采动模型,对底板裂隙破断过程和声发射进行模拟,研究煤层底板采动裂隙扩展突水通道,结果表明:离断层越近,断层内水压导升高度越高,断层出现活化,裂隙扩展发育,最终贯通形成导水通道,在进行注浆改造后,单个钻孔的最大涌水量为8 m³/h,说明注浆加固防治水效果较好,能确保工作面的安全回采。     

Dense and core-rim structured B4C-TiB2 ceramics with Mo-Co-WC additive

B₄C-TiB₂ ceramics (TiB₂ ranging 5~70 vol%) with Mo-Co-WC as the sintering additive were prepared by spark plasma sintering. In comparison with B₄C-TiB₂ without additive, the enhanced densification was evident in the sintered specimen with Mo-Co-WC additive. Core-rim structured grain was observed around TiB₂ grains. The interface of the rim between TiB₂ and B₄C phases demonstrated different feature: the inner borderline of the rim exhibited a smooth feature, whereas a sharp curved grain boundary was observed between the rim and the B₄C grain. The formation mechanism is discussed: the epitaxial growth of (Ti,Mo,W)B₂ rim around the TiB₂ core may occur as a result of the solid solution and dissolution-precipitation between TiB₂ phase and the sintering additive. It was revealed that the fracture toughness increased as the content of TiB₂ content increased, alongside the decreased hardness. B₄C-30 vol% TiB₂ specimen demonstrated the optimal combination of mechanical properties, reaching Vickers hardness of 24.3 GPa and fracture toughness of 3.33 MPa·m^1/2.     

丙烯酸装置循环气压缩机叶片损伤分析与修复

某石化公司丙烯酸装置循环气压缩机在运行过程中,一级叶片突然发生断裂,导致机组停机。采用宏观检查、扫描电子显微镜、能谱分析等方法对断裂叶片进行检验和检测,将断裂叶片的材质、裂纹及断口特征检测结果与疲劳断裂特征和机组运行状况进行对比,确定压缩机叶片的断裂系其达到疲劳寿命所致,提出采用激光熔覆方法对压缩机叶片进行修复,介绍了修复工艺操作程序要点,可为同类故事的处理提供参考。     

矿用直线振动筛结构故障分析

针对煤矿选煤厂直线振动筛工作过程中出现的结构故障问题,采用有限元仿真与现场测试结合的方法对振动筛出现故障的原因进行了分析研究。介绍了振动筛的主要结构及常见故障,并以某矿选煤厂发生大梁断裂的振动筛为例,对该振动筛进行三维建模和有限元模态分析,分析结果表明:随着模态阶次的增加,振型的变化逐渐由移动转为结构本身的扭曲变形。在该振动筛空载工作状态下,选用本质安全型便携式测振记录仪进行振动测试并处理测试信号,得到该振动筛的工作频率。结合模态分析结果和实际测试结果,判断出空载时频繁运行振动筛是造成其大梁断裂的主要原因。根据故障原因给出维护建议:应当尽量避免振动筛在空载或物料较少的状态下长时间运行;在振动筛投入使用前,应预先了解振动筛的工作状态及可能存在的薄弱环节,尽可能避免结构故障,保证振动筛可靠运行。     

不同脆性致密砂岩裂缝扩展规律实验

岩石的脆性与致密油气储集层压裂改造效果密切相关,但致密岩石的脆性对裂缝扩展规律的影响仍不明确。基于真三轴压裂模拟实验系统,对鄂尔多斯盆地东部3种不同脆性致密砂岩开展了压裂模拟实验,分析了脆性、压裂液类型和层理对裂缝扩展规律的影响。研究表明,山1段致密砂岩脆性最强,长7段致密砂岩次之,盒8段致密砂岩脆性最弱;在层理不发育的条件下,相比于中等脆性的盒8段致密砂岩,强脆性的山1段致密砂岩采用滑溜水压裂形成的单条裂缝扩展更充分,液态CO₂压裂形成的分支裂缝数量更多;在层理发育的条件下,长7段致密砂岩采用滑溜水压裂和液态CO₂压裂形成的裂缝的形态均较复杂;相比于滑溜水压裂,液态CO₂压裂形成的裂缝宽度更小;液态CO₂压裂更适用于脆性较强、层理发育的长7段致密砂岩储集层压裂改造。     

PA6B柴油机进排气阀断裂原因分析

针对PA6B柴油机进排气阀断裂故障,根据现场勘验情况并结合该柴油机当时的热工参数,建立相应的故障树;对制造质量、装配质量、配气定时、异物进入、热工参数等因素进行逐一排查。结果表明:导致PA6B柴油机进排气阀断裂的原因为喷油器制造质量存在问题。     

砂砾岩含水层下综放开采导水裂隙演化及防治水措施

以伊犁矿区第三系砂砾岩含水层下综放开采为工程背景，利用相似模拟实验研究了采动引起覆岩的破断特征。结果表明，工作面推进到135 m左右，裂隙带即与砂砾岩含水层贯通，这对于6-7煤层安全高效开采造成较大威胁。为了保障工作面回采安全，设计了超前探放水钻孔，累计泄水量344 800 m³，大幅度减少了对粗砂岩流砂层的补给作用；对首采综放工作面现场观测表明，垮落到采空区的粗砂岩流砂层成为湿润的固体砂，固体砂覆盖于采空区又起到防灭火的作用，对矿井安全生产十分有利。     

Inhibition of stress corrosion cracking in 304 stainless steel through titanium ion implantation

The effects of titanium ion implantation on the stress corrosion cracking (SCC) behaviour of 304 austenitic stainless steel were studied. Slow strain rate tests (SSRTs) were conducted on 304 steel in air and in 5?wt-% NaCl solution. The microscopic effects of ion implantation were evaluated by Stopping and Range of Ions in Matter Procedures (SRIM). Fracture morphologies and microstructures were investigated by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The fracture surfaces illustrate that ion implantation significantly inhibits the corrosion pits that initiate SCC. A dense passive film, which inhibits SCC, was formed during the ion implantation process. SCC initiation was restrained due to the dense dislocation nets that were generated by titanium ion implantation.

Highlights

• Ion implantation inhibits SCC susceptibility.

• The lack of Cr at the grain boundary leads to the expansion of SCC along the grain boundary.

• Implantation-induced damage leads to high-density dislocations.

• The surface was amorphised due to high-density dislocations.

     

Microstructure−fracture toughness relationships and toughening mechanism of TC21 titanium alloy with lamellar microstructure

The independent influence of microstructural features on fracture toughness of TC21 alloy with lamellar microstructure was investigated. Triple heat treatments were designed to obtain lamellar microstructures with different parameters, which were characterized by OM and SEM. The size and content of α plates were mainly determined by cooling rate from single β phase field and solution temperature in two-phase field; while the precipitation behavior of secondary α platelets was dominantly controlled by aging temperature in two-phase field. The content and thickness of α plates and the thickness of secondary α platelets were important microstructural features influencing the fracture toughness. Both increasing the content of α plates and thickening α plates (or secondary α platelets) could enhance the fracture toughness of TC21 alloy. Based on energy consumption by the plastic zone of crack tip in α plates, a toughening mechanism for titanium alloys was proposed.