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1.
《Advanced Powder Technology》2022,33(11):103833
Eliminating the gold preg-robbing effect of carbonaceous matter in carbonaceous gold ores is crucial for gold leaching. In this study, suspension oxidation roasting was proposed to accelerate the decarbonization of carbonaceous gold ore. The characteristics of oxidation reaction process and gas release were analyzed by TG-DTA-FTIR. The phase transformation and microstructure evolution of samples during roasting were analyzed by XRD, SEM and BET. The results show that the gold preg-robbing effect was eliminated after the gasification of carbonaceous matter, and the CaO generated by decomposition of carbonates can effectively capture the SO2. After roasting for 75 min at 650 °C in a 20% O2 atmosphere, the total carbon removal rate reached 99.42%, the distribution of exposed gold increased from 28.85% to 77.10% and the gold leaching efficiency increased from 4.55% to 84.83%. In addition, about 70% sulfur was mainly fixed in the roasted products in the form of sulfate. Therefore, the suspension oxidation roasting process is an efficient and clean pretreatment method for carbonaceous gold ores. 相似文献
2.
Sk Tanbir Islam Sudip K. Samanta Santanu Das Himadri Chattopadhyay 《Journal of the American Ceramic Society》2022,105(7):4608-4620
The micro-powder injection molding (micro-PIM) process has the potential to bridge the gap between the design and manufacturing of micro-components that are often used in small and handy devices. Numerical modeling helps to analyze and overcome various difficulties of micro-PIM. In the present work, a numerical model is developed to predict the powder–binder separation (a common defect in PIM and especially severe in micro-PIM) during the injection of an alumina feedstock. A powder–binder separation criterion is proposed dealing with applied injection pressure and friction force between the powder and binder. An indirect comparison of feedstock travel time between two locations is used to validate the model. The predicted segregation from the simulated result is supported by a qualitative experimental measurement. The developed model can be used to optimize injection parameters to get a defect-free product. 相似文献
3.
《Journal of the European Ceramic Society》2022,42(15):7036-7048
MgB2 superconductor pellets were synthesized through Mg gas infiltration method using nanosized- and microsized B powders. There was a marked difference in the superconducting properties of the two samples, particularly in the pinning force and dominant pinning mechanism. The microstructures of the samples were observed using HR-TEM and STEM-HAADF, and the results showed that the primary reason for the difference in the superconducting properties is the distribution of the nanosized second-phase particle MgO. Additionally, a feasible reaction model for the Mg gas infiltration method was established. Compared to the Mg liquid infiltration method, the gas infiltration showed better penetrability ability with a small amount of residual Mg. This study presents a novel synthesis process to fabricate an MgB2 pellet with superior density and superconducting properties. This method can be used in multiple applications such as superconducting bearings, compact superconductor magnets, and magnetic shielding. 相似文献
4.
5.
《Current Opinion in Solid State & Materials Science》2022,26(6):101024
One of the main challenges in the laser powder bed fusion (LPBF) process is making dense and defect-free components. These porosity defects are dependent upon the melt pool geometry and the processing conditions. Power-velocity (PV) processing maps can aid in visualizing the effects of LPBF processing variables and mapping different defect regimes such as lack-of-fusion, under-melting, balling, and keyholing. This work presents an assessment of existing analytical equations and models that provide an estimate of the melt pool geometry as a function of material properties. The melt pool equations are then combined with defect criteria to provide a quick approximation of the PV processing maps for a variety of materials. Finally, the predictions of these processing maps are compared with experimental data from the literature. The predictive processing maps can be computed quickly and can be coupled with dimensionless numbers and high-throughput (HT) experiments for validation. The present work provides a boundary framework for designing the optimal processing parameters for new metals and alloys based on existing analytical solutions. 相似文献
6.
《Soils and Foundations》2022,62(5):101206
Coral sand is one kind of the important building materials in coral reef engineering practice. The use of cement as a stabilizing agent can significantly improve the mechanical properties of coral sands and is widely applied in the subbase engineering construction in coral reef islands. Cement-stabilized coral sand structures may contain high contents of fine coral particles and salinity because of the high crushability of coral sands and the existence of seawater surrounding them. In this study, the effects of coral sand powders and seawater salinity on the dynamic mechanical properties of cemented coral sand (CCS) were investigated through the split Hopkinson pressure bar (SHPB) tests and Scanning Electron Microscope (SEM) analysis. It was found that the strength (i.e., the peak stress) of CCS specimens increased firstly and then decreased with the increase of powder content. The specimens reached the maximum peak stress when 3% powder content was included. The initial improvement of CCS strength was attributed to the pore-filling effect of coral powders, namely, the micro pores of the CCS specimens could be more effectively filled with higher percentages of coral powders being used in the experiments. However, excessive coral powders resulted in the reduction of specimen strength because these powders could easily be cemented into agglomerates by absorbing water from the specimens. These agglomerates could reduce the cementation strength between the coarse coral particles and the cement. Meanwhile, the peak stress of CCS specimens was found to be negatively correlated with the average strain rate and the ultimate strain. The degree of specimen fracture was found to be correlated with the amount of specific energy absorption during the tests. Furthermore, the “sulfate attack” caused by the inclusion of salinity of water had different influences on the CCS specimens with different coral powder contents. The ettringite and gypsum produced in “sulfate attack” could fill the pores and lead to cracking of the specimens, significantly affecting the specimen strength. 相似文献
7.
Rong Zhu Juan Li Lisen Lin Jibin Song Huanghao Yang 《Advanced functional materials》2021,31(10):2005709
Plasmonic gold nanocrystal represents plasmonic metal nanomaterials, and has a variety of unique and beneficial properties, such as optical signal enhancement, catalytic activity, and photothermal properties tuned by local temperature, which are useful in physical, chemical, and biological applications. In addition, the inherent properties of predictable programmability, sequence specificity, and structural plasticity provide DNA nanostructures with precise controllability, spatial addressability, and targeting recognition, serving as ideal ligands to link or position building blocks during the self-assembly process. Self-assembly is a common technique for the organization of prefabricated and discrete nanoparticle blocks for the construction of extremely sophisticated nanocomposites. To this end, the integration of DNA nanotechnology with Au nanomaterials, followed by assembly of DNA-functionalized Au nanomaterials can form novel functional Au nanomaterials that are difficult to obtain through conventional methods. Here, recent progress in DNA-assembled Au nanostructures of various shapes is summarized, and their functions are discussed. The fabrication strategies that employ DNA for the self-assembly of Au nanostructures, including dimers, tetramers, satellites, nanochains, and other nanostructures with more complex geometric configurations are first described. Then, the characteristic optical properties and applications of biosensing, bioimaging, drug delivery, and therapy are discussed. Finally, the remaining challenges and prospects are elucidated. 相似文献
8.
《Ceramics International》2022,48(10):14192-14200
In this study, mold powder slurries with high solid loading and low viscosity were prepared during the ball-milling process for improving the homogeneity and mechanical properties of granules after spray-drying. The effect of ball-milling parameters, such as solid loading, binder/dispersant content, and ball-milling time, on the flowability, dispersibility, stability, and rheological behavior of mold powder slurries was systematically investigated by rheology observation and sedimentation tests. As these parameters varied, the slurry exhibited the shear-thinning behavior of a non-Newtonian fluid with a shear rate range of 0–50 s?1, which was adequately described by the Herschel-Bulkley model. The optimal parameters that optimized the flowability, dispersibility, and stability of the slurry, along with its rheological behavior, were chosen as follows: solid loading, 60 wt%; modified sodium carboxymethyl cellulose binder content, 1.0 wt%; sodium tripolyphosphate dispersant content, 0.5 wt%; ball-milling time, 60 min. 相似文献
9.
对金品位为1.55 g/t的氧化矿采用非氰药剂进行浸金的工艺流程,考察了磨矿细度、药剂DZC浓度和浸出时间对金浸出率的影响。确定该金矿适宜的非氰浸出条件:磨矿细度-74μm含量占69.90%、石灰用量4 000g/t、矿浆液固比为2∶1、浸出药剂DZC浓度0.08%、浸出时间8 h,可获得金的浸出率为93.33%的良好指标。表明该氧化金矿在常温常压下,采用非氰浸出工艺是可行的。 相似文献
10.