倾斜入射下的单截面平面度绝对检验

针对大尺寸光学平面的直线度的纳米级测量精度需求，提出了倾斜入射下单截面平面度绝对检验方法，实现了对超过相移干涉仪口径的长平晶绝对检验。利用棱镜转向实现倾斜入射角度的精密预标定，棱镜标定角度的精度高于圆光栅和图像分析等方法，可提高测量不确定度到0.0042 μm。对比了常规三面互检绝对检验结果与本方法的差异，在相同尺寸下，直线度误差仅为1.2 nm。在确认标定反射镜位置后，整个倾斜入射的干涉图调整过程将被完全集中到待测长平晶的工作面上，不需要再对反射平晶进行操作。调整长平晶时各个维度的操作互不干涉，可快速简便地得到测量结果。     

Labeling and Characterization of Phenol-Containing Glycopeptides Using Chemoselective Probes with Isotope Tags

Secondary metabolites are structurally diverse natural products (NPs) and have been widely used for medical applications. Developing new tools to enrich NPs can be a promising solution to isolate novel NPs from the native and complex samples. Here, we developed native and deuterated chemoselective labeling probes to target phenol-containing glycopeptides by the ene-type labeling used in proteomic research. The clickable azido-linker was included for further biotin functionalization to facilitate the enrichment of labeled substrates. Afterward, our chemoselective method, in conjunction with LC-MS and MSn analysis, was demonstrated in bacterial cultures. A vancomycin-related phenol-containing glycopeptide was labeled and characterized by our labeling strategy, showing its potential in glycopeptide discovery in complex environments.     

储能水管-冲击式水轮机发电系统设计及发电效益分析

为充分利用高层建筑物内部的水能包括生活污水及高层建筑物顶楼雨水,可将其转化为电能。由此设计的储能水管-冲击式水轮机装置即通过冲击式水轮机和发电机将高层建筑物内部储存的生活污水及雨水的势能转变为可供使用的电能,并通过建立单户用水模拟模型,设置储能水管对30、100层建筑进行发电模拟。模拟结果表明,储能水管-冲击式水轮机发电具有很好的发电效益和节能减排社会效益,获得了日发电过程中冲击式水轮机的水头变换和启停特性,为该系统中冲击式水轮机的个性设计提供了依据。     

锅炉二次风道流动特性的模拟优化

以武汉武锅能源工程有限公司设计的二次风道为对象,运用数值模拟的方法考查了改造前后二次风道各出口空气的速度分布和质量流量分配情况。结果表明,通过布置弧形挡板,风道出口速度的均匀性显著提升,最大变异系数Cv由29%下降到9%,而且还避免了因风速不均引起的烧边现象。此外,改进后风道各出口空气的流量分配非常接近理想工况,与理想工况的偏差从9.9%缩小到2.1%。     

两种发酵方式柑橘果醋品质特性的比较

以柑橘为原料，在单因素试验的基础上通过正交试验对柑橘果醋一次发酵法发酵条件进行优化，并对一次发酵法与二次发酵法制备的柑橘果醋的品质特性进行比较。结果表明，柑橘果醋一次发酵法最优发酵条件为酒精度6.0%vol、柑橘果汁含量为50%、发酵温度34 ℃，在此优化条件下，柑橘果醋中总酸含量为6.0%，酒精转化率为96.31%，分别比优化前提高了0.27%、5.24%。一次发酵法和二次发酵法制备的柑橘果醋中最高总酸含量无显著差异（P＞0.05），但一次发酵法的启动时间比二次发酵法延迟48 h，整个发酵时间延迟了24 h。以柑橘果汁为参比，一次发酵法与二次发酵法制备的柑橘果醋相比，黄色度（b*值）、透光率、嗅觉成分、味觉中的鲜味和丰富度更相近于柑橘果汁。     

Slag eye formation in single and dual bottom purged industrial steelmaking ladles

ABSTRACT

Argon gas is often injected from the bottom of the ladle during steel refining operations. The injected gas interacts with the liquid (metal and slag) bath and enhances the momentum, heat, and mass transfer rate in the melt. However, during these gas–liquid interactions, an opening of the slag layer called slag eye is formed, which exposes the molten metal surface to the atmosphere, which is generally undesirable. In the current work, a transient, three-dimensional mathematical model is used to study the turbulent gas–liquid interactions in single as well as dual bottom blown industrial steelmaking ladles. A Coupled Level Set Volume of Fluid (CLSVOF) model is used for tracking the steel-argon, steel-slag, and argon-slag interfaces, from which the slag-eye area has been predicted. It is found that the inlet gas purging rate, melt height, slag layer thickness, angular and radial positions of the gas inlets affect the slag opening area. Non-dimensional empirical correlations are proposed to predict the slag opening area in both single as well as dual purged ladles, using non-linear regression analysis.     

Automated delineation of non-small cell lung cancer: A step toward quantitative reasoning in medical decision science

Quantitative reasoning in medical decision science relies on the delineation of pathological objects. For example, evidence-based clinical decisions regarding lung diseases require the segmentation of nodules, tumors, or cancers. Non-small cell lung cancer (NSCLC) tends to be large sized, irregularly shaped, and grows against surrounding structures imposing challenges in the segmentation, even for expert clinicians. An automated delineation tool based on spatial analysis was developed and studied on 25 sets of computed tomography scans of NSCLC. Manual and automated delineations were compared, and the proposed method exhibited robustness in terms of the tumor size (5.32–18.24 mm), shape (spherical or irregular), contouring (lobulated, spiculated, or cavitated), localization (solitary, pleural, mediastinal, endobronchial, or tagging), and laterality (left or right lobe) with accuracy between 80% and 99%. Small discrepancies observed between the manual and automated delineations may arise from the variability in the practitioners' definitions of region of interest or imaging artifacts that reduced the tissue resolution.     

对于厚度70mm〜140mm焊缝超声检测的讨论

超声检测作为一种面积型缺陷的有效检测方法,被广泛应用在气化炉、除氧器、汽包等的焊缝检测上。随着近年来电厂、化工厂对质量的要求提升,确保焊缝质量就成了生产制造厂的重点。对于这些重型容器,焊缝厚度普遍在70mm~140mm,在这个厚度区间,采取的多道焊接,工艺控制不严很容易产生缺陷。无损检测标准的制定只是简单的对此厚度划分两个区间,并未给出划定此区间的依据。本文通过实际检测气化炉、除氧器、汽包等焊缝来讨论超声检测在厚度70mm?140mm区间的划定依据。     

探究智能变电站的继电保护二次回路故障诊断问题

本文即针对当前智能变电站中的故障诊断问题展开分析,主要以继电保护二次回路故障检测为主,就诊断检测系统进行阐述,总结了能够针对各种故障问题进行检测手段,意在能够借此提升变电站的智能化发展水平。