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1.
Ram Bilas 《Bulletin of Materials Science》1993,16(2):109-116
X-ray diffraction, electron paramagnetic resonance, microwave absorption and resistivity measurements were carried out on
YBa2−x
Bi
x
Cu3O7 (0≤x≤0·5) superconductors in order to study the effect of bismuth on the structural and superconducting properties. A decrease
in sintering temperature increased the amount of impurity phase. Transition from an orthorhombic (superconducting) phase to
tetragonal structure produced no significant change in EPR zero-field signal at liquid nitrogen temperature (LNT). The non-resonance
signal height decreased on higher concentration of bismuth. Sintered YBa2−x
Bi
x
Cu3O7 superconductor had a strong EPR zero-field signal at LNT. We have evaluated particle size from XRD and EPR studies. The average
particle size was about 0·4μm. 相似文献
2.
叙述了从铅阳极泥回收金银后的渣料中综合回收有价金属的生产实践。根据渣料性质,将火法和湿法工艺相互结合,使渣料中的锑、铋、金、银、铅、铜得以较彻底的分离和回收。 相似文献
3.
Control over crystallographic orientation in ceramic thin films is important for highly anisotropic structures. Layered perovskites, like Bi4 Ti3 O12 , have interesting properties associated with their ferroelectric nature, which may be fully exploited only when films are highly textured. Textured films of this titanate were fabricated via a sol–gel technique without using epitaxial growth. Orientation in the film is confirmed by XRD and SEM, and supported by refractive index and dielectric measurements. In an attempt to explain the orienting effect, light scattering experiments were conducted to yield information about the molecular size, shape, and conformation of macromolecules as the sol–gel solution ages and condensation reactions proceed. These experiments clearly show an increase in the size of molecular clusters with time. We believe that it is the organization of these large clusters during spin coating, and the relationship of the backbone chemistry to the crystal structure of Bi4 Ti3 O12 , that are responsible for the observed orientation. 相似文献
4.
从铅阳极泥中回收铋的火法工艺实践 总被引:4,自引:2,他引:2
主要论述了从铅阳极泥中回收铋的全火法工艺流程改造与实践,并取得了预期的效果。 相似文献
5.
(反应)模晶生长法制备NBT-6BT织构陶瓷的研究 总被引:1,自引:0,他引:1
以熔盐法合成的片状SrTiO3,Bi4Ti3O12为种晶,分别采用模晶生长法(TGG)和反应模晶生长发(RTGG)制备了具有〈001〉取向的0.94(Na1/2Bi1/2)TiO3-0.06BaTiO3(NBT-6BT)织构陶瓷。研究了不同种晶选择、流延和热处理工艺参数对陶瓷织构化程度、显微结构和压电性能的影响。结果表明,RTGG制备的织构陶瓷比TGG的在结构和性能等方面都具有优势,且用该方法以Bi4Ti3O12为种晶,制备出了高密度(f≥96%)、高织构度(F≈95%)、高性能(d33≈241pC/N)的NBT-6BT无铅压电陶瓷。 相似文献
6.
Toshio Kimura Toru Takahashi Toshihiko Tani Yasuyoshi Saito 《Journal of the American Ceramic Society》2004,87(8):1424-1429
Bi0.5 Na0.5 TiO3 (BNT) and 0.94Bi0.5 Na0.5 TiO3 ·0.06BaTiO3 (BNT–BT) bulk ceramics with extensive 〈100〉 texture were prepared by the reactive-templated grain growth method, using platelike Bi4 Ti3 O12 (BIT) particles as templates for BNT. Calcined compacts were composed of matrix grains with random orientation and 〈100〉-oriented grains transformed from aligned BIT particles, and the texture developed by the growth of oriented grains during sintering. Ceramics with extensive texture were obtained by using the starting mixture containing the maximum concentration of platelike BIT to form the maximum volume fraction of oriented grains. 相似文献
7.
8.
用DSC研究了高T_e超导体B_(2-r)Pb_rSr_2Ca_2Cu_sO_v(x=0,0.2,0.4,0.6)从室温至600℃范围内的相变。在320℃和440℃附近有二个吸热蜂,每一个峰对应一个相变过程。440℃附近的相变是不可递的,其原子激活能为1.37eV,是由高T_e相向低T_e相的转变。而320℃附近的相变则与超结构的形成有关。 相似文献
9.
Mohammad A. Alim 《Journal of the American Ceramic Society》1989,72(1):28-32
The lumped parameter/complex plane analysis technique revealed several contributions to the terminal admittance of the ZnO—Bi2 O3 based varistor grain-boundary ac response. The terminal capacitance has been elucidated via the multiple trapping phenomena, a barrier layer polarization, and a resonance effect in the frequency range 10−2 ≤ f ≤ 109 Hz. The characterization of the trapping relaxation behavior near ∼ 105 Hz (∼ 10−6 s) provided a better understanding of a previously reported loss-peak. The possible nonuniformity in this trapping activity associated with its conductance term observed via the depression angle of a semicircular relaxation in the complex capacitance ( C *) plane has been postulated. 相似文献
10.
共沉淀法制备Bi3.25La0.75Ti3O12纳米粉体 总被引:1,自引:1,他引:1
用硝酸铋、硝酸镧和钛酸四丁酯为原料,硝酸、无水乙醇和去离子水为溶剂,氨水为沉淀剂,采用共沉淀法合成了单相铋层状钙钛矿结构Bi3.25La0.75Ti3O12(BLT)纳米粉体。用DTA/TG和XRD研究了BLT前驱体的热行为和晶相转化过程,用场致发射扫描电子显微镜观察了BLT粉体的颗粒形貌和大小的变化。结果表明:共沉淀前驱体溶液的配制过程中,硝酸铋水解生成的硝酸氧铋不利于层状钙钛矿结构BLT相的合成。利用浓度较高的硝酸作溶剂,可以防止硝酸铋的水解,采用氨基共沉淀法直接合成出了单一相的BLT纳米粉体,在煅烧过程中,未出现Bi2Ti2O3焦绿石相。700℃煅烧2h合成的BLT粉体颗粒不大于100nm,颗粒间结合疏松,具有良好的分散性。 相似文献