Precision equipment for symmetrical bending— Part 1. The loading system

The design and performance of precision bending equipment for testing straight beams with constant rectangular section under a pure bending moment is described. Part 1 deals with the loading arrangements and Part 2 with the rig for measuring beam deflection. The methods for recording deflection of strain gauges applied on the beam have been described elsewhere.^1–4
The reactions to the deadweight gravity loads are taken via ball bearings. The total bending moment inaccuracy, i.e. the sum of estimated systematic errors and random errors, the latter expressed as the 2Ga confidence interval about the mean (2G_cim), is about ± 25 x. 10^-4%, for 23 tests with a steel beam with 15 mm × 75 mm cross sectional dimensions, loaded to 1-1.5 mm/m strain.
The measuring rig stands on the beam via hardened and polished spherical segment feet and uses a capacitive transducer system with less than 5nm resolution. Various application tasks are described. The total inaccuracy of the measured deflection, i.e. apart from bending moment inaccuracy, is about ± 35 times 10^4% for about 10 reproduced, not repeated, tests with the same steel beam. The deflection for such a beam is of the order of 2 to 4 mm.     

波长为515nm的氩离子激光器的频率稳定

用声光晶体对氩离子激光作频率调制,获得了碘分子的差拍饱和吸收信号。将得到的斜率极陡的—阶微商形式的饱和吸收信号作为鉴频曲线把氩离子频率激光稳定到~(127)I_2分子的p(13)43—0的a_3超精细分量上。通过与一稳定到相同精细分量的稳频氩离子激光拍频,给出激光频率稳定性优于±6.5×10~(-12),重复性优于±3.4×10~(-11)。     

彩色摄像机彩色重现性改善的一种方法

本文在彩色摄像机实际光谱特性曲线未知,并与理论光谱特性曲线又存在偏离情况下使用线性变换原理,提出一种改善摄像机彩色重现性的方法。     

相对压强对白炭黑氮吸附表面积测试稳定性的影响

研究相对压强对白炭黑氮吸附表面积测试稳定性的影响。结果表明:在相同液氮纯度、脱气温度、脱气时间、氮吸附点数量条件下,与相对压强范围为0.05~0.1时相比,相对压强范围为0.05~0.2时白炭黑的氮吸附表面积测量值偏低,且差值随氮吸附表面积的增大呈增大趋势;相对压强范围较小时,氮吸附表面积测试结果的线性相关因数较大,再现性较好,测试结果较稳定。     

用于测定钢液低氧含量的双层固体电解质研究

采用“毛坯浆料法”在ＺｒＯ２（９％摩尔含量ＭｇＯ）管状固体电解质基体表面制备了厚度为１－４μｍ的ＺｒＯ２（１０％摩尔含量Ｙ２Ｏ３）固体电解质涂层，并分别对此在本实验室和美国ＬｅｅｄｓａｎｄＮｏｒｔｈｒｕｐ公司进行了钢液低氧含量测试，结果表明：涂层没有破坏基体的抗热震性：氧浓差电池电动势的重现性偏差由原来的±２ｍＶ；电动势的绝对值提高１０ｍＶ左右；而比日本Ｔｏｒａｙ公司的同类产品提高３５ｍＶ，这说明     

镱应力传感器的制作与应用

在数十MPa~2 GPa范围内的动态应力测量中,镱传感器的压阻系数高,可灵活埋置于待测材料中使用。该种传感器对研究冲击波在岩石、土壤、液体介质和结构材料中的传播与衰减规律显示出了优异性能。对国内外镱应力传感器研制工作进行了总结,介绍了该类传感器在爆炸、射弹侵彻、高速碰撞以及高能激光辐照等方面的应用,并指出了该种传感器存在的一些问题。     

A Modified Region Approach for Multivariate Measurement System Capability Analysis

Measurement system capability analysis is to determine whether the measurement system is capable for use in quality control. The existing research has been extended from univariate to multivariate cases. Two approaches, the multivariate analysis of variance (MANOVA) and the weighted principal components (WPC), were advocated in literature. The MANOVA method is constructed based on the volume ratio that treats the volume of constant‐density contours as the variability estimations. However, it ignores the fact that the relative position change of multivariate measurement errors could affect the measurement system capability. The WPC method uses dimension reduction to reduce the complexity but is unable to build the precision‐to‐tolerance ratio because it does not include tolerance. In this paper, we propose a modified‐region‐based method to compute the precision‐to‐tolerance ratio, the percent of repeatability and reproducibility, and the signal‐to‐noise ratio. This method also incorporates the variance–covariance structure of the measurement errors when dealing with the constant‐density contours of tolerances, total variation, and process variation. The performance of the modified‐region‐based method is evaluated based on a dataset from the literature and a set of relevant simulation. The proposed method proves to be effective compared with other methods.Copyright © 2014 John Wiley & Sons, Ltd.     

Reference Range Estimation: Accounting for Measurement System Errors

Reference range is a statistic that is used in health related fields to represent the range of the most likely values for a variable of interest. Based on this range, individuals are classified as being healthy or unhealthy. In biostatistics, the reference range is calculated as the (1 ? α)% prediction interval, where this prediction interval is based on the estimated population variance from the data. Such estimation of population variance is not precise, because obtained test results do usually have errors associated with them. These errors are due to the imprecise test procedure or gauge used. In this paper, the total variability in the data is decomposed into two categories. The first is the patient‐to‐patient variability and the other is the variability due to the measurement system used. Estimation of the two kinds is performed through a gauge repeatability and reproducibility study, then the reference range is calculated, taking into account only the patient‐to‐patient variability. The revised reference range procedure is illustrated through a case study of vitamin B12 test results. A closed form formula is given to calculate the probability of a given test result being within the revised reference range. Copyright © 2015 John Wiley & Sons, Ltd.     

A Two‐Stage Annealing Strategy for Crystallization Control of CH3NH3PbI3 Films toward Highly Reproducible Perovskite Solar Cells

The solvent‐engineering method is widely used to fabricate top‐performing perovskite solar cells, which, however, usually exhibit inferior reproducibility. Herein, a two‐stage annealing (TSA) strategy is demonstrated for processing of perovskite films, namely, annealing the intermediate phase at 60 °C for the first stage then at 100 °C for the second stage. Compared to conventional direct annealing temperature (DHA) at 100 °C, using this strategy, MAPbI₃ films become more controllable, leading to superior film uniformity and device reproducibility with the champion device efficiency reaching 19.8%. More specifically, the coefficient of variation of efficiency for 49 cells is reduced to 5.9%, compared to 9.8% for that using DHA. The TSA process is carefully studied using Fourier transform infrared spectroscopy, X‐ray diffraction, and UV–vis absorption spectroscopy. It is found that in comparison with DHA the formation of hydrogen bonding and crystallization of perovskite are much slower and can be better controlled when using TSA. The improvements in film uniformity and device reproducibility are attributed to: 1) controllable MAPbI₃ crystal growth stemming from the progressive formation of hydrogen bonding between methylammonium and halide; 2) suppression of intermediate phase film dewetting, which is believed to be due to its decreased mobility at the initial low‐temperature annealing stage.