光电直读光谱仪在管线钢成分分析中的应用

为了进一步提高SPECTRO LAB直读光谱仪在管线钢成分分析中的准确度和效率，通过参数调整及控样研究，对直读光谱仪分析方法进行了优化，并提出了两种优化方案。结果表明，调整光源参数，能够缩短试验分析时间，减少氩气消耗；综合控样的研究实施，可以解决多块标样分步骤操作的繁琐和误差，省时省力。经实践验证，优化后的方案能够满足生产检验要求，分析方法简单、快捷，降低了成本消耗。     

葡萄酒高级醇检测方法的优化及其在本土酿酒酵母筛选中的应用

该研究在国标GB/T 5009.48—2003《蒸馏酒与配制酒卫生标准的分析方法》的基础上，建立起一种显色稳定、准确性更高的高级醇检测法。结果表明，当葡萄酒酒样在梯度稀释20倍，加样静置1 min，80 ℃水浴30 min且以50%硫酸溶液作为稀释剂的条件下进行检测，精密度试验结果相对标准偏差（RSD）为1.665%，加标回收率为99.11%，均优于国标法；采用气质联用（GC-MS）法对6株本土酵母产高级醇含量进行对比检测，结果显示所测总量无显著差异（P＞0.05），证明优化法较为准确、可靠。该研究筛选获得了两株低产高级醇菌株LFP529和LFP525，其发酵酒的高级醇含量较对照分别降低了55.44%、58.31%，为解决我国部分产区葡萄酒高级醇含量较高提供了解决方案。     

数字化羊绒测色法及其在长度测量中的应用

针对光电法测试纤维长度等性质时,存在纤维的透光及反光信号与颜色高度相关的问题,采用数字化方法表征羊绒的颜色类别并精准地测量羊绒的长度。将彩色光电耦合器作为测色传感器,搭建了更适合纤维材料的测色装置;通过颜色模型在3种色空间的转换,得到3类颜色的羊绒在三维色空间的分布;基于系列实验,创建了有色羊绒的光学参数即无穷厚时的表观反射率表观反射率与测色装置计算的亮度指标之间的换算模型,并用实验证明采用测得的表观反射率可计算得到准确的须丛线密度曲线,从而可用光电法精准测量有色羊绒的长度。结果表明,该测色方法的测样面积大,代表性好,成本低,同时可用于其他纤维和纺织品的颜色测量。     

Categorical observers for metamerism

A method is proposed to generate categorical colour observer functions (individual colour matching functions) for any field size based on the CIE 2006 system of physiological observer functions. The method combines proposed categorical observer techniques of Sarkar et al with a physiologically-based individual observer model of Asano et al and a clustering technique to produce the optimal set of categorical observers. The number of required categorical observers varies depending on an application with as many as 50 required to predict individual observers' matches when a laser projector is viewed. However, 10 categorical observers are sufficient to represent colour-normal populations for personalized colour imaging. The proposed and recommended categorical observers represent a robust and inclusive technique to examine and quantify observer metamerism in any application of colorimetry.     

柔性钙钛矿太阳能电池的制备及性能研究

采用钛箔作为衬底,原位生长二氧化钛薄膜,然后制备有机钙钛矿吸收层及固态空穴传输层,组装成太阳能电池。通过电压-电流曲线测试,结果表明,这种钙钛矿太阳能电池的光生电压达到0.8 V、光生电流达到16 mA/cm²、光电转化效率为10.2%。进一步对电池进行弯折试验,弯折20次后,光电转化效率能达到初始值的85%,表现出良好的柔性特征。     

Naming the colors: Color names designation from the colorimetric values. The French GPEM/PV work revisited

This publication describes a work related to the French language, for assigning a color name to an object whose colorimetric characteristics have been measured. This is the subject of a recently published book. The work is the result of an old publication by Afnor, the French standardization organization, work unfortunately obsolete by its colorimetric part. This publication describes the work that has been done to update it and make it convenient to use. The present text, by publishing some of the tables and graphs of the French book, presents the work done in French by a method that differs from that used by Kelly and Judd years ago.     

Reinvestigation of the photostrictive effect in lanthanum-modified lead zirconate titanate ferroelectrics

Photostriction of lanthanum-modified lead zirconate titanate (PLZT) was commonly attributed to the combination of anomalous photovoltaic effect and inverse piezoelectric response. Herein, distinct photostrictions are detected in both poled and unpoled PLZT ceramics under 405 and 520 nm laser illuminations. The maximum photostriction around 0.09% is obtained in unpoled PLZT under 405 nm illumination, which is nine times of previously reported value that deduced from poled PLZT. The photoelectric and photovoltaic characterizations of poled/unpoled PLZT further evidence that the detected photostriction shows no direct association with the photovoltage-induced inverse piezoresponse. The light-induced microstructure changes observed by in situ piezoelectric force microscopy are revealed by domain evolutions along the boundaries. The possible photostriction mechanism of PLZT is attributed to the strong photo-induced electron-lattice coupling, which is suggested by the light-induced changes of the Zr/Ti-O-Zr/Ti bonds reflected by the power-dependent Raman spectra. This study extends the photostriction of PLZT to visible light range and will also stimulate reappraisal of the underlying mechanism of photostrictive effect involving ferroelectrics.     

多功能食品安全综合快速现场检测仪设计

目的设计一种食品安全快速检测仪,实现多功能、高通量检测与数据采集传输一体化,提高食品安全现场检测效率。方法通过分析比色法、酶联免疫法(enzyme-linked immunosorbent assay,ELISA)、胶体金试纸及相应仪器的工作原理,依据现场快速检测的实际需求,提出了基于分光光度法的单光束与多光束光路集成的仪器优化方案和一种基于图像处理技术的现场胶体金试纸自动快速检测方案。以MC9S12XS128单片机为控制核心,设计搭建了分光机构、胶体金试纸图像采集、试样容器、光电转换与信号调理电路等模块,实现了4通道和96通道ELISA的光路转换、信号采集与处理、试样载板控制、胶体金多元检测等功能。结果 ELISA检测模块光度准确度?T1.403%,光度重复度δT0.14%,通道间透光率差异小于0.97%;比色检测模块光度准确度?T1.650%,光度重复度δT0.50%;胶体金试纸自动读取模块,快检试纸的量化结果与真值的相关度r~2=0.84。结论 ELISA模块和比色法各项指标符合食品安全快速检测的应用要求,胶体金试纸自动读取模块量化结果与真值的相关度低于要求,需要继续进行算法和装置的优化。     

智能光电选矿预选抛废技术研究及应用

随着国家对矿产资源开采的不断深入,富矿石、易选矿石逐渐枯竭,入选的贫矿石和难选矿石比例不断上升,导致生产处理成本增加。人工智能、智能光电选矿技术,可以甄别和分拣矿石,实现提前抛废,对矿石进行预富集,提高矿石的入选品位,提升矿石综合利用率,成为解决经济增长中矿产资源短缺重要手段,确保矿产资源安全和矿业经济稳定发展的研究方向。     

德兴铜矿酸碱废水水质分析方法

为了给德兴铜矿酸碱废水治理工艺提供准确的酸性废水的酸度，碱性废水的碱度，TFe和Fe^2 以及CaCO3的浓度数据，进行分析方法的研究和探讨。采用电位洋定法测定酸度碱度，辈我啉比色法测定TFe和Fe^2 ，以及用修列达法（JISK／451）测定尾矿浆碱水中的CaCO3含量。介绍分析方法的改进，分析过程步骤和分析结果。