Influence of the SiC matrix introduction time on the microstructure and mechanical properties of Cf/Hf0.5Zr0.5C-SiC ultra-high temperature composites

C_f/Hf_0.5Zr_0.5C-SiC composites were prepared by introducing Hf_0.5Zr_0.5C matrix (11 cycles) and SiC matrix (9 cycles) into the carbon cloth preform through precursor impregnation and pyrolysis (PIP) process. The influence of the introduction time of SiC matrix on the microstructure and mechanical properties of C_f/Hf_0.5Zr_0.5C-SiC composites was studied, and the results show that with the increase of the PIP cycles of the SiC matrix introduced before Hf_0.5Zr_0.5C matrix, the composite open porosity decreased, and the flexural strength and modulus presented an obvious upward trend. CS45 sample, which has 4 cycles of PIP SiC introduced in advance, has the highest flexural strength, flexural modulus and interfacial shear strength of 402.73 ± 35.73 MPa, 56.92 ± 3.97 GPa and 100.88 ± 7.79 MPa, respectively. Hf_0.5Zr_0.5C matrix has a loose and porous structure, so when more SiC matrix was introduced in advance, its covering effect on the surface of fibers led to less intra-bundle pores and thusly denser composite structure, and due to the compactness of SiC matrix, better overall bonding of fiber, interface and matrix was achieved, as well as better load transfer effect, which led to obvious interfacial debonding and cracking based on the in-situ SEM observation during flexural tests. While in the sample without pre-introduced SiC, the cracking occurred mainly between the interface and porous matrix and the overall performance of the material was poor.     

超声波辅助水蒸气提取柠檬精油工艺优化及成分分析

以柠檬果皮为原料,研究超声波辅助水蒸气蒸馏提取柠檬精油的最佳工艺条件。在单因素试验基础上,选取超声波功率、料液比、超声波时间及蒸馏时间为影响因素,以提取率为响应值,设计响应面试验;通过气相色谱—质谱法对柠檬精油的化学组分进行检测,采用扫描电镜对柠檬皮的微观结构进行观察。结果表明,最佳工艺条件为:超声波功率320W、液料比15.51(mL/g)、超声波时间36min、蒸馏时间140min,提取率可达1.97%;柠檬精油中共鉴定出26种化学成分,占总成分的96.16%,主要成分为柠檬烯;扫描电镜观察表明,超声波显著破坏原料细胞结构,促进了精油的快速释放。该工艺与水蒸气蒸馏提取相比,提取率相近,但明显缩短了提取时间。超声波辅助提取柠檬精油是一种有效的提取方法。     

Asynchronous control for two‐dimensional hidden Markovian jump systems with partly known mode observation conditional probabilities

This study focuses on the asynchronous control problem for two‐dimensional discrete‐time hidden Markovian jump systems where the mode observation conditional probability matrix is partly known. Considering the original system modes are invisible, the observed modes emitted from an observer serve as an alternative for stability analysis and controller design where a mode observation conditional probability matrix is constructed to characterize the emission between system modes and observed modes. Specially, only partly known information of the mode observation conditional probability matrix is accessible. With the introduction of the free‐connection weighting matrices, the asymptotic mean square stability criterion is firstly derived based on Lyapunov method. This introduction provides a further degree of relaxation and less conservatism is therefore achieved. Secondly, we present synthesis conditions for asynchronous state feedback controller design given in terms of a set of interconnected linear matrix inequalities. Moreover, cluster concept based on the partitions of observed modes is adopted which helps to decrease the number of controllers and simplify the design complexity. A numerical example, regarding the cases with and without clustering of the observed modes, is presented to illustrate the effectiveness of the proposed method.     

干扰床分选机分选磷矿规律的试验研究

文中分析了我国丰富的磷矿资源及传统的分选磷矿方法,阐述了研究干扰床分选机分选磷矿的规律具有重要意义,研究设计了试验室干扰床分选机分选系统,试验采用宜昌某磷矿原矿中0~3.0mm粒度的粗矿泥进行试验研究,分析了干扰床分选机分选磷矿的规律,找出了分选最佳工况点并进行了对比曲线分析,论证了显著的经济效益和广阔的市场前景。     

特高砂砾石面板坝流变效应及面板防裂措施

针对高面板坝后期变形导致的面板破坏问题,采用大型室内试验测定了大石峡筑坝料流变力学特性,重点研究了后期流变效应对坝体、防渗体应力变形的影响。评估了各期面板浇筑前坝体沉降速率,复核了面板浇筑前预沉降时间的合理性。研究结果表明,该坝各期面板浇筑前设置的预沉降期可将坝顶沉降率控制在5mm/月以内。大坝蓄水运行后面板应力,尤其是轴向应力,较初次蓄水增加明显,存在挤压破坏的风险。论证了在面板受压区设置柔性缝的面板应力改善措施,结果表明该工程措施对削减面板轴向压应力效果明显。总体上,250m级的特高砂砾石面板坝坝体和防渗体应力变形能满足安全控制要求,通过合理的工程措施可保证大坝施工与运行安全。     

海底管道固结沉降分析

介绍海底管道沉降的发展过程。基于太沙基一维固结理论，以Boussinesq应力解的分层总和法完成海底管道在黏性土质海床下固结沉降量的计算。为验证计算结果的准确性，借助有限元分析软件Abaqus对某工程实例进行数值模拟求解，结论表明公式计算与数值求解得到的结果具有较好的吻合性。研究内容对海底管道的设计与分析具有参考意义。     

软土地区管幕群顶管施工地面沉降监测与分析

依托上海14号线桂桥路站管幕段实例工程,对管幕群顶管顶进施工过程地面沉降情况进行监测,分析群顶管施工对地面沉降的影响,在此过程中对本工程采用水土分算或合算进行讨论。根据顶进过程实际工况和监测数据,分析管幕群顶管施工影响地面的原因,提出相应控制措施。结果表明:①管幕群顶管施工引起最大地面沉降出现在始发井出加固区区域;②在本工程中采用水土合算计算正面土压力较为符合实际情况;③管幕群顶管施工过程中影响地面变形的因素主要包括前舱压力、顶进速度、洞门止水、管壁摩擦和同步注浆等方面。