Hydrothermal synthesis of SrF2：yb^3＋/Er^3＋ micro-/nanocrystals with multiform morphologies and upconversion properties

Micro-and nanocrystals cubic-phase SrF2:Yb3+/Er3+ upconversion luminescence phosphors were synthesized via a facile hydro-thermal route in the presence of different surfactants.The samples were characterized with X-ray diffraction (XRD),Fourier transform infra-red spectra (FT-IR),scanning electron microscopy (SEM),transmission electron microscopy (TEM),and upconversion emission spectra.As-prepared products showed a variety of morphologies,such as cubic-shaped microcrystal,hierarchical structure microspheres...     

Luminescence properties of a new red emitting Eu~(3+)-doped alkaline-earth fluoborate phosphor: BaCa_(1-2x)BO_3F:xEu~(3+), xM~+ (M=Li, Na, K)

A series of new red-emitting BaCa1-2xBO3F:xEu3+, xM+ (M=Li, Na, K) phosphors were synthesized by the solid-reaction method. X-ray diffraction (XRD), diffuse reflection (UV-vis) and photoluminescence spectra were utilized to characterize the crystallization process, structure and luminescence properties of the as-synthesized phosphors. The XRD results indicated that the sample began to crystallize at 800 oC, and single-phase BaCaBO3F was fully obtained after annealing at 1000 oC. The charge compensated behav...     

闪蒸法聚乙烯无纺布的研究进展

介绍了无纺布的发展历程以及我国无纺布的现状，着重讨论了开展闪蒸法聚乙烯纺粘型无纺布研究的意义、方法、生产工艺。     

无机片状微晶对化学光源发光效率的影响研究

以双（2,4,5-三氯-6-正丁烷氧羰基苯基）草酸酯（简称CPPO）和红色荧光剂罗丹明B组成的过氧草酸酯类化学发光体系为研究对象,从粒径、用量和种类的角度讨论了分散剂云母等对体系发光效率的影响．结果表明,添加30μm云母50mg后,体系的发光寿命、强度均显著增加,发光效率较高。     

不球磨无机粉体发光材料制备技术进展

综述了不球磨无机粉体发光材料制备技术进展，着重总结了稀土掺杂型无机粉体发光材料的制备方法。介绍了溶胶-凝胶法，燃烧合成法，微波合成法，共沉淀法，喷雾热解法，水热合成法，气相反应合成法和微乳液法等制备方法。对比总结了每种合成方法的优缺点，并对其未来发展趋势作了展望。综述国内外研究报告和论文82篇。     

无机粉体材料表面包膜研究与应用

综述了表面包膜技术在发光材料、纳米材料、珠光颜料等无机粉体材料中的研究进展。主要介绍了表面包覆无机物的研究现状 ,简要介绍了各种应用中的制备工艺 ,分析比较了各种制备工艺的优缺点及适用范围     

煤的芳烃化学研究进展

当世界上的石油资源逐渐枯竭之后，煤能否成为２１世纪化学工业的原材料？科学家们正面临极富感染力的挑战，即寻找和发展一条利用液化煤中的芳烃化合物合成有机化学品的新途径。近期研究表明，新兴的煤化学工业具有很大的发展潜力。本文主要讨论和介绍煤的非燃料利用问题，研究发展由煤制取芳烃化学品和材料的可能途径。综述有关文献２６篇。     

Spectral Characteristic and Its Regularity of Rare Earth Ions in Inorganic Microporous Material Ⅰ.The Spectral Characteristics of Eu~(3 ) in NaY,NaX and NaA Zeolites

In this paper,we have investigated the spectral characteristics of Eu~(3 )ion sorbed on NaY,NaX and NaAzeolites.During calcination,the influence of Eu~(3 )ion's positions in zeolites on its spectral structures are dis-cussed emphatically.The experimental results show that the electric dipole-to-magnetic dipole transition inten-sity ratios of Eu~(3 )emission in NaY,NaX and NaA zeolites calcinated at the same temperature increase inproper order.The bonding actions between Eu~(3 )ion and framework oxygens are studied by the measurementsof excitation spectra and X-ray photoelectron spectroscopy.In the Eu~(3 )content ranging from 0.95% to10.5%,the concentration quenching of the fluorescence in Eu(Ⅲ)-NaY is not observed.     

表面包覆制备云母系珠光颜料研究现状

介绍了天然白云母表面包覆金属氧化物、非金属氧化物、稀土氧化物和有机颜料或染料等制备云母系珠光颜料的研究现状