Synthesis of amphiphilic magnetic microspheres by dispersion copolymerization of styrene and poly(ethylene oxide) macromonomer

Amphiphilic magnetic microspheres ranging in diameter from 5 to 100 µm were prepared by dispersion copolymerization of styrene and poly(ethylene oxide) vinylbenzyl (PEO‐VB) macromonomer (MPEO) in the presence of Fe₃O₄ magnetic fluid. The effects of various polymerization parameters on the average particle size were systematically investigated. The average particle size was found to increase with increasing styrene concentration and initiator concentration. It also increased with decreasing stabilizer concentration and molecular weight of MPEO. The content of the hydroxyl groups localized in the microspheres ranged from 0.01 to 0.2 mmol g^?1. © 2003 Society of Chemical Industry     

新设备技术在催化裂化装置上的应用

文章介绍了近年来在催化裂化装置上应用的新设备、新技术,如BY型旋风分离器、BSX型旋分式三级旋风分离器、上下拱型三级旋风分离器、下拱型三级旋风分离器、SHS“自蔓延”技术、SWY外取热器、BWJ型喷嘴、自流浇注料、Actehem高耐磨衬里、弓形钢丝纤维、侧拉环锚固钉、分体可拆人孔等的结构特点及实际应用情况。     

波动方程数值模拟的隐式差分法

在有限差分波动方程数值模拟中,通常采用高阶差分方法来提高空间导数的数值逼近精度,以实现降低数值频散,提高数值模拟精度的目的。首先对差分频散进行了理论分析;然后讨论了估计一阶空间导数的隐式差分格式,并与通常采用的高阶精度显式差分格式进行了对比分析,结果表明,隐式差分格式能够在更宽的波数范围使差分频散控制在可接受的水平,如8阶精度的显式差分格式所适应的波数带宽约为O．55kmax,而隐式差分格式所适应的波数带宽约为0．7kmax;最后通过模型试算,对隐式差分格式的有效性进行了验证。模拟结果表明,用隐式差分格式在一定程度上降低了差分频散,提高了模拟精度。     

柳钢新建氧化球团工程的设计特点

介绍了柳钢新建120万t／a链篦机-回转窑氧化球团工程的主要设计特点。该工程是我国第一条自行设计、设备国产化和采用清洁气体能源的链篦机-回转窑生产线。它的顺利投产，标志着我国炼铁炉料生产技术有了一个新的进步。     

16×10.7 Gb/s 1 600 km普通单模光纤环路传输研究

利用双折射光纤环设计了可调功率均衡滤波器,实现了16路16×10.7 Gb/s NRZ码、超过1 600 km常规单模光纤(SMF)的系统传输及性能测试,信道误码率均小于3×10-5(FEC纠错前).数值仿真并实验研究了对单环长度240 km、损耗超过80 dB的环路16路10.7 Gb/s波分复用(WDM)系统传输的优化.传输7圈后,功率均衡器降低了信道功率不平坦度超过5 dBm.     

移动式宽频带高产额中子发生器

多用途中子发生器有着广阔的市场和应用领域 ,文章对移动式宽频带高产额中子发生器 ,在设计制造过程中所涉及到的技术难点 :绝缘尺寸小、频率适应范围宽、为中子管提供靶压的高压负载特性好等作了技术分析 ,使多用途中子发生器在更广阔的范围内应用 ,提供了广阔前景。     

A Topological Implementation for Motion Planning of a Robotic Arm

An efficient path planning algorithm based on topologic method is presented in this paper.The collision free path planning for three-joint robotic arm consists of three parts:partition of C-space,construction of CN and search for a path in CN.We mainly solved the problems of partitioning the C-space and undging the connectivity between connected blocks,etc.For the motion planning of a robotic arm with a gripper,we developed the concepts of global planning and local planning,and discussed the basic factors for constructing the planning system.In the paper,some evaluation and analysis of the complexity and reliability of the algorithm are given,together with some ideas to improve the efficiency and increase the reliability.At last,some experimental results are pesented to show the efficency and accuracy of the algorithm.     

预分解窑燃无烟煤生产水泥熟料技术及其应用

无烟煤着火温度高、燃烧速度低、燃烬时间长,故一直难以用作回转窑燃料.20世纪90年代,南京院率先进行了回转窑燃无烟煤生产的研究开发.经10多年的努力,解决了所有的技术问题,开发了配套的专有装备,已在福建三德水泥厂、福建南平水泥公司、龙岩春池集团、广西鱼峰水泥公司等厂的多条生产线上应用并获巨大成功.     

Processing of Yttria-Alumina Coated Silicon Nitride Slips by Slip Casting

Si₃N₄powders coated with 6 wt% Y₂O₃and 4 wt% Al₂O₃were prepared by coprecipitation. The resulting powders were dispersed in water at different pH values and with addition of various amounts of ammonium polyacrylate (NH₄PA) to produce 32 vol% slips. The influence of the amount of NH₄PA solution added and pH on the rheological properties of 32 vol% coated Si₃N₄slips were studied. In addition, the sintered density of cast samples was determined and related to the degree of slip dispersion. The adsorption of the NH₄PA on the coated particle surface was rather high and the surface became saturated near 0.86 mg/m²at pH 9.2. High NH₄PA concentrations (1.7–3 wt%) were necessary to obtain well dispersed 32 vol% coated Si₃N₄slips at pH 9.2. The best stabilization was obtained with the addition of 2.3 wt% NH₄PA; in this condition, the viscosity reached a minimum value of 35 mPa.s at 100 s^–1. The slip viscosity increased with increasing pH from 9.2 to 10.2. Slips with low viscosities gave a more dense packing of cast samples and consequently higher sintered density values.     

准噶尔盆地侏罗系储集层的基本特征及其主控因素分析

从描述储集层基本特征、分析储集层性质的主控因素、建立储集层成因模式和评价、预测储集层性质这 4个层次 ,研究准噶尔盆地重点勘探目标区的侏罗系储集层。系统总结侏罗系储集层岩石学特征 ,认为成岩压实作用强弱是控制储集层性质的关键因素 ;指出相对优质储集层均为剩余原生粒间孔隙型储集层 ,溶蚀作用对渗透率贡献小 ;非煤系储集层的孔隙保存条件明显比煤系储集层好 ,这是三工河组、头屯河组和吐谷鲁群的物性普遍优于八道湾组和西山窑组的原因。在确定储集层性质的控制因素和控制机理基础上 ,建立了煤系和非煤系两大类储集层的成因 演化模型。在上述研究的基础上 ,分地区、分层位评价了储集层 ,并预测了不同渗透率储集层的深度界线及相对优质储集层的平面分布。图 6参 10