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1.
《Advanced Powder Technology》2022,33(11):103833
Eliminating the gold preg-robbing effect of carbonaceous matter in carbonaceous gold ores is crucial for gold leaching. In this study, suspension oxidation roasting was proposed to accelerate the decarbonization of carbonaceous gold ore. The characteristics of oxidation reaction process and gas release were analyzed by TG-DTA-FTIR. The phase transformation and microstructure evolution of samples during roasting were analyzed by XRD, SEM and BET. The results show that the gold preg-robbing effect was eliminated after the gasification of carbonaceous matter, and the CaO generated by decomposition of carbonates can effectively capture the SO2. After roasting for 75 min at 650 °C in a 20% O2 atmosphere, the total carbon removal rate reached 99.42%, the distribution of exposed gold increased from 28.85% to 77.10% and the gold leaching efficiency increased from 4.55% to 84.83%. In addition, about 70% sulfur was mainly fixed in the roasted products in the form of sulfate. Therefore, the suspension oxidation roasting process is an efficient and clean pretreatment method for carbonaceous gold ores. 相似文献
2.
某铅锌矿原矿铅含量为1.26%,含锌6.53%,含硫30.38%。生产上采用“铅锌依次优先浮选-中矿顺序返回”工艺流程,生产指标为铅精矿铅品位50.69%,含锌12.61%,铅回收率75.53%,锌精矿锌品位48.77%,含铅1.59%,锌回收率73.91%。铅锌互含较高,锌精矿指标不理想。为了解决该问题,本文在了解现场生产工艺流程及矿石性质的基础上,针对该铅锌矿开展了详细的选矿工艺优化试验,通过对部分药剂制度进行优化,采用特效捕收剂BK-LY11,同时在锌浮选回路采用中矿再磨工艺,显著改善了铅锌互含情况,有效提高了铅锌选别指标,并成功应用于生产实践,优化后获得的铅、锌回收率分别提高了5.83、8.46个百分点。 相似文献
3.
超临界二氧化碳是一种特殊的流体,具有粘度低、扩散系数大、密度大和溶解性较好等特点,因此被认为是第四代核反应堆能量传递的首选材料。由于核反应堆的工作环境十分苛刻,超临界二氧化碳应用于核反应堆系统中易造成材料腐蚀,为确保核反应堆安全有效地运行,对超临界二氧化碳腐蚀行为进行系统研究,介绍了核反应堆的发展历程,重点探讨超临界二氧化碳对合金材料腐蚀的机理,详细阐述了温度、压力、杂质和流速等因素对材料在超临界二氧化碳中腐蚀行为的影响,针对目前的研究提出了亟待解决的问题。 相似文献
4.
本文以工业纯铝和混合稀土RE(Ce和La)为原料,制备出Al-8RE、Al-10RE和Al-15RE中间合金,并探讨了Al-RE中间合金对变形铝合金3102的细化机理。结果表明:Al-RE中间合金由α-Al、Al11RE3(Al11Ce3和Al11La3)、Ce和La组成,不同稀土含量Al-RE中间合金微观组织形貌不同,Al-8RE、Al-10RE和Al-15RE中间合金组织分别为亚共晶组织,伪共晶组织和过共晶组织,随稀土含量增加,Al-RE中间合金中Al11RE3相数量增多,尺寸增大;Al-RE中间合金对3102合金具有显著的细化效果,其中Al-10RE中间合金的细化效果最好;添加Al-RE中间合金可以提高产品性能,当添加10%RE时,性能提升最大。 相似文献
5.
Alexander Van-Brunt Patrick E. Farrell Charles W. Monroe 《American Institute of Chemical Engineers》2022,68(5):e17599
We present the Onsager–Stefan–Maxwell thermodiffusion equations, which account for the Soret and Dufour effects in multicomponent fluids. Unlike transport laws derived from kinetic theory, this framework preserves the structure of the isothermal Stefan–Maxwell equations, separating the thermodynamic forces that drive diffusion from the force that drives heat flow. The Onsager–Stefan–Maxwell transport-coefficient matrix is symmetric, and the second law of thermodynamics imbues it with simple spectral characteristics. This new approach allows for heat to be considered as a pseudo-species and proves equivalent to both the intuitive extension of Fick's law and the generalized Stefan–Maxwell equations popularized by Bird, Stewart, and Lightfoot. A general inversion process facilitates the unique formulation of flux-explicit transport equations relative to any choice of convective reference velocity. Stefan–Maxwell diffusivities and thermal diffusion factors are tabulated for gaseous mixtures containing helium, argon, neon, krypton, and xenon. The framework is deployed to perform numerical simulations of steady three-dimensional thermodiffusion in a ternary gas. 相似文献
6.
《Journal of the European Ceramic Society》2022,42(10):4377-4387
RE disilicates are good candidates as environmental/thermal barrier coating for SiCf/SiC composite in harsh gas turbine engines. We designed (Yb1?xHox)2Si2O7 solid solutions and studied mechanical properties, thermal properties, and water vapor resistance. Powders with different compositions were synthesized by pressureless sintering, and bulk samples were prepared by Spark Plasma Sintering (SPS). Polymorphic changes with temperature and composition of the solid solutions were examined. Through doping Ho into Yb2Si2O7, water vapor corrosion resistance is significantly promoted, and thermal expansion coefficient is maintained close to that of Si-based ceramics. Compared with host disilicates, thermal conductivity of solid solutions are decreased, and mechanical properties, including Vickers hardness and fracture toughness, are increased. A two-phase domain is found at (Yb1/2Ho1/2)2Si2O7, and the γ to δ phase transition of Ho2Si2O7 is observed during SPS. Among all samples, γ-(Yb1/3Ho2/3)2Si2O7 possesses superior high temperature stability, and excellent water vapor resistance, indicating its performance as environmental/thermal barrier coating. 相似文献
7.
《Journal of the European Ceramic Society》2022,42(13):5314-5322
Owing to the high melting points and high-temperature stability, transition-metal disilicides are potential components for aerospace, automotive, and industrial engineering applications. However, unwanted oxidation known as PEST oxidation severely limits their application owing to the formation of volatile transition metal oxides, especially in the temperature range of 500–1000 °C. To overcome this problem, a new class of high-entropy disilicides, (Mo0.2Nb0.2Ta0.2V0.2W0.2)Si2, was selected by first-principles calculations and then successfully fabricated using a hot-pressing sintering technique. Furthermore, the phase evolution, thermal expansion behavior, thermal conductivity, and oxidation behavior were systematically investigated. Compared with MoSi2, (Mo0.2Nb0.2Ta0.2V0.2W0.2)Si2 possessed a lower thermal conductivity (10.9–14.7 W·m?1·K?1) at 25–1000 °C, higher thermal expansion coefficients (8.6 ± 1.3–6 K–1) at 50–1200 °C, and especially an excellent thermal stability at 500–1000 °C owing to slow diffusion and selective oxidation. This work provides a strong foundation for the synthesis and application of high-entropy disilicides. 相似文献
8.
9.
为研究地铁施工风险耦合机理和地铁施工系统的脆弱性,提高地铁施工系统的安全性。结合脆弱性理论,归纳地铁施工安全风险因素,构建系统脆弱性模型;并对国内2008-2020年的地铁施工事故进行搜集整理,选取风险致因因素完整的130起事故,运用N-K模型计算不同耦合方式下的风险发生概率以及风险耦合值,获得影响系统脆弱性的关键风险耦合方式。结果表明:系统中的风险因素越多,事故发生的概率越大;人员因素、管理因素与环境因素完全耦合时,地铁施工安全系统脆弱性较大。研究明确系统中脆弱性的关键耦合风险,为地铁施工安全控制方面提供了参考价值。 相似文献
10.
目的 了解我国食品理化实验室专业技术人员食品安全知识、态度、行为现状,探讨其影响因素。方法 对我国15个省的省级、市级、区(县)级部门下属食品理化实验室及第三方机构、企业等非政府机构食品理化实验室的专业技术人员开展食品安全知识、态度、行为问卷调查,并对调查结果进行统计分析。结果 共回收有效问卷1339份。除性别对态度得分无显著影响,文化程度、就职年限等对行为无显著影响外,年龄、实验室类型、所在区域和最近一次接受培训时间等均是影响食品理化检验人员食品安全知识、态度、行为得分的因素,且知识、态度和行为得分存在正相关关系。结论 尽管存在满分问卷,但食品理化实验室专业技术人员KAP平均得分仅略高于及格水平。需要关注重点人群,如年龄25岁以下、就职年限2年以下或大专及以下学历的专业技术人员等食品安全知识水平的提升、态度的端正和行为的规范。 相似文献