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对激光选区熔化(Selective laser melting,SLM)成形马氏体时效钢进行固溶及500 ℃时效不同时间的热处理,分析时效时间对其组织性能的影响。结果表明:SLM 18Ni300钢经固溶+时效处理后,其组织为马氏体、逆转变奥氏体和Ni3(Mo, Ti)析出相,随时效时间增加,析出相数量逐渐增加并聚集长大,同时逆转变奥氏体含量增大。随时效时间的增加,其硬度和强度逐渐增加达到峰值后下降,而伸长率不断增加。SLM 18Ni300钢的最佳时效工艺为500 ℃×4 h。 相似文献
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对航天用紧固件TC4钛合金棒材进行固溶时效处理,对棒材不同位置进行显微组织观察、硬度和室温拉伸性能检测。结果表明:TC4钛合金棒材经固溶时效后表面至心部的组织与性能受冷却速度的影响呈现显著差异。固溶时效后的显微组织由稳定的等轴α相、弥散的马氏体α′相和亚稳定β相组成,试样端面上因冷却速度相差不大,次生α相的形态和含量没有明显差异;中部截面上边部至心部的次生α相含量逐渐增多,同时次生α相片层厚度逐渐增大并趋于等轴化。端面上不同位置显微硬度值没有明显差异,但中部截面上由边部至心部的显微硬度值呈总体降低趋势,且中部截面上边部的显微硬度值与端面相差不大。试样心部因固溶过程中冷却缓慢,整体试样的室温拉伸性能明显低于去除心部的试样。 相似文献
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Bingrong Li Yaowu Wei Jinhu Wang Junfeng Chen Nan Li 《Journal of the American Ceramic Society》2021,104(9):4878-4890
Well-sintered CaO granules with hydration resistance are very important for the manufacturing and application of CaO-containing refractories. CaO granules with sol-processed metal oxide protective layers were prepared by granulation and surface treatment. The obtained results indicated that the usage of nano sol greatly improved the hydration resistance of CaO granules, especially when the CaO granules were treated by alumina sol. The promoting effect of nano sols in the sintering processes improved the density of CaO granules. Nanoparticles reacted with lime at lower temperature and a new phase was formed uniformly in the treated layer, which promoted densification of the treated layer. The grain size of CaO granules in the treated layer was increased obviously with the promotion of sintering. Moreover, nanoparticles were favorable for the formation of direct bonding between CaO grains by decreasing the dihedral angle. 相似文献
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Barbora Peltanova Marketa Liskova Jaromir Gumulec Martina Raudenska Hana Holcova Polanska Tomas Vaculovic David Kalfert Marek Grega Jan Plzak Jan Betka Michal Masarik 《International journal of molecular sciences》2021,22(4)
Cancer-associated fibroblasts (CAFs) are one of the most abundant and critical components of the tumor stroma. CAFs can impact many important steps of cancerogenesis and may also influence treatment resistance. Some of these effects need the direct contact of CAFs and cancer cells, while some involve paracrine signals. In this study, we investigated the ability of head and neck squamous cell carcinomas (HNSCC) patient-derived CAFs to promote or inhibit the colony-forming ability of HNSCC cells. The effect of cisplatin on this promoting or inhibiting influence was also studied. The subsequent analysis focused on changes in the expression of genes associated with cancer progression. We found that cisplatin response in model HNSCC cancer cells was modified by coculture with CAFs, was CAF-specific, and different patient-derived CAFs had a different “sensitizing ratio”. Increased expression of VEGFA, PGE2S, COX2, EGFR, and NANOG in cancer cells was characteristic for the increase of resistance. On the other hand, CCL2 expression was associated with sensitizing effect. Significantly higher amounts of cisplatin were found in CAFs derived from patients who subsequently experienced a recurrence. In conclusion, our results showed that CAFs could promote and/or inhibit colony-forming capability and cisplatin resistance in HNSCC cells via paracrine effects and subsequent changes in gene expression of cancer-associated genes in cancer cells. 相似文献
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盐渍土在我国的分布区域非常广泛,尤其是在沿海地区,盐渍土由于自身的盐胀性和腐蚀性会对公路路基造成很大的破坏。因此,公路盐渍土路基的防腐蚀处理和病害防治对保证公路工程的建设质量具有重要意义。基于此,本文对公路盐渍土路基的病害成因进行了简要的分析,并提出了相应的防治策略。 相似文献
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目的 通过控制微弧氧化工艺参数来优化纯锌的耐蚀性,以实现临床降解的可控性.方法 通过设置正向电压、反应时间、占空比、负向电压和分段处理等,在纯锌表面制备微弧氧化膜层.利用扫描电镜(SEM)观察膜层的表面形貌和截面厚度,结合能谱仪(EDS)和X射线衍射仪(XRD)分析膜层元素和相结构,采用表面张力测量仪和电化学极化曲线分析润湿性和耐蚀性.结果 通过提高正向电压,降低占空比,控制处理时间和负向电压,可有效降低膜层孔隙率和腐蚀速度.微弧氧化处理可明显增强试样表面亲水性,分段处理对润湿性和耐蚀性有显著影响.当正向电压为300 V,占空比为10%,反应时间为5 min,负向电压为–100 V时,可获得亲水性好、耐蚀性强的微弧氧化膜层,其孔隙率为10.95%,膜层厚度为5.29μm,腐蚀电流密度达5.74×10–6 A/cm2.结论 微弧氧化处理可明显增强纯锌表面润湿性,可通过调节不同微弧氧化工艺参数改变膜层结构,优化其亲水性和耐蚀性. 相似文献
9.
Jiajia Yan Teng Zhang Haizheng Tao Hongbing Zhan Yuanzheng Yue 《Journal of the American Ceramic Society》2021,104(6):2560-2570
We study the structure, crystallization, and performances of the sealing glasses with the composition (mol.%) of 12Al2O3·8B2O3·40SiO2·40RO (R = Mg, Ca, Sr) for solid oxide fuel cells (SOFCs) before and after isothermal treatment at 700°C, which is within the operation temperature range (600-800°C) of SOFCs. The crystallization behavior has been investigated by differential scanning calorimetry and X-ray diffraction under both dynamic and isothermal conditions. The structural evolution is probed using the Raman and nuclear magnetic resonance spectroscopies. The performances of the sealing glasses are characterized in terms of the coefficient of thermal expansion, the crystallization-induced stress at glass–steel interface. We find that strong crystallization occurs at the operation temperature (700°C) far below the crystallization onset temperature measured by DSC. The structure origin of this anomalous crystallization is discussed in terms of structural heterogeneity of the three studied glasses. We determine the residual stress at the interface between the Ca-containing glass and the steel after isothermal treatment at 700°C for 48 h, but this stress does not lead to falling off the glass layer from the steel. This indicates that this glass is a good candidate to be applied in SOFCs. 相似文献
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