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这是一篇冶金工程领域的论文。以稀土抛光粉废料为原料,通过正交实验设计,首先进行废料与硫酸铵和硫酸氢铵混合物的焙烧实验,使稀土氧化物转化为硫酸盐。实验考查3个因素,每个因素取3个水平,选用正交表L9(34),安排了9个实验,统计分析实验结果:焙烧温度取480 ℃,焙烧时间取3 h,质量比取1.8∶1。然后在酸浸液中加入0.2%的硫脲作还原剂,研究用稀硫酸从焙烧固相中浸出稀土的工艺条件。实验考查4个因素,每个因素取4个水平,选用正交表L16(45),安排了16个实验,统计分析实验结果:酸浸温度取90 ℃,硫酸浓度取0.5 mol/L,浸出时间取4 h,稀硫酸与焙烧固相的液固比(质量)取4:1,稀土的浸出率可达97.8%~98.0%。 相似文献
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针对某含碳超显微包裹体难浸金矿石,分别开展了常规氰化浸出探索试验、优先浮碳再细磨浮金探索试验、细磨焙烧预处理再氰化提金探索试验。试验结果表明,采用常规氰化时金的浸出率仅为14.01%,即使进行脱碳处理后,金浮选的回收率也仅达到51.82%。该类型矿石若要解决受含碳和包裹金影响的问题,有效的途径之一就是进行焙烧预处理。矿石经细磨后,采用“焙烧-水洗-碱浸-氰化”的工艺流程,金的浸出率可达87.57%,从而使金得到了较好的回收。 相似文献
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Effects of various roasting conditions on antioxidant properties of five Theobroma cacao L. varieties were investigated. The cocoa beans were roasted at four different temperatures (110–150°C) and three different air humidities (0.3–5.0%). The raw cocoa beans were characterized by high antioxidant activities. The antioxidant properties of the roasted cocoa beans varied markedly among the analyzed cultivars and geographical regions and were affected by roasting conditions. Generally, cocoa beans of the cv. Forastero from Brazil exhibited higher total phenolic content, free radical scavenging activity, and metal chelating ability than samples of the other analyzed cocoa varieties. Roasting at 110°C caused negligible changes in total phenolics content and antioxidant activity of cocoa beans, while almost all samples tended to have lower antioxidant potential when roasting temperature increased. The air humidity used in roasting did not affect the total phenolics content and antioxidant activity for lowest roasting temperature (110°C). Moreover, the obtained results revealed that thermal processing at the higher temperatures and elevated air humidity resulted in the higher antioxidant capacities. It was also found that the ferrous ion chelating activity of cocoa beans increased with the roasting temperature (in the range from 110 to 150°C), with the exception of cv. Trinitario from Papua New Guinea. The data showed that roasting at lower temperatures with humid air are more favorable in terms of preserving the bioactivity of roasted cocoa beans. 相似文献
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As the sulfide ore deposits become less economically viable as a source of nickel, increasing attention is being paid to the nickeliferous laterite ores. However, in contrast to the sulfide ores, these oxide ores cannot be as easily concentrated by current technologies. Consequently, considerable research effort is being directed at developing new techniques for beneficiating the nickeliferous laterites. The pyrometallurgical production of a high-grade ferronickel alloy using a low cost carbonaceous reductant at relatively low temperatures is particularly attractive. In the current research, a thermodynamic model has been developed to aid in the understanding of the carbothermic reduction roasting process as a potential upgrading method for the nickeliferous limonitic laterite ores. The effects of process parameters such as temperature and reductant to ore ratio on the grade of the ferronickel alloy produced and the nickel recovery in the alloy have been studied. The thermodynamic predictions are shown to be in general agreement with the experimental results currently available in the literature. 相似文献
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Formation of Benzo(a)pyrene in Sesame Seeds During the Roasting Process for Production of Sesame Seed Oil 下载免费PDF全文
Weiwei Cheng Guoqin Liu Xuede Wang Xinqi Liu Bingge Liu 《Journal of the American Oil Chemists' Society》2015,92(11-12):1725-1733
The main aim of this research was to enhance the understanding of the formation mechanisms of benzo(a)pyrene (BaP) during roasting of sesame seeds (SS). BaP levels in hot‐ and cold‐pressed sesame seed oil (SSO) were evaluated to correlate oil technology and BaP formation. Extracted principal components from SS were roasted either singly or in mixtures at 230 °C for 30 min. BaP was measured by HPLC with fluorescence detection. The results showed that BaP levels in hot‐pressed SSO were significantly higher than those in cold‐pressed SSO (p < 0.05), BaP formation mostly occurred during SS roasting and increased with roasting temperature (between 80 and 280 °C) and time (from 10 to 50 min). Furthermore, the BaP level in the roasted hulled SS (3.64 μg/kg) was higher than it was in roasted whole SS (1.63 μg/kg). The maximum BaP level observed (5.03 μg/kg) was detected in a roasted mixture of SS protein and SSO. The addition of sesame protein to protein‐free SSO promoted the formation of BaP, which suggests that the pyrolysis products of protein and triacylglycerols are probably important precursors in BaP formation. 相似文献
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阐述了影响煤系硬质高岭土矿用于造纸涂料的主要因素和解决途径,并以四川普格高岭土矿加工利用研究为例,论述了该矿的矿石性质、加工工艺及其特点。通过研究最终获得了高档级涂布原料、中档级涂布原料和造纸填料三种产品,并进行了产品应用试验和技术经济分析。 相似文献
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