一种可用于可调谐环行Ti：Al_2O_3激光器的宽带单向器

本文介绍一种宽带单向器的原理及设计。选用ＴＧＧ作磁旋光介质，旋光石英晶片作补偿片，所设计的色散补偿型宽带单向器预计可在７００～１０００ｎｍ波长范围内实现环行激光腔中的单向行波运行；将其应用在可调谐环行Ｔｉ：Ａｌ２Ｏ３激光器中，获得了良好的实验结果。     

Thermophysical properties of a Ti–44%Al–8%Nb–1%B alloy in the solid and molten states

The families of titanium aluminide intermetallic alloys have attractive high temperature mechanical properties which make them potential candidate materials for a wide range of applications, particularly in the aeronautic and automobile sectors. The development of appropriate manufacturing techniques is an essential stage in the engineering exploitation of these materials, e.g., Induction Skull Melting is one of the techniques which needs to be optimised for the casting of titanium aluminides. Research is underway to develop a computer model of this process but data are required for the key thermophysical properties. Pulse-heating techniques have been used to measure properties for the Ti–44Al–8Nb–1B system. Rectangular samples have been prepared and are resistively heated as part of a fast capacitor discharge circuit. Time-resolved measurements with sub-μs resolution of currents through the specimen were made with a Pearson probe current monitor using the induction principle. Voltages across the specimen were determined with knife-edge contacts and voltage dividers, and radiance temperatures of the sample were measured with a pyrometer. These measurements allow the calculation of specific heat and dependencies between enthalpy, electrical resistivity and temperature of the alloy up into the liquid phase. Data for thermal diffusivity have been obtained by using the Wiedeman–Franz relation. The results are compared with those obtained using DSC and the four-probe method to measure the temperature dependence of the resistivity.     

TiB2表面渗层材料的研究和应用现状

综述了国内外钛金属表面渗硼强化技术的研究及其应用现状,总结并对比了钛金属渗硼方法及相应渗层的组织结构和力学性能,提出了相应的改进方向,重点讨论了Ti-B系扩散机理研究成果,归纳出Ti-B系互扩散反应的基本规律,最后展望了TiB2表面渗硼材料的应用前景.     

Annealing process of fine grained co-stabilised (Y,Mg)-PSZ/MgAl2O4 ceramics

Abstract

Co-stabilised (Y,Mg) partially stabilised zirconia (PSZ) ceramics with MgAl₂O₄ spinel additions were produced, with industrial zirconia as the main starting material. Powders were prepared using a mechanical milling–mixing process. The effect of the annealing process on the mechanical properties, phase compositions, and microstructure of fine grained PSZ ceramics was investigated.     

Studies about Microstructures and Mechanical Properties of Ti(C,N) Ceramic Material Using Different Solvents

Abstract

Ti(C,N) ceramic materail plays an important role in the field of material processing due to their good mechanical properties and thermal stability. In this experiment, Ti(C,N) powders were successfully prepared by solvothermal and high-temperature calcining method, using TiOSO₄ and C₃H₆N₆ as raw material, and n-propanol and ethylene glycol as solvents. The microstructure of Ti(C,N) powders were characterized by X-ray diffraction and field emission scanning electron microscope, and their hardness were tested by vickers microhardness tester. The microstructure and mechanical properties of Ti(C,N) powders using two different solvents were investigated comparatively. Ti(C,N) powders prepared using n-propanol with a size of about 20–30?μm can reach the maximum hardness of 660 HV after sintering. Ti(C,N) powders prepared using ethylene glycol with size range of 3?μm to 5?μm come up to the maximum hardness of 889 HV. The different mechanism of solvents in preparation of Ti(C,N) ceramic material was discussed.     

The influence of temporary hydrogenation on ECAP formability and low cycle fatigue life of CP titanium

It is generally believed that thermo-hydrogen processing has a beneficial effect on tensile ductility and fatigue properties of titanium. This study was concerned with investigating whether this also applies to titanium of commercial purity (CP) with an ultrafine-grained structure obtained by equal-channel angular pressing (ECAP). It was shown that despite the possibility to manipulate the microstructure of titanium the thermo-hydrogen processing offers, temporary hydrogenation was not able to improve ductility and low cycle fatigue life of CP titanium over the levels achievable by straight ECAP.     

高效全固化钛宝石腔内倍频蓝光和四倍频紫外激光器的研究

用半导体抽运的Q开关YLF倍频激光器抽运钛宝石晶体，在平凹腔内加入组合的石英双折射滤光片压缩线宽，用LBO晶体腔内激发二次谐波，聚焦到BBO上产生四次谐波深紫外光。在抽运功率3．8w时，输出610mW．416nm蓝光。用长焦距的透镜聚焦二次谐波．得到64mW，208nm的紫外激光。基频光的谱线宽度是决定倍频效率的关键因素。实验观察到激光器的频谱宽度与双折射滤光片的带宽有一个数量级的差别，考虑到模式竞争和增益饱和效应，数值模拟了加入双折射滤光片后的钛宝石激光器的实际线宽，结果与实验中测量的数据基本一致。实验还分析了基频光的线宽对二次谐波效率的影响、二次谐波的线宽对四次谐波效率的影响、基频光的波长对四次谐波激发效率的影响。     

钛合金的激光气体氮化研究

本研究了Ｔｉ－６Ａｌ－４Ｖ合金的激光气体氮化，试验结果表明在激光功率密度大于５．０×１０＾４Ｗ／ｃｍ＾２，氮气压力为０．４ＭＰａ，通过激光辐射可在Ｔｉ－６Ａｌ－４Ｖ合金表面形成氮化钛。其氮化层的厚度为４００μｍ。在氮化层中存在大量氮化钛枝晶。其平均二次枝晶间距为１．７７μｍ。细小的氮化钛枝晶均匀地分布在氮化层中。最后测定和分析了氮化层的显微组织、相成份和显微硬度，并讨论了氮化钛的形成过程。     

激光熔覆制备原位自生增强颗粒复合涂层

采用高能束横流HL-5000型CO2激光器在铸钢表面熔覆了含有碳氮化钛增强粒子的铁基熔覆层。利用X射线衍射(XRD)和能谱EDAX对熔覆层进行了分析, 并采用光学显微硬度计对熔覆层的硬度进行了测试。利用金相显微镜(OM)和扫描电镜(SEM)对激光熔覆层的微观组织进行了研究。结果表明: Ti(C0.3N0.7)可以通过原位反应合成, 新的颗粒状强化相Ti(C0.3N0.7)的形貌特征多呈不规则形状, 弥散分布在熔覆层基体中。熔覆层与母材形成良好的冶金结合, 熔覆层内为方向性强的胞状树枝晶, 晶粒细小。熔覆层的显微硬度HV0.3达到730～850。