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The evolution and distribution of Al2Sm phase in as-extruded AZ61–xSm (x=0, 1.5, 2.0 and 2.5, mass fraction, %) magnesium alloys during semi-solid isothermal heat treatment were investigated. The results showed that when as-extruded AZ61 magnesium alloys were modified with Sm, the smaller and rounder grains were obtained during semi-solid isothermal heat treatment. When the Sm content is 2.0% (mass fraction), the average size of the globular grains reached the smallest value of 90 μm. Although a few Al2Sm particles existed in the α-Mg grains, most of Al2Sm particles solidified at the edge of the globular grains with the width of ~20 μm. These phenomena are mainly attributed to the forces acting on Al2Sm particles in front of the solid–liquid interface, leading to Al2Sm particles accumulating at the solid–liquid interface and then solidifying at the edge of the globular grains in the quenching process.  相似文献   
3.
王井玲  邢书明 《材料导报》2018,32(Z2):406-409, 434
根据铝与Mg2Si的共晶反应而制备的Mg2Si/Al内生颗粒增强复合材料具有密度小、热稳定性高、增强体分布均匀、切削加工性和成型性能良好等优点,受到了国内外的广泛关注。这一材料的关键问题在于其中的Mg2Si相为小晶面长大模式,尺寸粗大、形貌规则,导致复合材料脆性严重,通常情况下其伸长率不足1.5%。本文对这一材料的变质处理、材料体系、成型与制备技术三方面进行了综述。Mg2Si的变质与细化研究是这一领域最为活跃的方面,研究证明,几乎所有在铝合金中具有变质作用的元素对Mg2Si都有一定的变质作用,其中变质作用最为显著的是稀土元素、碱金属和碱土金属以及B、Sb、Ti、Mn、Ni等微合金化元素。Al/Mg2Si的形貌通过恰当的变质处理,铸态Mg2Si/Al内生颗粒增强复合材料的强度可以达到280 MPa,伸长率可以达到约4%,显著高于基体材料的铸造性能。材料体系的选择方面的研究比较薄弱,主要集中在铝镁硅合金系,Mg2Si含量以15%的近共晶成分为多,过共晶体系中Mg2Si含量最高也没有超过30%。材料成型与改性方面的研究也只是刚刚开始,这一材料无一例外都是凝固成型。研究发现,凝固前的熔体过热处理和搅拌等熔体预处理都可以改善Mg2Si的形貌和尺寸,粗大的初生Mg2Si的平均尺寸可以细化到约40 μm;低过热浇注及凝固过程加压和快冷可以显著改善Mg2Si的尺寸和形貌,在快速凝固条件下,Mg2Si将由小晶面长大模式转变为非小晶面连续长大模式;凝固后的热变形以及热处理也能显著改善其微观组织和性能。内生Mg2Si/Al复合材料的成型技术研究比较薄弱,其中,挤压铸造Mg2Si/Al复合材料具有突出的优势,挤压铸造的A380铝合金-Mg2Si复合材料,平均尺寸由75 μm降为30 μm,形状系数由0.77降为0.22。  相似文献   
4.
由于节能环保以及轻量化的要求,Cu/Al异种金属复合管件被广泛应用于各工业领域,为此探索一种Cu/Al管件间高效可靠的连接技术具有较大应用价值和研究意义。为了探究Cu/Al管半固态钎焊连接机理并优化相关工艺参数,基于新提出的磁脉冲-半固态复合辅助钎焊方法制备了Cu/Al异种金属管件钎焊接头,利用LS-DYNA分析了半固态钎料不同表观粘度参数下外管内壁的受力情况,采用材料力学拉伸试验机,能谱仪和电子探针显微分析仪研究了半固态Zn-Al系钎料固相率及组分对焊接接头质量的影响。结果表明:外管内壁所受压力幅值随着表观粘度的增大而减小,剪切应力随着表观粘度的增大而增大;半固态钎料固相率为0.8时钎料与母材间没有良好冶金结合,固相率为0.4时会导致钎料填充不足的缺陷。在二次放电电压7 kV,半固态Zn-Al钎料固相率为0.6的条件下,磁脉冲-半固态复合辅助钎焊工艺能够实现Cu/Al管的无钎剂有效连接;与Zn-3Al和Zn-22Al相比,Zn-15Al钎料制得的接头综合性能更好,是较为合适的Cu/Al管磁脉冲辅助半固态钎焊用Zn-Al钎料。  相似文献   
5.
As texture properties in novel food categories have a crucial role in consumer acceptance, mouthfeel profile of different plant-based yogurt-like semi-solid products were studied and compared to dairy yogurts. Mouthfeel properties of five plant-based yogurt-like products and two dairy yogurts were analyzed using temporal dominance of sensations (TDS) with consumers (n = 87). The attributes evaluated were thick, thin, creamy, watery, sticky, and foamy. Following TDS, overall liking and mouthfeel liking were evaluated using a 7-point hedonic scale. Temporal drivers of mouthfeel liking were studied using correspondence analysis and penalty-lift analysis with different time points during mastication. For penalty-lift analysis TDS data was analyzed as check-all-that-apply (CATA) data. Results from the present work show that mouthfeel perception in non-dairy yogurt alternatives is a dynamic process. Attributes typically used to describe dairy yogurts are also relevant for describing non-dairy yogurt alternatives. Yogurt alternatives and dairy yogurts can be similar and equally liked by their mouthfeel profile. Temporal drivers of liking in plant-based products are thickness and creaminess and temporal drivers of disliking are thinness and wateriness. In this study, the first dominant attributes were found to have a stronger impact on mouthfeel liking than the dominant attributes perceived later during mastication.  相似文献   
6.
研究了传统液态挤压铸造与半固态挤压铸造成形ZL104铝合金连杆的充填状态、微观组织及力学性能。结果表明:传统液态挤压铸造成形连杆充填饱满,但其抗拉强度及伸长率低于半固态挤压铸造成形连杆。对于半固态挤压铸造成形,浇注温度高于565℃时,铸件充填性能良好;平均晶粒尺寸及形状因子随浇注温度的升高而逐渐增大;连杆抗拉强度及伸长率先增加后减小。挤压压力高于25MPa时,铸件均充填饱满;挤压压力升高,平均晶粒尺寸不断减小且形状因子不断增大,连杆机械性能不断提高。模具预热温度升高,平均晶粒尺寸和形状因子不断增大,连杆机械性能逐渐提高。但当模具预热温度超过300℃时,平均晶粒尺寸进一步增大而其形状因子减小,导致连杆的机械性能下降。  相似文献   
7.
The hot cracking tendency of 7075 semi-solid alloy under different conditions was studied by critical diameter method. The experiment and simulation results show that the dendrite arms of the rod grow from the edge to the center. The smaller the diameter of the rod is, the more obvious the directional growth of dendrite is, and the greater the tendency of hot cracking is. Compared with ordinary melt, for semi-solid slurry, increasing mould temperature or decreasing pouring temperature can significantly decrease hot cracking tendency of 7075 alloy, decreasing hot cracking grade from 256 to 100 mm2. Furthermore, based on the RDG criterion, the effects of solidification conditions on the hot cracking tendency were discussed combined with simulation. At the same time, the application and development of RDG criterion were also researched.  相似文献   
8.
Cylindrical samples of Ni-based GH4037 alloy were compressed at solid temperatures (1200, 1250 and 1300 °C) and semi-solid temperatures (1340, 1350, 1360, 1370 and 1380 °C) with different strain rates of 0.01, 0.1 and 1 s−1. High temperature deformation behavior and microstructure evolution of GH4037 alloy were investigated. The results indicated that flow stress decreased rapidly at semi-solid temperatures compared to that at solid temperatures. Besides, the flow stress continued to increase after reaching the initial peak stress at semi-solid temperatures when the strain rate was 1 s−1. With increasing the deformation temperature, the size of initial solid grains and recrystallized grains increased. At semi-solid temperatures, the grains were equiaxed, and liquid phase existed at the grain boundaries and inside the grains. Discontinuous dynamic recrystallization (DDRX) characterized by grain boundary bulging was the main nucleation mechanism for GH4037 alloy.  相似文献   
9.
7075 aluminum alloy was used to obtain elbow parts by complex thixoextrusion and the microstructure evolution and mechanical properties during this process were studied by SEM, TEM and other analytical methods. The results show that different parts in 7075 aluminum alloy show quite different microstructures. The microstructure of the thin walls formed by back-extrusion is stratified, and the bottom of the parts formed by angular extrusion is obviously deformed. Shear forces contribute to the crushing of grains and the coarse second phase. The main strengthening phases in the material are η phase and E phase, whose amounts greatly decrease during heating to semi-solid and thixoextrusion. After heat treatment, they can precipitate evenly to improve the mechanical properties of the material. The average tensile strength of whole part after thixoextrusion and heat treatment is 485.49 MPa, while the average elongation is 5.49%.  相似文献   
10.
以新型阻燃钛合金Ti14 (α+Ti2Cu)为对象,研究了合金在不同温度半固态锻造过程中的偏析和偏聚现象及由此导致的变形机制的变化。结果表明,半固态温度影响液相含量和分布,随着温度的升高液相在晶界由不连续分布转变为连续分布析出,并最终形成了网状结构分布。锻造过程中由于液相和应力的共同作用出现了宏观偏析现象,液相在压力作用下的流动在晶界处产生了宏观液相/固相分离现象,靠近试样中心固相离子集中;这种现象导致了锻造过程中变形机制的变化,中心区仍旧是固相粒子的塑性变形为主变形机制,靠近试样外边缘主变形机制转变为固相粒子的相对滑移,通过唯象模型对其过程进行讨论  相似文献   
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