排序方式: 共有4条查询结果,搜索用时 0 毫秒
1
1.
研究了磺胺二甲嘧啶(SM2)的示波极谱法。磺胺二甲嘧啶在0.01mol/LHCl介质中于-0.995V附近出现一清晰的阴极还原波。在1×10-7~1×10-4mol/L范围内,浓度与波高有良好的线性关系。检测下限可达3.0×10-9mol/L。测定了小儿胺散中的SM2的含量,与紫外-可见分光光度法对照,结果一致。测定了尿样中SM2的含量,结果令人满意。 相似文献
2.
建立限量检测磺胺二甲基嘧啶中杂质的方法.采用薄层层析的方法,用2种展开剂系统.双向层析对样品中的杂质进行检测.展开剂Ⅰ氨水-水-硝基甲烷-二氧六环(3mL:5mL:40mL:50mE),其中氨水体积分数为4%,展开剂Ⅱ为氯仿-甲醇-无水甲酸(45mL:5mL:0.15mL).结果表明:该方法能简便有效地检测出磺胺二甲基嘧啶中各种可能存在的杂质,并能对其进行限量分析. 相似文献
3.
Residues of veterinary antibiotics in manures from feedlot livestock in eight provinces of China 总被引:48,自引:0,他引:48
The residue levels of selected fluoroquinolones, sulfonamides and tetracyclines in 143 animal dung samples collected in 2007 from large-scale livestock and poultry feedlots in 8 provinces were determined by using ultrasonic extraction and liquid chromatography. Recoveries from spiked pig dung samples (spike level = 1 mg/kg) ranged from 73.9 to 102.0% for fluoroquinolones, from 81.6 to 92.3% for sulfonamides, and from 57.2 to 72.6% for tetracyclines. Relative standard deviations of the recoveries were less than 10% within the same day. Method quantification limits were measured from 0.031 to 0.150 mg/kg for fluoroquinolones, from 0.023 to 0.082 mg/kg for sulfonamides, and 0.091 to 0.182 mg/kg for tetracyclines in spiked pig manure samples. Analysis of 61 pig, 54 chicken and 28 cow dung samples collected in China revealed that in pig and cow dung, up to 33.98 and 29.59 mg/kg ciprofloxacin, 33.26 and 46.70 mg/kg enrofloxacin, 59.06 and 59.59 mg/kg oxytetracycline, and 21.06 and 27.59 mg/kg chlortetracycline could be detected, respectively. A maximum concentration of 99.43 mg/kg fleroxacin, 225.45 mg/kg norfloxacin, 45.59 mg/kg ciprofloxacin and 1420.76 mg/kg enrofloxacin could be detected in chicken dung. No appreciable sulfonamide antibiotic concentrations (less than 10 mg/kg) were found in any animal dung, and only sulfadimidine was observed, at a maximum concentration of 6.04 mg/kg, in chicken dung. Both enrofloxacin and chlortetracycline were detected with a very high occurrence in three animal manure samples. The residue levels for most antibiotics showed significant statistical differences among the sampling districts and the animal species. 相似文献
4.
1