稳产国Ⅵ柴油并兼产喷气燃料技术方案的工业应用

介绍了浙江石油化工有限公司新建的3 Mt/a柴油加氢精制装置，其配套使用中国石化石油化工科学研究院有限公司开发的催化剂级配技术，并实施了可根据原料供应及市场产品需求情况灵活调整切换的2种生产技术方案。1 a的安稳生产运行结果表明:该装置以直馏柴油为主原料，通过分馏塔的馏分切割及其侧线抽出，实现了稳产国Ⅵ柴油并兼产喷气燃料技术方案的工业化应用；在实施以兼产喷气燃料为主的生产技术方案时，通过调整常一线柴油的掺炼量，不仅可以生产含硫量小于10.0 μg/g的精制柴油产品，同时兼产所得到的喷气燃料产品含硫量小于0.5 μg/g，赛波特颜色号值大于30；在实施主产精制柴油组分方案时，通过掺炼质量分数为20%~40%的催化柴油，并使所提炼得到的精制柴油组分含硫量小于6.0 μg/g的前提下，这些精制柴油组分产品既可直接作为满足国Ⅵ柴油产品出厂待售，也可作为柴油调和组分储存待用于产品的进一步优化。     

A new systematic firefly algorithm for forecasting the durability of reinforced recycled aggregate concrete

This study presents a new systematic algorithm to optimize the durability of reinforced recycled aggregate concrete. The proposed algorithm integrates machine learning with a new version of the firefly algorithm called chaotic based firefly algorithm (CFA) to evolve a rational and efficient predictive model. The CFA optimizer is augmented with chaotic maps and Lévy flight to improve the firefly performance in forecasting the chloride penetrability of strengthened recycled aggregate concrete (RAC). A comprehensive and credible database of distinctive chloride migration coefficient results is used to establish the developed algorithm. A dataset composite of nine effective parameters, including concrete components and fundamental characteristics of recycled aggregate (RA), is used as input to predict the migration coefficient of strengthened RAC as output. k-fold cross validation algorithm is utilized to validate the hybrid algorithm. Three numerical benchmark analyses are applied to prove the superiority and applicability of the CFA algorithm in predicting chloride penetrability. Results show that the developed CFA approach significantly outperforms the firefly algorithm on almost tested functions and demonstrates powerful prediction. In addition, the proposed strategy can be an active tool to recognize the contradictions in the experimental results and can be especially beneficial for assessing the chloride resistance of RAC.     

Fatigue behavior and damage evolution of SiC/SiC composites under high-temperature anaerobic cyclic loading

In the present study, the fatigue behavior and damage evolution of SiC/SiC minicomposites at elevated temperatures in oxygen-free environment are investigated which are important for their application and are still unclear. The high-temperature fatigue test platform is developed and the fatigue stress-life curve and the stress-strain response are obtained. The test result shows that the life of the material at elevated temperature is shorter than that at room temperature under the same stress level. Moreover, the hysteresis loop width and the residual strain increase with the increasing of the cycles while the hysteresis modulus decreases during the fatigue cycling. The evolution process of matrix cracks is observed using the real-time remote detection system. It is found that matrix cracking is insensitive to the cyclic loading which is similar to room temperature and is due to that the degeneration of the interfacial shear stress reduces the area of high stress in matrix. The fiber/matrix interfacial shear stress under different cycles is determined based on the fatigue modulus of each hysteresis loop. The result shows a fatigue enhancement phenomenon for the interface which is not observed at room temperature.     

Study of the influence of notch radii and temperature on the probability of failure: A methodology to perform a combined assessment

The fracture assessment of notched components based on cracked components approaches leads to over‐conservative failure predictions. In the research literature, several approaches are proposed to overcome this problem using an apparent fracture toughness, . Nevertheless, most of these approaches are based on deterministic assumptions despite the large and variable scatter exhibited by for different notch radii (ρ) or temperatures (T). This paper proposes a methodology for deriving a probabilistic field including the effect of temperature on the failure of notched components. First, the theory of critical distances is applied to transform each apparent fracture toughness into the equivalent fracture toughness for ρ = 0. Then, the temperature is supposed to act as a scale effect in the Weibull cumulative distribution function of the equivalent fracture toughness, and the corresponding scale effect function is derived. Finally, the applicability of the proposed methodology is illustrated by an example using two ferritic‐pearlitic steels: S275JR and S355J2.     

一种新型毛羽检测装置的设计开发

设计了一种新型毛羽检测装置,对其结构组成进行了重新设计,主要包括传动箱与传动装置、收纱框、横动装置、检测盒、预张力加压装置,以及导纱组件与伸缩组件等。与现有的纱线毛羽检测装置相比,该装置结构简单合理,操作方便快捷,不会出现缠纱现象,可适用于不同大小的纱管进行毛羽检测,检测结果精确,并且能够在检测纱线毛羽的同时检测纱线的线密度,节约纱线,减少浪费。     

锡盟地区小尾寒羊副产物营养成分分析与评价

以锡盟地区小尾寒羊的心、肝、脾、肺、肾、大肠、小肠、胃（瘤胃、网胃、瓣胃、皱胃）及血液等副产物为研究对象，对其常规营养成分、氨基酸、脂肪酸以及矿物质含量进行分析与评价。结果表明：锡盟地区小尾寒羊各副产物营养成分含量（鲜质量分数）为水分含量68.86%～83.62%、蛋白质含量11.10%～19.92%、脂肪含量0.19%～16.93%、灰分含量0.45%～3.82%；各副产物经酸水解处理后测定，含天冬氨酸、亮氨酸、赖氨酸等17 种氨基酸，其中包含人体必需的7 种氨基酸，必需氨基酸占氨基酸总量的34.44%～44.35%，且谷氨酸、天冬氨酸、亮氨酸等含量丰富；各副产物中不饱和脂肪酸含量（除羊血8.26%外）为35.56%～56.09%，其中以单不饱和脂肪酸为主，网胃、瓣胃、皱胃、大肠、小肠中油酸含量均在30%以上，且网胃、肝脏、肺脏中亚油酸含量较高；各副产物中含有多种微量元素，其中脾脏中K和Fe含量最高，4 个胃中Ca含量均较高。     

兼香型年份酒中香味物质的分析

通过单因素试验优化顶空固相微萃取（HS-SPME）条件，并结合气相色谱-质谱（GC-MS）技术研究兼香型年份酒中香味物质成分含量及差异。结果表明，最佳HS-SPME萃取条件为酒样酒精度14%vol，萃取温度40 ℃，萃取时间30 min，解吸时间5 min。GC-MS法共鉴定出67种挥发性风味物质，包括50种酯类，3种醇类，5种酸类，1种芳香族化合物，1种含硫化合物，2种呋喃类，3种酮类和2种醛类。酯类、醇类、酸类和呋喃类总含量随贮藏年份增长呈现上升趋势，醛类和酮类总含量变化规律不明显。经香气活度值（OAV）分析，确定出22种（OAV＞1）成分对白酒香味有贡献，其中有9种（OAV＞10）为重要香气成分，酯类为白酒香气的主要贡献物质。