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1.
《Ceramics International》2021,47(19):27386-27394
In order to control the pore characteristics and macroscopical performance of porous ceramics, roles of the freeze casting parameters are the key points. Herein, aligned dendritic porous SiC was fabricated by freeze casting of PCS-camphene solutions with different solid loading, freeze front velocity, temperature gradient, and freezing temperature. Influence of these parameters on the microstructure and compressive strength of porous SiC was investigated. With increasing the PCS content, freeze temperature, freeze front velocity or temperature gradient, degree of undercooling of the camphene was increased, resulting in the formation of smaller pore size, decreased porosity and increased compressive strength. Compared to variables of freeze temperature and temperature gradient, increased freeze front velocity was more efficiency in improving the compressive strength of porous SiC, owing to the formation of smaller pore size and longer secondary dendritic crystals. Promising micron-sized porous SiC with high porosity (79.93 vol%) and satisfactory strength (15.84 MPa) was achieved for 10% PCS-camphene solution under optimized freezing conditions. 相似文献
2.
Dr. Saeed Chashmniam Dr. João M. C. Teixeira Prof. Juan Carlos Paniagua Prof. Miquel Pons 《Chembiochem : a European journal of chemical biology》2021,22(6):1001-1004
Coupling of side chain dynamics over long distances is an important component of allostery. Methionine side chains show the largest intrinsic flexibility among methyl-containing residues but the actual degree of conformational averaging depends on the proximity and mobility of neighboring residues. The 13C NMR chemical shifts of the methyl groups of methionine residues located at long distances in the same protein show a similar scaling with respect to the values predicted from the static X-ray structure by quantum methods. This results in a good linear correlation between calculated and observed chemical shifts. The slope is protein dependent and ranges from zero for the highly flexible calmodulin to 0.7 for the much more rigid calcineurin catalytic domain. The linear correlation is indicative of a similar level of side-chain conformational averaging over long distances, and the slope of the correlation line can be interpreted as an order parameter of the global side-chain flexibility. 相似文献
3.
为了抑制铣削过程中产生的颤振,提高铣削加工过程中零部件表面质量。设计了小波神经网络PID控制方法,并对控制效果进行仿真。采用时域数值法对动态铣削过程中离散时间进行求解,利用小波神经网络PID控制方法对铣削过程进行控制。通过仿真和实验对铣削金属表面粗糙度进行测量,并且与增量式PID控制系统进行比较和分析。结果显示,采用增量式PID控制方法,铣削力和铣削深度实际值与理论值存在较大误差;采用小波神经网络PID控制方法,铣削力和铣削深度实际值与理论值存在较小误差。采用小波神经网络PID控制方法,可以提高铣削参数控制精度,减少铣削过程中对颤振的影响,提高铣削零部件表面质量。 相似文献
4.
针对燃油系统地面模拟试验气箱压力控制所存在的非线性、时变性问题,提出了一种基于改进粒子群算法(IPSO)优化的BP-PID控制器。该控制器结合改进粒子群算法全局搜索能力强和收敛速度快的特点,对BP神经网络的连接权值不断地调整,输出最优的PID控制参数。依据地面模拟试验参数,建立了主要器件的数学模型,利用Simulink软件对各器件的仿真模块进行搭建,构成一个完整的气箱控制系统进行研究。结果表明,IPSO-BP-PID控制比BP-PID控制响应速度快,稳定性好,超调量小,大大提高了气箱压力控制过程的精确性与鲁棒性。 相似文献
5.
采用热重分析法研究了经KOH浸渍的甲壳素的热解特性,并考察了不同浸渍比对热解过程的影响;同时采用Coats-Redfern积分法拟合计算出热解动力学参数,探究了KOH对甲壳素主要热解过程中活化能的影响。热重分析结果表明:KOH的加入改变了甲壳素的热解行为,降低了热解所需的活化能,加快了反应速率,促进了甲壳素热解;当浸渍比即m(65% KOH)∶m(甲壳素)=2∶1或3∶1时,KOH浸渍后能使甲壳素在140℃左右开始迅速热解。热解动力学参数计算结果表明:无论反应级数选择多大,其线性拟合效果均比较好,相关系数基本都高于0.95;KOH作用下甲壳素热解是一个复杂的化学反应,而不是单一的某一级反应。 相似文献
6.
为解决传统预裂爆破与光面爆破技术难以满足现如今高质量、高标准施工要求的难题,根据切缝药包的作用机理,对切缝药包在边坡预裂爆破中的应用进行研究。根据现场施工情况,设计相应爆破参数,进行切缝药包预裂爆破参数优化试验,并对切缝药包预裂爆破和传统预裂爆破的工程应用进行对比研究。试验结果表明:在中硬岩、90 mm直径预裂孔的条件下,采用外径40 mm、内径36 mm,切缝长度0.8m,切缝宽度10mm的PVC管作为切缝管进行切缝药包预裂爆破,其爆破效果较好;通过与传统预裂爆破相比,切缝药包预裂爆破后预裂缝宽度增加了1.12倍,预裂面不平整度减少了52.8%,半孔率提高了21%,振动速度峰值降低了29.02%,有效减少了爆破能量对保留边坡与周边构建筑物的损害,显著提高了爆破施工的质量。 相似文献
7.
《Ceramics International》2021,47(19):27351-27360
A series of xPbO–(45-x)CuO–55B2O3 glasses (5 ≤ x ≥ 40 mol %) were prepared by the melt-quenching technique. The X-ray diffraction (XRD) patterns of the prepared glasses are found to have amorphous structure. An extensive ultrasonic study has been made to explore the structural role of PbO and CuO in the borate network. Various elastic properties were calculated from the measured data of density and ultrasonic velocity. Ultrasonic velocity and elastic moduli revealed broad humps at about 20 mol % PbO, which are attributed to the borate anomaly. Below 20 mol % PbO, all Pb2+ ions are considered to be entering the borate network as a glass modifier. This results in the transforms the borate network from an open structure to a denser three-dimensional structure due to BO3 → BO4 conversion. Beyond 20 mol, addition of PbO results in the formation of metaborate, pyroborate, and orthoborate units with NBOs. This weakness the glass structure and decrease both ultrasonic velocity and elastic moduli. The elastic properties were predicted and quantitatively analyzed by taking into account the effect of boron coordination number on the compositional and structural parameters involved in Makishima–Mackenzie's theory, ring deformation model and bond compression model. An excellent agreement between the computed theoretical and experimental elastic moduli, micro-harness and Poisson's ratio was achieved for majority of samples. 相似文献
8.
利用有限元分析软件ABAQUS研究微织构PCBN刀具车削Cr12MoV的过程,采用田口法进行正交试验设计,通过信噪比分析方法研究刀?屑实际接触面积、切削力和切削温度随织构参数的变化规律,并获得织构参数的最优组合。结果表明,刀?屑实际接触面积分别随织构槽宽和织构刃边距的增大而减小,织构槽宽和织构刃边距对刀具的切削性能影响最显著;与无织构刀具对比,选取最优织构参数组合的微织构PCBN刀具可使切削力降低5.2%,切削温度降低4.7%。 相似文献
9.
《中国有色金属学会会刊》2021,31(7):1939-1950
The isothermal extrusion process of hollow aluminium profile was investigated using incremental proportional–integral–derivative (PID) control algorithm and finite element simulations. The range of extrusion speed was determined by considering the maximum extrusion load and production efficiency. By taking the optimal solution temperature of the secondary phase as the target temperature, the extrusion speed–stroke curve for realizing the isothermal extrusion of the aluminium profile was obtained. Results show that in the traditional constant extrusion speed process, the average temperature of the cross-section of the aluminium profile at the die exit rapidly increases and then slowly rises with the increase in ram displacement. As the extrusion speed increases, the temperature difference at the die exit of the profile along the extrusion direction increases. The exit temperature difference between the front and back ends of the extrudate along the extrusion direction obtained by adopting isothermal extrusion is about 6.9 °C. Furthermore, the heat generated by plastic deformation and friction during extrusion is balanced with the heat transfer from the workpiece to the container, porthole die and external environment. 相似文献
10.
The effect of an external electric field on laser-generated plasma has been studied. It is observed that the laser-generated plasma can be used for the ignition of a spark in the presence of a low voltage external electric field. An eight-fold emission intensity enhancement in Cu Ⅰ spectral lines are measured as compared to the signal intensity in the absence of an external electric field.The plasma parameters remain the same initially, up to a few microseconds after the generation of plasma, and this feature makes it more interesting for the quantitative analysis of any sample using laser induced breakdown spectroscopy(LIBS). In the presence of an external electric field,fluctuations(contraction and expansion) in the laser-generated plasma are observed which increase the plasma decay time and consequently result in enhanced signal intensity. 相似文献