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1.
目的 开发环境友好、抗高温耐浓酸的长效缓蚀剂复配体系.方法 采用红外光谱仪对席夫碱基吡啶季铵盐的分子结构进行表征,采用高温高压腐蚀测定仪、吸附等温模型、动力学参数、扫描电镜和量子化学计算,研究了缓蚀剂对N80的缓蚀性能及其吸附机理.结果 在120、140、160℃温度下,随着席夫碱基吡啶季铵盐缓蚀剂(以下简称Shif-PyQA)质量分数的增大,腐蚀速率在低浓度时大幅减小,缓蚀率在低浓度时大幅增加,两者在高浓度时均逐渐趋于平稳.在所测温度范围内,N80在空白溶液中的腐蚀速率远大于在加有Shif-PyQA溶液中的腐蚀速率.随着温度的升高或反应时间的增加,N80的腐蚀速率持续增大,缓蚀率逐渐减小,但减小幅度不大.当温度为120℃、Shif-PyQA质量分数为2%时,N80在20%盐酸中的腐蚀速率为28.77 g/(m2·h),缓蚀率为97.97%;当温度为140℃、Shif-PyQA质量分数为3%时,N80在20%盐酸中的腐蚀速率为37.12 g/(m2·h),缓蚀率为97.71%;当温度为160℃、Shif-PyQA质量分数为4%时,N80在20%盐酸中的腐蚀速率为63.91 g/(m2·h),缓蚀率为96.41%.Shif-PyQA在N80表面的吸附遵循Langmuir等温吸附模型,属于单分子层化学吸附,且N80表面的吸附为自发过程.动力学参数结果表明,添加不同质量分数的Shif-PyQA后,活化能大大增加为74.16~88.43 kJ/mol,属化学吸附.量子化学研究表明,席夫碱基吡啶季铵盐(以下简称PyQ-S)分子可与金属形成多中心的稳定吸附,同时PyQ-S分子接受电子的趋势大于供出电子的趋势.结论 Shif-PyQA在温度为120、140、160℃时,均可达到SY/T 5405—2019中相关指标要求,对N80具有较好的缓蚀作用.  相似文献   
2.
张文烨  尚方信  郭浩 《计算机应用》2021,41(5):1299-1304
浮点数位宽的深度神经网络需要大量的运算资源,这导致大型深度神经网络难以在低算力场景(如边缘计算)上部署。为解决这一问题,提出一种即插即用的神经网络量化方法,以压缩大型神经网络的运算成本,并保持模型性能指标不显著下降。首先,基于Octave卷积将输入特征图的高频和低频成分进行分离;其次,分别对高低频分量应用不同位宽的卷积核进行卷积运算;第三,使用不同位宽的激活函数将高低频卷积结果量化至相应位宽;最后,混合不同精度的特征图来获得该层卷积结果。实验结果证实了所提方法压缩模型的有效性,在CIFAR-10/100数据集上,将模型压缩至1+8位宽时,该方法可保持准确率指标的下降小于3个百分点;在ImageNet数据集上,使用该方法将ResNet50模型压缩至1+4位宽时,其正确率指标仍高于70%。  相似文献   
3.
The transient liquid phase (TLP) bonding of CoCuFeMnNi high entropy alloy (HEA) was studied. The TLP bonding was performed using AWS BNi-2 interlayer at 1050 °C with the TLP bonding time of 20, 60, 180 and 240 min. The effect of bonding time on the joint microstructure was characterized by SEM and EDS. Microstructural results confirmed that complete isothermal solidification occurred approximately at 240 min of bonding time. For samples bonded at 20, 60 and 180 min, athermal solidification zone was formed in the bonding area which included Cr-rich boride and Mn3Si intermetallic compound. For all samples, the γ solid solution was formed in the isothermal solidification zone of the bonding zone. To evaluate the effect of TLP bonding time on mechanical properties of joints, the shear strength and micro-hardness of joints were measured. The results indicated a decrement of micro-hardness in the bonding zone and an increment of micro-hardness in the adjacent zone of joints. The minimum and maximum values of shear strength were 100 and 180 MPa for joints with the bonding time of 20 and 240 min, respectively.  相似文献   
4.
《Ceramics International》2021,47(19):27351-27360
A series of xPbO–(45-x)CuO–55B2O3 glasses (5 ≤ x ≥ 40 mol %) were prepared by the melt-quenching technique. The X-ray diffraction (XRD) patterns of the prepared glasses are found to have amorphous structure. An extensive ultrasonic study has been made to explore the structural role of PbO and CuO in the borate network. Various elastic properties were calculated from the measured data of density and ultrasonic velocity. Ultrasonic velocity and elastic moduli revealed broad humps at about 20 mol % PbO, which are attributed to the borate anomaly. Below 20 mol % PbO, all Pb2+ ions are considered to be entering the borate network as a glass modifier. This results in the transforms the borate network from an open structure to a denser three-dimensional structure due to BO3 → BO4 conversion. Beyond 20 mol, addition of PbO results in the formation of metaborate, pyroborate, and orthoborate units with NBOs. This weakness the glass structure and decrease both ultrasonic velocity and elastic moduli. The elastic properties were predicted and quantitatively analyzed by taking into account the effect of boron coordination number on the compositional and structural parameters involved in Makishima–Mackenzie's theory, ring deformation model and bond compression model. An excellent agreement between the computed theoretical and experimental elastic moduli, micro-harness and Poisson's ratio was achieved for majority of samples.  相似文献   
5.
针对槽钢插打容易引发弯曲失稳的问题,提出了一种沿槽钢设置缀板的构造措施,基于空间配位法提出了一种缀板加劲效应理论,并推导出带缀板槽钢轴压构件的整体稳定性计算方法,为工程中开口槽钢的局部加固优化设计提供了理论依据。算例证明,本方法能够有效量化缀板的位置效应和其自身的尺寸效应,对缀板的数量和板宽、布置方式和构件长度等因素进行稳定临界荷载的规律性分析,计算结果和规律基本合理,充分验证了实际工程的应用效果。  相似文献   
6.
The isothermal extrusion process of hollow aluminium profile was investigated using incremental proportional–integral–derivative (PID) control algorithm and finite element simulations. The range of extrusion speed was determined by considering the maximum extrusion load and production efficiency. By taking the optimal solution temperature of the secondary phase as the target temperature, the extrusion speed–stroke curve for realizing the isothermal extrusion of the aluminium profile was obtained. Results show that in the traditional constant extrusion speed process, the average temperature of the cross-section of the aluminium profile at the die exit rapidly increases and then slowly rises with the increase in ram displacement. As the extrusion speed increases, the temperature difference at the die exit of the profile along the extrusion direction increases. The exit temperature difference between the front and back ends of the extrudate along the extrusion direction obtained by adopting isothermal extrusion is about 6.9 °C. Furthermore, the heat generated by plastic deformation and friction during extrusion is balanced with the heat transfer from the workpiece to the container, porthole die and external environment.  相似文献   
7.
Knowledge of the underlying structural response during deformation processes is essential for understanding the macroscopic mechanical response of glass. Here we present results from cold compression-decompression molecular dynamics (MD) simulations of two multicomponent borosilicate glasses, Borofloat®33 (Boro33) and N-BK7® (N-BK7). Our results suggest that the densification of these two borosilicate glasses involves different types of structural changes. The fraction of permanent densification can be correlated to the change in intermediate-range structure. By performing Voronoi analysis, we quantify the contributions to densification from different cation types in these two multicomponent borosilicate glasses, finding that 3-coordinated cations facilitate the densification process. Higher-coordinated cations are relatively stable and can even show a slight expansion in their Voronoi volume.  相似文献   
8.
特快速暂态过电压(VFTO)是气体绝缘变电站(GIS)中切换隔离开关时产生的特殊电磁暂态现象。VFTO会以传导和辐射方式影响二次设备的正常运行。为探究VFTO对二次设备的干扰特性,文中采用自制的二次侧干扰测量装置对某1 000 kV GIS的电压互感器(PT)二次侧共模干扰进行现场实测。接着,对比了5种时频分析方法的性能,采用其中性能较优的同步压缩小波变换(SWT)对实测波形进行了时频分析。实测结果表明:PT二次侧的共模干扰电压峰峰值最高可达9.65 kV。微脉冲的时频分析结果表明:7.8 MHz频率分量幅值高,且贯穿波形的始终,是PT二次侧干扰的主导频率分量。该分析结果可为GIS中二次设备的电磁抗扰度测试和电磁防护设计提供参考。  相似文献   
9.
10.
According to the circle-packing theorem, the packing efficiency of a hexagonal lattice is higher than an equivalent square tessellation. Consequently, in several contexts, hexagonally sampled images compared to their Cartesian counterparts are better at preserving information content. In this paper, novel mapping techniques alongside the wavelet compression scheme are presented for hexagonal images. Specifically, we introduce two tree-based coding schemes, referred to as SBHex (spirally-mapped branch-coding for hexagonal images) and BBHex (breadth-first block-coding for hexagonal images). Both of these coding schemes respect the geometry of the hexagonal lattice and yield better compression results. Our empirical results show that the proposed algorithms for hexagonal images produce better reconstruction quality at low bits per pixel representations compared to the tree-based coding counterparts for the Cartesian grid.  相似文献   
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