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1.
《Ceramics International》2021,47(24):34845-34850
The interfacial delamination of electrode/ceramic multilayer structure will seriously damage the reliability of low temperature co-fired ceramic (LTCC) module in practical applications. In this work, three kinds of glasses employed in Au electrode are designed and prepared to study the abnormal expansion and delamination process in the Au/ceramic LTCC multilayer structure. The interfacial delamination in the co-fired structure is found to be attributed to the abnormal expansion of glass in respect to Au electrode at high temperature, which is originated from the enlarged closed pores during the co-firing process. This conclusion is further confirmed by co-firing the sample in a low-pressure condition. The mechanism and elimination of interfacial delamination here provides a feasible solution for the design of novel glasses in Au electrode for LTCC applications. 相似文献
2.
Minsu Kang Jooyong Lee Sangyoon Ko Dr. Sang-Hee Shim 《Chembiochem : a European journal of chemical biology》2021,22(8):1396-1399
Expansion microscopy combined with single-molecule localization microscopy (ExSMLM) has a potential for approaching molecular resolution. However, ExSMLM faces multiple challenges such as loss of fluorophores and proteins during polymerization, digestion or denaturation, and an increase in linkage error arising from the distance between the fluorophore and the target molecule. Here, we introduce a trifunctional streptavidin to link the target, fluorophore and gel matrix via a biotinylizable peptide tag. The resultant ExSMLM images of vimentin filaments demonstrated high labeling efficiency and a minimal linkage error of ∼5 nm. Our ExSMLM provides a simple and practical means for fluorescence imaging with molecular resolution. 相似文献
3.
《Ceramics International》2022,48(8):10733-10740
Multivalent ion-conducting ceramics are required for the manufacture of high-safety, high-capacity rechargeable batteries. However, the low ionic conductivity of solid electrolytes and discrepancies in the thermal expansion between the battery components limit their widespread application. Furthermore, anisotropic thermal expansion in crystals during battery manufacturing and the charge-discharge cycles causes the formation of microcracks, which degrade the battery performance. The physical properties of ceramic materials with anisotropic crystal structures can be modified by varying the crystallographic orientation of their grains. In this study, a co-precipitation approach was used to synthesize an Mg2+-conducting (Mg0.1Hf0.9)4/3.8Nb(PO4)3 solid electrolyte, and the grain orientation in the bulk sample was controlled using strong magnetic fields during the slip casting process. The results showed that inducing an orientation along the c-axis enhanced the apparent ionic conductivity of the bulk sample. It was also observed that (Mg0.1Hf0.9)4/3.8Nb(PO4)3 crystal has a negative volumetric thermal expansion despite a positive linear thermal expansion along its c-axis. By adjusting the c-axis orientation of the grains, (Mg0.1Hf0.9)4/3.8Nb(PO4)3 electrolytes with negative or positive linear thermal expansion coefficient have been produced. The findings of this study suggest that solid-electrolytes with negative, positive, or zero linear thermal expansion can be produced to create more compatible and higher-performance solid-state devices. 相似文献
4.
针对煤炭开采过程中出现的突水事故,采用RFPA数值模拟软件建立采动模型,对底板裂隙破断过程和声发射进行模拟,研究煤层底板采动裂隙扩展突水通道,结果表明:离断层越近,断层内水压导升高度越高,断层出现活化,裂隙扩展发育,最终贯通形成导水通道,在进行注浆改造后,单个钻孔的最大涌水量为8 m3/h,说明注浆加固防治水效果较好,能确保工作面的安全回采。 相似文献
5.
《Ceramics International》2022,48(1):548-555
Silica-based ceramic cores are widely utilized for shaping the internal cooling canals of single crystal superalloy turbine blades. The thermal expansion behavior, creep resistance, and high temperature flexural strength are critical for the quality of turbine blades. In this study, the influence of zircon, particle size distribution, and sintering temperature on the high-temperature performance of silica-based ceramic cores were investigated. The results show that zircon is beneficial for narrowing the contraction temperature range and reducing the shrinkage, improving the creep resistance and high-temperature flexural strength significantly. Mixing coarse, medium and fine fused silica powders in a ratio of 5:3:2, not only reduced high temperature contraction, but effectively improved the creep resistance. Properly increasing the sintering temperature can slightly reduce the thermal deformation and improve the high-temperature flexural strength of the silica-based core, but excessively high sintering temperature negatively impacts the creep resistance and high-temperature flexural strength. 相似文献
6.
《International Journal of Hydrogen Energy》2022,47(2):1217-1228
In this article, pre-assembly hot-press pressure and thermal expansion effects in gas-diffusion layers (GDLs) are addressed to explore the practicalities of the constitutive model reported in the companion article. A facile technique is proposed to include deformation history dependent residual strain effects. The model is implemented in the numerical environment and compared with widely followed conventional models such as isotropic and orthotropic material models. With the normal and accelerated thermal expansion effects no significant variation in stresses or strains is reported with the compressible GDL model in contrast to the conventional incompressible form of the GDL model. The present work identifies the critical differences with advanced and extended variants of the model along with conventional GDL material models in terms of planar stress/strain distribution and the membrane response. Finally, the model is simulated for micro-cyclic stress loads of varying amplitudes that imitate the real working conditions of fuel cell. The inelastic energy dissipation in GDLs is predicted using the proposed model, which is utilized further to distinguish the safe (elastic) and unsafe (inelastic shakedown) operating limits. The inelastic collapse of GDLs is shown to be a active function of high amplitude micro-cyclic load with high initial clamping load. 相似文献
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9.
对蒙古精矿在包钢624 m2带式球团的合理利用进行了全面研究。研究表明,随着蒙古精矿配比增加,球团矿品位提高,还原膨胀率增加,当配比小于20%时,还原膨胀率小于20.0%,主要是由于还原后球团矿矿物组成中析出大量金属铁,在浮氏体(FexO)转变为铁的阶段,铁晶粒自浮士体表面向外长出晶须,晶须的生长让晶粒产生位移或晶粒开裂,导致球团结构疏松发生膨胀。通过添加适量矽石,可显著降低球团还原膨胀率,当配加30%~50%的蒙古精矿时,可通过添加1.0%~2.0%的矽石,将球团还原膨胀率降低至20%以内,球团矿质量满足高炉冶炼生产要求。 相似文献
10.
Yuan Baohe Cao Wensi Wang Weishu Liang Erjun Cheng Tao 《International Journal of Applied Ceramic Technology》2019,16(2):647-653
The optical property and phase transition of ZrV2O7 were investigated by temperature-dependent X-ray diffraction, photoluminescence (PL), and Raman spectra. It was found that the material exhibited PL emission in the visible region. The temperature-dependent PL emission showed that the peak energy for emission (at red wavelength) presented a red shift from 10 to 80 K, and then a blue shift with the increase in temperature. The PL emission bands of ZrV2O7 shifted with change in temperature relating to its phase transition (80-100 K), which could be confirmed by temperature-dependent Raman spectra. 相似文献