汽轮机叶片用X20Cr13钢的热处理工艺研究

采用正交试验对汽轮机叶片用X20Cr13钢进行了热处理工艺研究，以获得该钢的最佳热处理工艺，并在回火后以不同的速度冷却，以揭示冷却速度对钢的回火脆性的影响。结果，X20Cr13钢的最佳热处理工艺为900℃油淬或风冷，670℃回火，风冷。     

健康长江评价指标体系与标准研究

科学的指标体系和标准是评价河流健康状况的技术依据。根据科学性、代表性、创新性等原则，运用主成分分析法和聚类分析法．构建了健康长江评价指标体系，包括河岸稳定性、河床稳定性等19个定量指标和水系连通性、河岸栖息地状况和珍稀水生动物存活状况3个定性指标；给出了相应指标的量化评价方法，并通过国内外相关研究成果的综合分析．提出了健康长江的评价标准及分类标准，为维持河流健康理论发展提供了新方法。     

高强度钢的Zn—Ti合金新镀层

本文研究了一种Ｚｎ－Ｔｉ合金新镀层，经盐水浸泡、中性盐雾和大气暴露试验结果试验，其耐蚀明显超过镀Ｚｎ层，并与镀Ｃｄ层相近，用缺口持久拉伸试验检验氢脆性，拉伸持续时间超过２００ｈ，达到原航空部部颁标准（ＨＢ５０６７－８５），该镀层适用于高强度钢防护。     

SA299钢冷脆行为的研究

某锅炉厂生产的锅炉汽包,在冬季制造过程中发生破裂,汽包材料为 SA299钢,对断口的初步分析发现为脆性解理断口,据此认为是冷脆破坏。本文依据冷脆特征温度 Tc 的概念对 SA299钢的冷脆行为进行了细致的分析。     

Preparation and characterization of new photoactive polyamides containing 4‐(4‐dimethylaminophenyl)urazole units

4‐(4‐dimethylaminophenyl)‐1,2,4‐triazolidine‐3,5‐dione ( DAPTD ) was prepared from 4‐dimethylaminobenzoic acid in five steps. The compound DAPTD was reacted with excess acetyl chloride in N,N‐dimethylacetamide (DMAc) solution and gave 1,2‐bisacetyl‐4‐[4‐(dimethylaminophenyl)]‐1,2,4‐triazolidine‐3,5‐dione as a model compound. Solution polycondensation reactions of monomer with succinyl chloride (SucC), suberoyl chloride (SubC), and sebacoyl chloride (SebC) were performed under conventional solution polymerization techniques in the presence of triethylamine and pyridine as a catalyst in N‐methylpyrrolidone (NMP) and led to the formation of novel aliphatic polyamides. These novel polyamides have inherent viscosities in the range of 0.09–0.21 dL/g in N,N‐dimethylformamide (DMF) at 25°C. Fluorimetric studies of the model compound as well as polymers were performed. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 947–954, 2007     

Preparation of new poly(amide–imide)s with chiral architectures via direct polyamidation reaction

N‐trimellitylimido‐L ‐methionine ( 3 ) was prepared by reaction of trimellitic anhydride ( 1 ) with ‐L ‐methionine ( 2 ) in acetic acid solution at refluxing temperature. This diacid was reacted with thionyl chloride, and N‐trimellitylimido‐L ‐methionine diacid chloride ( 4 ) was obtained in quantitative yield. The resulting diacid chloride was reacted with p‐aminobenzoic acid in dry acetone and bis(p‐aminobenzoic acid)‐N‐trimellitylimido‐L ‐methionine ( 5 ) was obtained as a novel optically active amide–imide diacid monomer in high yield. The direct polycondensation of amide–imide diacid monomer 5 with several aromatic diamines was carried out with tosyl chloride (TsCl)/pyridine (Py)/dimetheylformamide (DMF) system. The resulting thermally stable poly(amide–imide)s (PAIs) were obtained in good yields and inherent viscosities ranging between 0.24 and 0.46 dL g^?1 and were characterized with FTIR, ¹H NMR, CHN, and TGA techniques. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 1248–1254, 2007     

40CrMnMo活塞杆的断裂

借助于光学显微镜和扫描电镜对 4 0CrMnMo活塞杆的组织、裂纹形态、断口的形貌以及活塞杆横截面的硬度进行研究 ,分析该活塞杆的断裂原因。结果表明 ,断裂的原因是材质不合格 ,存在成分偏析 ,热处理工艺不符合规定以及硫元素含量偏高。这就使得首先在偏析的边缘产生开裂 ,并且在轴向应力的影响下 ,裂纹沿着垂直于轴线的方向扩展 ,直至断裂     

用传递矩阵法计算换热管固有频率

本文分析了用传递矩阵法计算换热管固有频率时的振动方程,并编制程序来求解,通过例子和其它算法结果对比,验证了本方法和程序的可靠性。