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1.
In recent years,iron(Fe)based degradable metal is explored as an alternative to permanent fracture fixation devices.In the present work,copper(Cu)is added in Fe-Mn system to enhance the degradation rate and antimicrobial properties.Fe-Mn-xCu(x=0.9,5 and 10 wt.%)alloys are prepared by the melting-casting-forging route.XRD analysis confirms austenite phase stabilization due to the presence of Mn and Cu.As predicted by Thermo-Calc calculations,Cu rich phase precipitations are noticed along the austen-ite grain boundaries.Degradation behaviours of Cu added Fe-Mn alloys are investigated through static immersion and electrochemical polarization where enhanced degradation is found for higher Cu added alloys.When challenged against E.Coli bacteria,the Fe-Mn-Cu alloy media extract shows a significant bac-tericidal effect compare to the base alloy.In vitro cytocompatibility studies,as determined using MG63 and MC3T3-E1 cell lines,indicate increased cell density as a function of time for all the alloys.When implanted in rabbit femur,the newly developed alloy does not show any kind of tissue necrosis around the implants.Better osteogenesis and higher new bone formation are observed with Fe-Mn-10Cu alloy as evident from micro-computed tomography(μ-CT)and fluorochrome labelling.  相似文献   
2.
《Ceramics International》2020,46(7):9256-9262
Foam ceramics with high strength were successfully fabricated by using sand shale and steel slag as the major materials and SiC as foam agent. The influence of raw materials ratio and heat treatment temperatures on crystalline phases, porosity, mechanical properties and pore structures was investigated via XRF, XRD, SEM, DTA-TG, Micro-CT. The results indicate that the raw materials composed of 94 wt% sand shale and 6 wt% steel slag enable the fabrication of foam ceramics possessing strength of 29.98 MPa, bulk density of 0.821 g/cm3, total porosity of 67.22%, closed porosity of 55.27% and thermal conductivity of 0.08 W/(m·K). Micro-CT result shows that the pores with an average size of 267.05 μm are isolated. Pore wall thickness conforms to normal distribution, and it ranges from 18 to 42 μm. The superior property makes it promising high-strength and lightweight material in application fields, including thermal insulation materials and lightweight building materials.  相似文献   
3.
煤的孔隙结构是影响煤中气体吸附和渗流的一个重要因素。从实现精细化、无损化和定量化入手,应用μCT 225kVFCB型高精度CT试验分析系统,通过显微CT切片,提取研究了4个煤样孔隙分布特征,讨论了煤级、煤显微组分和灰分对煤孔隙结构的影响程度。采用公约数网格序列盒维数法定量表征了孔隙结构的复杂程度和不规则性,探讨了孔隙率、渗透率和分形维数的关系。研究表明,研究煤样的孔隙分布总体受煤显微组分含量控制,同时煤中矿物充填作用在一定程度上降低了煤的孔隙率、平均孔径和孔隙数量。煤孔隙分形维数D的变化与孔隙分布特征密切相关,有效地反映了孔隙结构的非均质性。孔隙率、渗透率与分形维数呈现显著的幂指数正相关关系。由此指示,基于显微CT切片的煤孔隙分形维数可作为煤储层孔隙特征和渗透性评价的定量指标之一。  相似文献   
4.
The challenge associated with large-scale hydrogen storage is a pertinent one to achieve a hydrogen economy. The increasing global demand for clean and green energy is the driving force to propel such an economy. Furthermore, hydrogen is also considered an alternative energy source compared to fossil fuel as a clean energy alternative. Hydrogen geo-storage in a deep saline aquifer, depleted oil and gas reservoirs can resolve this challenge. We assess the potential of a saline aquifer in a sandstone formation to store hydrogen through first-of-its-kind x-ray micro-computed tomography miniature coreflood experiments. The investigation shows that ~65% of the sandstone's pore volume can be occupied by hydrogen when injected at a slow rate. Residual saturation of hydrogen upon brine injection can be ~41%.  相似文献   
5.
《Ceramics International》2021,47(22):31319-31328
Manufacturing lightweight aggregate (LWA) at high temperature is an effective way to immobilize heavy metals in solid waste. This work investigated the performance and solidification mechanism of LWA prepared from copper contaminated soil. The volume expansion of LWA could reach a maximum of 28%, and its lowest density accounted of 1.5 g/cm3, which met the standard requirements. Optical microscope and micro-CT test illustrated that the addition of Cu leaded to obvious phase separation in LWA. The Cu leaching result of LWA first increased and then dropped with the temperature. The XRD test found that the main formation phase of Cu in LWA were t-CuFe2O4 and amorphous phase that they had different acid resistance ability. XPS revealed that the main cause of the agglomeration of liquid phase in LWA was the chain broken reaction between Cu and Si–O tetrahedron. SEM-EDS results showed that the distribution of Cu and Si had a strong correlation, which meant that Cu mostly formed amorphous phase. This work showed the uniqueness of Cu in the high temperature immobilization and pointed out the best immobilization target phase.  相似文献   
6.
通过对炭/炭复合材料纤维束界面不同成型阶段结构和性能的研究,探索束界面在制备过程中的形成规律.采用顶出实验、SEM、Micro-CT、XRD以及Raman对不同成型阶段的炭/炭复合材料中纤维束/基体界面剪切强度、界面层结构进行了分析.结果发现材料密度较低时,石墨化程度增加不利于束界面剪切强度的提高;随着材料密度的增大,束界面剪切强度明显升高.通过对其界面结构进行分析,可以看出在沥青浸渍、炭化和石墨化的制备过程中,炭基体优先在束内形成,然后逐步向束界面层及束间空间发展,最后束界面层组织结构趋于完善.随着热处理温度的升高,其界面层组织结构的石墨化程度逐渐增强,其结晶程度也不断增强.  相似文献   
7.
This study analyzed convective drying of wastewater sludge cakes with three-dimensional cake structures probed using an X-ray micro-computerized tomography scanner (micro-CT), considering the development of cracks and cake morphology. The presence of artificial cracks on cake surface assist drying, but those occurred naturally cannot. The cake surface is noted far from saturation over drying. Moreover, the cracks transport easily moisture to cake surface, hence yielding high surface humidity (and rates) for drying. Comprehensive drying model has to incorporate real boundary conditions for success modeling.  相似文献   
8.
As a polymer material, UPR anchoring material has pyrolysis at high temperature, which directly affect its mechanical stability. Using micro-CT scans and 3D image reconstruction to analysis pyrolysis characteristics and the pore structure evolution of UPR anchoring material at high temperatures, and the results showed that the thermal decomposition cause obvious changes in internal microstructure at high temperatures; the average gray attenuated 20.7%, pore groups number increased 47.5% and pore group size increased 201.5% between 350 °C and 500 °C; organic cemented body corresponding to attenuation coefficient ranges from 0.0163 to 0.0373, the inner pore increased significantly after organic pyrolysis, and connected with each other to form larger pores group; the pyrolysis critical temperature is 350 °C, pyrolysis affects significantly to the internal structure and the density of the material. Mechanical properties decayed significantly at high temperature (400 °C), compressive strength decreased by 95% and pull-out strength decreased by 68.3%.  相似文献   
9.
Progressive failure model is developed to investigate shear behaviors of 2D C/SiC z-pinned joint prepared by chemical vapor infiltration (CVI). It includes progressive failure model of 2D C/SiC composites and cohesive model of faying plane, in order to describe joint nonlinear shear behaviors and z-pin shear-off failure mode, respectively. All cohesive parameters are directly obtained from mechanical properties of 2D C/SiC composites. Results show that the model can almost reproduce joint shear behaviors and z-pin shear-off failure process. Joint failure results from coupled fiber tensile and fiber–matrix shearing damages at faying plane. The model also successfully demonstrates that joint shear properties can be effectively improved by changing z-pin density and diameter. The relationship between joint properties and mechanical properties of 2D C/SiC composites are subsequently obtained with the model. In this sense, joint shear strength increases with cohesive or in-plane shear strengths of 2D C/SiC composites.  相似文献   
10.
显微CT技术及其在生物医学领域的应用   总被引:1,自引:1,他引:0  
专门用于小动物研究的显微CT技术,经过20多年的研究,目前已经非常成熟。本文综述显微CT的发展历史、分类、系统构成及发展趋势,并对其在生物领域的应用作概括描述。最后还对目前显微CT在中国大陆的开发和应用的情况做一总结,作者认为各种基金对CT研究的支持促进显微CT的发展。并提出目前显微CT的研究及应用方面存在的问题,并给出解决这些问题的初步设想。  相似文献   
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