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1.
Li-Xiang Wu Lin-Lin Zhu Wei-Ming Guo Shi-Kuan Sun Wen-Bin Niu Jia-Xiang Xue Jian-Han Zhai Hai-Bin Ma Rui-Lin Lin Hua-Tay Lin Kevin Plucknett Ye-Hong Liao Tong Liu Qi-Sen Ren 《Journal of the European Ceramic Society》2021,41(1):225-232
The joining of liquid-phase sintered SiC (LPS-SiC) ceramics was conducted using spark plasma sintering (SPS), through solid state diffusion bonding, with Ti-metal foil as a joining interlayer. Samples were joined at 1400 °C, under applied pressures of either 10 or 30 MPa, and with different atmospheres (argon, Ar, vs. vacuum). It was demonstrated that the shear strength of the joints increased with an increase in the applied joining pressure. The joining atmosphere also affected on both the microstructure and shear strength of the SiC joints. The composition and microstructure of the interlayer were examined to understand the mechanism. As a result, a SiC-SiC joining with a good mechanical performance could be achieved under an Ar environment, which in turn could provide a cost-effective approach and greatly widen the applications of SiC ceramic components with complex shape. 相似文献
2.
Fangjun Zhu You Shi Guorong Hu Zhongdong Peng Yanbing Cao Qian Sun Zhichen Xue Yinjia Zhang Ke Du 《Ceramics International》2021,47(3):3070-3078
Titanium and boron are simultaneously introduced into LiNi0.8Co0.1Mn0.1O2 to improve the structural stability and electrochemical performance of the material. X-ray diffraction studies reveal that Ti4+ ion replaces Li+ ion and reduces the cation mixing; B3+ ion enters the tetrahedron of the transition metal layers and enlarges the distance of the [LiO6] layers. The co-doped sample has spherical secondary particles with elongated and enlarged primary particles, in which Ti and B elements distribute uniformly. Electrochemical studies reveal the co-doped sample has improved rate performance (183.1 mAh·g-1 at 1 C and 155.5 mAh·g-1 at 10 C) and cycle stability (capacity retention of 94.7% after 100 cycles at 1 C). EIS and CV disclose that Ti and B co-doping reduces charge transfer impedance and suppresses phase change of LiNi0.8Co0.1Mn0.1O2. 相似文献
3.
To obtain the great surface quality of Ti–6Al–4V and achieve high efficiency in the polishing process, the chemistry enhanced shear thickening polishing (C-STP) was proposed, and the polishing performance of different pH slurry was studied. The results show that the material removal rate gradually increases as the pH value decreases from 10 to 1, and the best surface quality is obtained at pH 2. The corrosion current density and potential were measured by potentiodynamic polarization under three typical pH values. It is confirmed that the most massive corrosion rate presents at pH 2, and the passive film is most susceptible to be produced at pH 10. The reaction resistance was measured by electrochemical impedance spectroscopy to clarify the polishing mechanism. Under acidic conditions, the chemical reaction product on the surface can be quickly removed by mechanical action of the abrasive. On the contrary, the passive film formed on the surface under the alkaline condition is difficult to be removed. The corrosion reaction products were determined by X-ray photoelectron, and the chemical reaction under acid-base environment was derived. MRR reached 107.3 nm/min under the selected process parameters, and the surface roughness (Sa) is reduced from 124 nm to 8.6 nm within 15 min. 相似文献
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塔里木盆地深部碳酸盐岩储层以次生溶蚀孔、洞、缝为主,空间分布具有极强的非均质性。传统的"相控建模"、"岩溶建模"和"碳酸盐岩储层相控建模"方法均不能准确刻画储层分布特征。为此,提出地震约束建模方法:首先基于线性反演去除资料的AVO效应获得纯纵波数据,然后结合测井信息计算相对波阻抗,并进一步转化为绝对波阻抗属性定量质控波阻抗反演质量。采用的建模方法本质上属于确定性建模,流程包括纯纵波数据提取、相对阻抗计算、振幅约束低频建模、波阻抗反演等。ZG8井区的实例分析证实:基于纯纵波振幅约束建模的反演方法可以避免传统插值建模方法受井资料影响大的局限,克服了常规融合层速度等建模方法精度不高的缺陷,准确反演了强非均质储层的分布规律。 相似文献
6.
《Ceramics International》2020,46(3):2654-2660
Brown fused alumina is a cost-effective alumina material, and the state of Ti in alumina has a great influence on its high-temperature performance. In this paper, the Ti-containing phases in brown fused alumina particles and Al-brown fused alumina refractory were successfully transformed into Ti(C,N) at 1973 K in flowing N2. The evolution of the Ti-containing phases in brown fused alumina under high temperature and nitrogen conditions was investigated by XRD, SEM and EDS. The results show that the Ti-containing phases in brown fused alumina include Ti2O3, Ti(C,N,O), TiFeSi2, Ca0·95Mg0·9Al10·1(Ti)O17 and a low-melting point Ca3Al2Si3(Mg,Ti)O12 phase. Under high temperature and nitrogen conditions, the TiO2[liquid], MgO[liquid] and SiO2[liquid] in the low-melting point phase are transformed into Ti(C,N), Mg(g) and SiO(g), while they are supplemented from Ti2O3, Ti(C,N,O) and Ca0·95Mg0·9Al10·1(Ti)O17. After heat treatment at 1973 K for 3 h, Ti2O3 and Ti(C,N,O) disappear, Ca0·95Mg0·9Al10·1(Ti)O17 is transformed into plate-like Ca0·55Al11O17.05, and Ti(C,N) is formed on the surface of the corundum particles. The formation of Ti(C,N) reduces the porosity of the brown fused alumina particles and increases their strength. 相似文献
7.
为探索醚化2D树脂对纯棉织物抗皱整理的可行性和最佳工艺设置,设计正交试验探究醚化2D树脂、催化剂、保护剂、柔软剂在成衣免烫技术中的应用工艺,确定最佳工艺为醚化2D树脂F-AP质量浓度150 g/L、催化剂FM质量浓度40 g/L、保护剂HDP质量浓度35 g/L、柔软剂NUP质量浓度15 g/L。应用SPSS统计分析软件对4种助剂对棉织物的抗皱整理效果做显著性检验,结果表明:相对另外3种助剂,醚化2D树脂对棉织物的抗皱整理效果影响最为显著。重点分析了醚化2D树脂对整理后织物性能的影响,发现醚化2D树脂质量浓度超过160 g/L时,棉纤维与树脂的反应呈现饱和,使棉织物折皱回复角和断裂强力变化趋缓,过多的树脂残留使纱线间的摩擦力增加,对织物抗撕破起负效果。 相似文献
8.
本文将研究不同方法发酵的酸豆角品质对比分析。选取质地嫩脆、条形均匀、无病虫害的新鲜豆角为泡制原料。采用自然干法发酵、自然湿法发酵与纯种湿法发酵的发酵方法制作酸豆角。检测发酵过程中,pH值、还原糖含量、总酸含量、总糖含量、亚硝酸盐含量以及氨基酸态氮含量,分析纯种湿法发酵与自然湿法发酵对酸豆角品质的影响。结果表明:纯种湿法发酵25 d后,其pH值和还原糖含量分别为3.92、0.03%,均高于自然湿法发酵;总酸、总糖、亚硝酸盐含量、氨基酸态氮含量分别为0.25%、0.04%、0.01 mg/kg和0.01%,均低于自然湿法发酵。另外,纯种湿法发酵酸豆角的甲氧基乙酸含量为0.37%,乙酸乙酯为0.51%,含水量为81.15%,感官评分为45.52,均高于自然干法发酵。纯种湿法发酵对酸豆角品质的效果最好,亚硝酸盐的含量在发酵后期显著降低,感官评分较高,对豆角工业化生产提供了较好的参考价值。 相似文献
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10.
《能源学会志》2020,93(2):496-507
Hydrocarbons could be used as the reductant for elimination of NOx emissions. Liquid petroleum gas, with higher carbon hydrocarbons and cheaper costs, may be of practical value as reducing agents. Due to the consumption of hydrocarbons by oxygen, the NOx reduction efficiency is significantly inhibited by oxygen in the flue gas. In this research, a novel rotary reactor, realizing the alternating cycle of adsorption zone and reduction zone, was proposed to overcome this negative effect. Co–Ce–Ti mixed oxide catalysts synthesized by a sol–gel method were tested in a simulated rotary reactor for NOx removal by liquid petroleum gas and characterized by SEM, BET, XRD and XPS. The results showed that catalysts exhibited better NO conversion efficiency at higher temperature but were highly susceptible to oxygen. Catalysts achieved nearly full removal of NOx from flue gas at 300 °C in a simulated rotary reactor, and 300 °C is considered to be the most optimum temperature with lower energy consumption and excellent flue gas purification performance. 相似文献