Multilayer Clad Plate of Stainless Steel/Aluminum/Aluminum Alloy

The 3, 5, 20 layer clad plate from austenitic stainless steel, pure aluminum and aluminum alloy sheets were fabricated in different ways. The stretch and interface properties were measured. The result shows that 20 layer clad plate is better than the others. Well-bonded clad plate was successfully obtained in the following procedure: Basic clad sheet from 18 layer Al1060/Al3003 sheets was firstly obtained with an initial rolling reduction of 44% at 450 ℃, followed by annealing at 300 ℃, and then with reduction of 50% at 550 ℃ from STS304 on each side. The best 20 layer clad plate was of 129 MPa bonding strength and 225 MPa stretch strength.     

浅析层状复合板轧制新工艺

本文在对国内外层状金属复合板生产研究文献查阅分析的基础上,着重介绍了钎焊热轧法、燃烧合成轧制法、包套轧制法、PPR方法、ARB方法、PIT方法等复合新工艺基本工作原理,以及目前国内外应用各种新工艺所生产研究的新材料复合板,同时分析了复合板生产存在的问题,展望了复合板生产工艺的发展方向。     

Homogenization heat treatment of Mg-7.68Gd-4.88Y-1.32Nd-0.63Al-0.05Zr alloy

The microstructures and mechanical properties of the Mg-7.68Gd-4.88Y-1.32Nd-0.63A1-0.05Zr magnesium alloy were investigated both in the as-cast condition and after homogenization heat treatment from 535 to 555 ℃ in the time range 0-48 h by op- tical microscopy, scanning electron microscopy and hardness measurement. The as-cast alloy consisted of ct-Mg matrix, Mgs（Y0.5Gd0.5） phase which is a eutectic phase, strip of Al2（Y0.6Gd0.4） phase, little A13Zr and Mg（Y3Gd） phase. With the increasing of homogenization temperature and time, the Mgs（Y0.5Gd0.5） phase was completely dissolved into the matrix. The Al2（Y0.6Gd0.4） phase was almost not dissolved which impeded grain boundaries motion making the grain size almost not changed in the process of ho- mogenization. The optimum homogenization condition was 545 ℃/16 h. The tensile strength increased, yield strength decreased and the plasticity improved obviously after 545 ℃/16 h homogenization treatment.     

关于镁合金中长周期有序结构的研究综述

系统地介绍了6H、10H、14H、18R、24R型LPSO结构的原子堆垛和RE、Zn的占位特点,探讨了LPSO结构的形成条件和形成机制,分析了含LPSO结构相合金的组织演变过程并概述了组织演变方面最新的研究成果,总结了含LPSO结构相镁合金的室温和高温性能的研究现状,最后对该类合金未来的研究方向进行了展望。     

铸态Mg-2Zn-1.5Cu合金组织及力学性能

利用金相显微镜、扫描电镜、透射电镜、XRD物相分析以及力学性能测试等手段,研究了Mg-2Zn-1.5Cu(at%)合金的显微组织及力学性能。结果表明:铸态合金存在较为明显的元素偏析,主要的第二相为MgCuZn相;合金的力学性能随着温度的提高而不断降低,塑性变化幅度要明显高于强度,合金的断裂方式也由低温时的沿晶断裂转变为高温时的穿晶断裂;在相同温度下,随着应力的提升,合金的稳态蠕变速率提高,蠕变机制由晶界控制转变为晶界及位错共同控制;在相同的应力下,随着温度的提升,合金的稳态蠕变速率存在数量级的提升,蠕变激活能由130kJ/mol降低到36.4 kJ/mol;在200℃,45 MPa时,出现加速蠕变阶段,发生蠕变断裂,断口存在明显的穿晶断裂特征,基体中有大量的沿基面运动的位错,部分位错发生攀移,MgZnCu相具有减缓蠕变变形的作用。     

EW75-0.7Al合金挤压、时效态的组织及力学性能

通过OM、SEM、硬度及拉伸等测试手段,研究了EW75-0.7Al合金挤压及时效态的组织和力学性能。结果表明,挤压后合金晶粒明显细化,室温力学性能显著提高,抗拉强度为330MPa,屈服强度为242MPa,伸长率为11%。通过对合金进行T5时效处理,确定EW75-0.7Al合金的最佳T5峰时效制度为225℃×12h,经过T5峰时效处理后,合金的室温强度相比挤压态提高约100MPa。T5峰时效态合金在200℃高温下,力学性能下降不明显,在250℃高温下力学性能显著降低。通过分析合金高温下的断裂方式,发现250℃高温下,EW75-0.7Al合金的晶界强度显著降低,且时效析出相与基体的结合能力下降,最终导致合金在该温度下力学性能明显降低。     

Characterization of p precipitate phase in Mg-7Gd-5Y-1Nd-0.5Zr alloy

As reported in our previous works,a Mg-7Gd-5Y-1Nd-0.5Zr alloy recently developed exhibited remarkable age-hardening responses and excellent mechanical properties at both room and elevated temperatures.In Mg-7Gd-5Y-1Nd-0.5Zr alloy,the β precipitate phase was assumed to be one of the main strengthening phases in peak-aged samples.This study aimed to determine the crystal structure and orientation relationship of the β precipitate phase in Mg-7Gd-5Y-1Nd-0.5Zr alloy using transmission electron microscopy and high-resolution electron microscopy.The results indicated that the β precipitate had a face-centered cubic structure with a lattice parameter of a=2.22 nm.The orientation relationship between the β precipitate phase and the α-Mg matrix was(12)β$$$$(100)α,[110] β/[0001] α.The β plates formed on prismatic planes could play an important role in alloy strengthening by proving effective barriers to gliding dislocations.A single β plate often contained several domains of(11)β twin-related variants.A composition of Mg 5(Y0.4Gd0.4Nd0.2) was suggested for the β phase in Mg-7Gd-5Y-1Nd-0.5Zr alloy.     

Mg-Gd-Y-Nd-Zr合金中β相的形貌和晶体学特征(英文)

通过OM、SEM、TEM及EDS分析,研究MgGdYNdZr镁合金中β相的形貌、成分和晶体学特征,分析连续冷却与等温时效两种方式对β相析出行为的影响规律。结果表明,合金在400°C过时效阶段的沉淀相为(1100)面上的板状和块状β相。β相以(1100)为惯习面,与基体的取向关系为(211)//(0110),[011]//[0001]。根据EDS统计分析确定β相的成分为Mg5(Y0.4Gd0.4Nd0.2),与Mg5Gd同型。在连续冷却方式中,相变驱动力较小,晶界等缺陷处结构紊乱,易于松弛、应变,因而优先在晶界附近形核。     

Influence of Deformation Twins on Mechanical Properties and β Precipitation of Large-Cross-Section (290 mm × 230 mm) AZ80 Bar Fabricated by “Multi-direction Forging + Extrusion + Cold Compression ” Technique

采用“多向锻造+挤压+在线水冷”技术制备出截面尺寸为290 mm×230 mm的Mg-8Al-1Zn (AZ80,质量分数,%) 合金棒材,沿横截面的230 mm方向 (ND) 对棒材进行冷压缩,压下量约为20 mm,冷压缩导致横截面心部 (C) 产生大量变形孪晶,而表层 (O) 的孪晶较少。研究了形变孪生对力学性能和析出反应的影响。沿挤压方向 (ED)、截面的290 mm方向 (TD) 和 ND 3个方向从C 和 O 切取拉伸试样。测试结果表明：棒材的室温力学性能存在显著的各向异性和表里不一致性。挤压材的 O 沿 ED（ED-O）具有最高的强度,其性能为：RP0.2、Rm和 A分别为 295 MPa、401 MPa和10%, 而 C 沿 ND（ND-C）具有最低的强度,其性能为：RP0.2、Rm和 A 分别为164 MPa、273 MPa和 7%。织构是导致各向异性和表里不一致性的主要原因,而变形孪生对织构有重要影响。冷压缩之前,C存在2种取向,即： [0001]Mg∥TD 和 [0001]Mg∥ND;冷压缩后,O的织构几乎没有变化,而变形孪晶导致C的织构发生重大转变,[0001]Mg∥TD取向被大幅弱化,而[0001]Mg ~∥ND取向被大幅加强。合金155 ℃/7 h时效后,变形孪晶内析出了β连续析出相,这些孪晶内的β析出相比层片状β非连续析出相更加细小弥散     

Mg-7Gd-5Y-1Nd-0.5Zr合金静态再结晶机理的研究

利用硬度测试、OM和原位观察等方法研究了Mg-7Gd-5Y-1Nd-0.5Zr(wt%)合金在退火过程中的静态再结晶机理。结果表明:合金退火1min后出现析出相回溶和静态再结晶现象,静态再结晶晶核优先在原始晶界上形成,在动态再结晶区域中产生亚晶界;在退火5 min后,亚晶迅速转变为静态再结晶晶核,同时有大量黑色析出相产生;进一步延长退火时间,静态再结晶过程十分缓慢,长时间退火后部分变形晶粒仍然存在;在传统退火处理中静态再结晶过程十分迅速,静态再结晶模型符合JMAK模型,并没有析出相产生;随着退火时间的延长,静态再结晶晶粒尺寸不断增大,微观组织不均匀性加剧;退火15 min后,硬度与平均晶粒尺寸之间服从Hall-Petch关系。